DNA Methylation Markers and the Identification of Buccal Samples for Forensic Tissue Determination

Background: The identification of body fluids collected from crime scenes is crucial for determining the type and nature of assaults and for advancing the resolution of crimes. Objectives: The primary aim of this study was to investigate tissue-specific DNA methylation markers that can effectively d...

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Main Authors: Kuppareddi Balamurugan, Elizabeth Staples, Hussain Alghanim, George Duncan, Bruce McCord
Format: Article
Language:English
Published: MDPI AG 2025-06-01
Series:Forensic Sciences
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Online Access:https://www.mdpi.com/2673-6756/5/2/26
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author Kuppareddi Balamurugan
Elizabeth Staples
Hussain Alghanim
George Duncan
Bruce McCord
author_facet Kuppareddi Balamurugan
Elizabeth Staples
Hussain Alghanim
George Duncan
Bruce McCord
author_sort Kuppareddi Balamurugan
collection DOAJ
description Background: The identification of body fluids collected from crime scenes is crucial for determining the type and nature of assaults and for advancing the resolution of crimes. Objectives: The primary aim of this study was to investigate tissue-specific DNA methylation markers that can effectively distinguish buccal samples from blood, semen, and vaginal epithelial tissue. Methods: We screened various markers and selected four genomic locations for further analysis. Genomic DNA was extracted from tissue samples, followed by bisulfite conversion, locus-specific polymerase chain reaction (PCR) amplification, and pyrosequencing. Results: Four loci—cg-9652652, cg-11536474, cg-3867465, and cg-10122865—along with several adjacent CpG sites, were found to be hypermethylated in buccal samples compared to other tissue types. The difference in DNA methylation of buccal samples was statistically significant (<i>p</i> < 0.0001) compared to other tissues, indicating the potential usefulness of these loci for forensic tissue identification. Two additional studies were conducted: (a) a species specificity study and (b) a mixture study involving two different tissue types. The species specificity study showed that the primers used in the assay were specific to primates and humans. They did not amplify five non-primate samples, while the two primate samples—chimpanzee and rhesus—provided usable methylation data. The mixture study involved DNA from two different tissues—buccal samples and semen—combined in varying proportions. The results showed a decrease in the overall percentage of DNA methylation at the locus cg-9652652 as well as five adjacent CpG sites when the amount of buccal cell DNA in the mixture was reduced. Conclusion: The specificity of the primers and the significant differences in percent DNA methylation between buccal cells and other tissues make these markers excellent candidates for forensic tissue identification.
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spelling doaj-art-e34d237a7a8845749b411f7687153aa72025-08-20T03:27:10ZengMDPI AGForensic Sciences2673-67562025-06-01522610.3390/forensicsci5020026DNA Methylation Markers and the Identification of Buccal Samples for Forensic Tissue DeterminationKuppareddi Balamurugan0Elizabeth Staples1Hussain Alghanim2George Duncan3Bruce McCord4School of Criminal Justice, Forensic Science, and Security, The University of Southern Mississippi, Hattiesburg, MS 39406, USASchool of Criminal Justice, Forensic Science, and Security, The University of Southern Mississippi, Hattiesburg, MS 39406, USAGeneral Department of Forensic Science and Criminology, Dubai Police, Dubai P.O. Box 1493, United Arab EmiratesNova Southeastern University, Dania Beach, FL 33004, USADepartment of Chemistry and Biochemistry, Florida International University, Miami, FL 33199, USABackground: The identification of body fluids collected from crime scenes is crucial for determining the type and nature of assaults and for advancing the resolution of crimes. Objectives: The primary aim of this study was to investigate tissue-specific DNA methylation markers that can effectively distinguish buccal samples from blood, semen, and vaginal epithelial tissue. Methods: We screened various markers and selected four genomic locations for further analysis. Genomic DNA was extracted from tissue samples, followed by bisulfite conversion, locus-specific polymerase chain reaction (PCR) amplification, and pyrosequencing. Results: Four loci—cg-9652652, cg-11536474, cg-3867465, and cg-10122865—along with several adjacent CpG sites, were found to be hypermethylated in buccal samples compared to other tissue types. The difference in DNA methylation of buccal samples was statistically significant (<i>p</i> < 0.0001) compared to other tissues, indicating the potential usefulness of these loci for forensic tissue identification. Two additional studies were conducted: (a) a species specificity study and (b) a mixture study involving two different tissue types. The species specificity study showed that the primers used in the assay were specific to primates and humans. They did not amplify five non-primate samples, while the two primate samples—chimpanzee and rhesus—provided usable methylation data. The mixture study involved DNA from two different tissues—buccal samples and semen—combined in varying proportions. The results showed a decrease in the overall percentage of DNA methylation at the locus cg-9652652 as well as five adjacent CpG sites when the amount of buccal cell DNA in the mixture was reduced. Conclusion: The specificity of the primers and the significant differences in percent DNA methylation between buccal cells and other tissues make these markers excellent candidates for forensic tissue identification.https://www.mdpi.com/2673-6756/5/2/26DNA methylationepigeneticsbuccal cellssalivaforensicstissue identification
spellingShingle Kuppareddi Balamurugan
Elizabeth Staples
Hussain Alghanim
George Duncan
Bruce McCord
DNA Methylation Markers and the Identification of Buccal Samples for Forensic Tissue Determination
Forensic Sciences
DNA methylation
epigenetics
buccal cells
saliva
forensics
tissue identification
title DNA Methylation Markers and the Identification of Buccal Samples for Forensic Tissue Determination
title_full DNA Methylation Markers and the Identification of Buccal Samples for Forensic Tissue Determination
title_fullStr DNA Methylation Markers and the Identification of Buccal Samples for Forensic Tissue Determination
title_full_unstemmed DNA Methylation Markers and the Identification of Buccal Samples for Forensic Tissue Determination
title_short DNA Methylation Markers and the Identification of Buccal Samples for Forensic Tissue Determination
title_sort dna methylation markers and the identification of buccal samples for forensic tissue determination
topic DNA methylation
epigenetics
buccal cells
saliva
forensics
tissue identification
url https://www.mdpi.com/2673-6756/5/2/26
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