Durability of Ag-TiO2 Photocatalysts Assessed for the Degradation of Dichloroacetic Acid

The stability of Ag-TiO2 photocatalysts was examined for the photocatalytic degradation of dichloroacetic acid (DCA) as a function of the recycling times. The photocatalytic activity was investigated by measuring the rate of H+ ions released during the photodegradation of DCA and confirmed by measur...

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Main Authors: Víctor M. Menéndez-Flores, Donia Friedmann, Detlef W. Bahnemann
Format: Article
Language:English
Published: Wiley 2008-01-01
Series:International Journal of Photoenergy
Online Access:http://dx.doi.org/10.1155/2008/280513
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author Víctor M. Menéndez-Flores
Donia Friedmann
Detlef W. Bahnemann
author_facet Víctor M. Menéndez-Flores
Donia Friedmann
Detlef W. Bahnemann
author_sort Víctor M. Menéndez-Flores
collection DOAJ
description The stability of Ag-TiO2 photocatalysts was examined for the photocatalytic degradation of dichloroacetic acid (DCA) as a function of the recycling times. The photocatalytic activity was investigated by measuring the rate of H+ ions released during the photodegradation of DCA and confirmed by measuring the total organic carbon removal. The photodegradation reactions were studied at pH 3 and pH 10 for a series of Ag-TiO2 photocatalysts as different with Ag loadings . All the Ag-TiO2 and bare TiO2 photocatalysts showed a decrease in photocatalytic activity on recycling for the DCA photodegradation reaction. The decrease in activity can be attributed to poisoning of active sites by Cl− anions formed during the photocatalytic DCA degradation. The photocatalytic activity was, however, easily recovered by a simple washing technique. The reversibility of the poisoning is taken as evidence to support the idea that the recycling of Ag-P25 TiO2 photocatalysts does not have a permanent negative effect on their photocatalytic performance for the degradation of DCA. The choice of the preparation procedure for the Ag-TiO2 photocatalysts is shown to be of significant importance for the observed changes in the photocatalytic activity of the Ag-TiO2 particles.
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issn 1110-662X
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language English
publishDate 2008-01-01
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series International Journal of Photoenergy
spelling doaj-art-e31523c55fdc4167a3d0c265b8a794162025-08-20T02:21:24ZengWileyInternational Journal of Photoenergy1110-662X1687-529X2008-01-01200810.1155/2008/280513280513Durability of Ag-TiO2 Photocatalysts Assessed for the Degradation of Dichloroacetic AcidVíctor M. Menéndez-Flores0Donia Friedmann1Detlef W. Bahnemann2Institut für Technische Chemie, Leibniz Universität Hannover, Callinstraße 3, D-30167 Hannover, GermanyInterdisciplinary Nanoscience Center, University of Aarhus, Building 520, 8000 Aarhus C, DenmarkInstitut für Technische Chemie, Leibniz Universität Hannover, Callinstraße 3, D-30167 Hannover, GermanyThe stability of Ag-TiO2 photocatalysts was examined for the photocatalytic degradation of dichloroacetic acid (DCA) as a function of the recycling times. The photocatalytic activity was investigated by measuring the rate of H+ ions released during the photodegradation of DCA and confirmed by measuring the total organic carbon removal. The photodegradation reactions were studied at pH 3 and pH 10 for a series of Ag-TiO2 photocatalysts as different with Ag loadings . All the Ag-TiO2 and bare TiO2 photocatalysts showed a decrease in photocatalytic activity on recycling for the DCA photodegradation reaction. The decrease in activity can be attributed to poisoning of active sites by Cl− anions formed during the photocatalytic DCA degradation. The photocatalytic activity was, however, easily recovered by a simple washing technique. The reversibility of the poisoning is taken as evidence to support the idea that the recycling of Ag-P25 TiO2 photocatalysts does not have a permanent negative effect on their photocatalytic performance for the degradation of DCA. The choice of the preparation procedure for the Ag-TiO2 photocatalysts is shown to be of significant importance for the observed changes in the photocatalytic activity of the Ag-TiO2 particles.http://dx.doi.org/10.1155/2008/280513
spellingShingle Víctor M. Menéndez-Flores
Donia Friedmann
Detlef W. Bahnemann
Durability of Ag-TiO2 Photocatalysts Assessed for the Degradation of Dichloroacetic Acid
International Journal of Photoenergy
title Durability of Ag-TiO2 Photocatalysts Assessed for the Degradation of Dichloroacetic Acid
title_full Durability of Ag-TiO2 Photocatalysts Assessed for the Degradation of Dichloroacetic Acid
title_fullStr Durability of Ag-TiO2 Photocatalysts Assessed for the Degradation of Dichloroacetic Acid
title_full_unstemmed Durability of Ag-TiO2 Photocatalysts Assessed for the Degradation of Dichloroacetic Acid
title_short Durability of Ag-TiO2 Photocatalysts Assessed for the Degradation of Dichloroacetic Acid
title_sort durability of ag tio2 photocatalysts assessed for the degradation of dichloroacetic acid
url http://dx.doi.org/10.1155/2008/280513
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AT doniafriedmann durabilityofagtio2photocatalystsassessedforthedegradationofdichloroaceticacid
AT detlefwbahnemann durabilityofagtio2photocatalystsassessedforthedegradationofdichloroaceticacid