The Application of Response Surface Methodology for Lead Ion Removal from Aqueous Solution Using Intercalated Tartrate-Mg-Al Layered Double Hydroxides

Layered double hydroxide intercalated with tartrate (tartrate-Mg-Al) was used as an adsorbent to remove lead ions from aqueous solutions. The effects of various optimization parameters such as contact time, solution pH, lead ion concentrations, and adsorbent dosage were investigated by the use of Re...

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Main Authors: Yamin Yasin, Maszlin Mohamad, Faujan B. H. Ahmad
Format: Article
Language:English
Published: Wiley 2013-01-01
Series:International Journal of Chemical Engineering
Online Access:http://dx.doi.org/10.1155/2013/937675
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author Yamin Yasin
Maszlin Mohamad
Faujan B. H. Ahmad
author_facet Yamin Yasin
Maszlin Mohamad
Faujan B. H. Ahmad
author_sort Yamin Yasin
collection DOAJ
description Layered double hydroxide intercalated with tartrate (tartrate-Mg-Al) was used as an adsorbent to remove lead ions from aqueous solutions. The effects of various optimization parameters such as contact time, solution pH, lead ion concentrations, and adsorbent dosage were investigated by the use of Response Surface Methodology (RSM). The Response Surface Methodology (RSM) based on a four-level four-variable Central Composite Rotatable Design (CCRD) was employed to evaluate the interactive effects of the various optimization parameters. The parameters were contact time (6–10 h), solution pH (1–3), adsorbent dosage (0.06–0.1 g), and lead ion concentrations (10–30 mg/L). The percentage of lead ions removal for each of the parameters studied was determined by Inductively Coupled Plasma-Optical Emission Spectrophotometer. Simultaneously by increasing contact time and amount of dosage of tartrate-Mg-Al used the percentage of lead ions removal from aqueous solution will increase; however, the percentage removal decreases with an increase in pH and concentrations of lead ions. The experimental percentage removal recorded under optimum conditions was compared well with the maximum predicted value from the RSM, which suggest that Central Composite Rotatable Design of RSM can be used to study the removal of lead from aqueous solution by the use of tartrate-Mg-Al as an adsorbent.
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spelling doaj-art-e33964d6625042f287a3340bcfd5dcfd2025-08-20T03:21:07ZengWileyInternational Journal of Chemical Engineering1687-806X1687-80782013-01-01201310.1155/2013/937675937675The Application of Response Surface Methodology for Lead Ion Removal from Aqueous Solution Using Intercalated Tartrate-Mg-Al Layered Double HydroxidesYamin Yasin0Maszlin Mohamad1Faujan B. H. Ahmad2INTEC Education College, Universiti Teknologi MARA, 40450 Shah Alam, MalaysiaFaculty of Applied Sciences, Universiti Teknologi MARA, 40450 Shah Alam, MalaysiaFaculty of Applied Sciences, Universiti Teknologi MARA, 40450 Shah Alam, MalaysiaLayered double hydroxide intercalated with tartrate (tartrate-Mg-Al) was used as an adsorbent to remove lead ions from aqueous solutions. The effects of various optimization parameters such as contact time, solution pH, lead ion concentrations, and adsorbent dosage were investigated by the use of Response Surface Methodology (RSM). The Response Surface Methodology (RSM) based on a four-level four-variable Central Composite Rotatable Design (CCRD) was employed to evaluate the interactive effects of the various optimization parameters. The parameters were contact time (6–10 h), solution pH (1–3), adsorbent dosage (0.06–0.1 g), and lead ion concentrations (10–30 mg/L). The percentage of lead ions removal for each of the parameters studied was determined by Inductively Coupled Plasma-Optical Emission Spectrophotometer. Simultaneously by increasing contact time and amount of dosage of tartrate-Mg-Al used the percentage of lead ions removal from aqueous solution will increase; however, the percentage removal decreases with an increase in pH and concentrations of lead ions. The experimental percentage removal recorded under optimum conditions was compared well with the maximum predicted value from the RSM, which suggest that Central Composite Rotatable Design of RSM can be used to study the removal of lead from aqueous solution by the use of tartrate-Mg-Al as an adsorbent.http://dx.doi.org/10.1155/2013/937675
spellingShingle Yamin Yasin
Maszlin Mohamad
Faujan B. H. Ahmad
The Application of Response Surface Methodology for Lead Ion Removal from Aqueous Solution Using Intercalated Tartrate-Mg-Al Layered Double Hydroxides
International Journal of Chemical Engineering
title The Application of Response Surface Methodology for Lead Ion Removal from Aqueous Solution Using Intercalated Tartrate-Mg-Al Layered Double Hydroxides
title_full The Application of Response Surface Methodology for Lead Ion Removal from Aqueous Solution Using Intercalated Tartrate-Mg-Al Layered Double Hydroxides
title_fullStr The Application of Response Surface Methodology for Lead Ion Removal from Aqueous Solution Using Intercalated Tartrate-Mg-Al Layered Double Hydroxides
title_full_unstemmed The Application of Response Surface Methodology for Lead Ion Removal from Aqueous Solution Using Intercalated Tartrate-Mg-Al Layered Double Hydroxides
title_short The Application of Response Surface Methodology for Lead Ion Removal from Aqueous Solution Using Intercalated Tartrate-Mg-Al Layered Double Hydroxides
title_sort application of response surface methodology for lead ion removal from aqueous solution using intercalated tartrate mg al layered double hydroxides
url http://dx.doi.org/10.1155/2013/937675
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