Tert-butyl-diphenylmethylnitroxyl radical formation with the reaction of triphenylbismuth dicrotonate and C-phenyl-N-tert-butylnitrone in benzene

Decomposition of triphenylbismuth dicrotonate in diffused light in bensene in the presence of spin trap of C-phenyl-N-tert-butylnitrone leads to formation of phenyl radicals which are registered as the adduct PhCH(Ph)N(O•)Bu-t. Triphenylbismuth dicrotonate Ph3Bi(O2CCH=CHCH3)2 in benzene solition in...

Full description

Saved in:
Bibliographic Details
Main Authors: A. V. Gushchin, O. S. Kalistratova, A. I. Maleeva, V. A. Kuropatov, D. N. Yemelyanov
Format: Article
Language:English
Published: Ural Federal University 2017-09-01
Series:Chimica Techno Acta
Subjects:
Online Access:https://chimicatechnoacta.ru/article/view/2247
Tags: Add Tag
No Tags, Be the first to tag this record!
Description
Summary:Decomposition of triphenylbismuth dicrotonate in diffused light in bensene in the presence of spin trap of C-phenyl-N-tert-butylnitrone leads to formation of phenyl radicals which are registered as the adduct PhCH(Ph)N(O•)Bu-t. Triphenylbismuth dicrotonate Ph3Bi(O2CCH=CHCH3)2 in benzene solition in the presence of C-phenyl-N-tert-butylnitrone PhCH=N(O)Bu-t decomposes in light. An adduct of phenyl radical and spin trap PhCH(Ph)N(O•)Bu-t was registered by ESR method.
ISSN:2411-1414