Comprehensive Characterization and Comparison of Aroma Profiles of <i>Tricholoma matsutake</i> Soup During the Cooking Process by HS-GC-IMS and HS-SPME-GC-MS

Many scholars have studied <i>Tricholoma matsutake</i> soup, but there are relatively few studies exploring the aroma changes during its cooking process using different detection methods. The aroma of <i>T. matsutake</i> soup was analyzed and compared using electronic nose (E...

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Main Authors: Ni-Na Yan, Cheng-Jian Xu, Shuang-Li Xiong, Xiang Li, Si-Yu Gu, Zhong-Yan Zhu, Yang Liu, Nan Zhu, Yu Zhou, Hang Xiao
Format: Article
Language:English
Published: MDPI AG 2025-04-01
Series:Foods
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Online Access:https://www.mdpi.com/2304-8158/14/9/1478
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author Ni-Na Yan
Cheng-Jian Xu
Shuang-Li Xiong
Xiang Li
Si-Yu Gu
Zhong-Yan Zhu
Yang Liu
Nan Zhu
Yu Zhou
Hang Xiao
author_facet Ni-Na Yan
Cheng-Jian Xu
Shuang-Li Xiong
Xiang Li
Si-Yu Gu
Zhong-Yan Zhu
Yang Liu
Nan Zhu
Yu Zhou
Hang Xiao
author_sort Ni-Na Yan
collection DOAJ
description Many scholars have studied <i>Tricholoma matsutake</i> soup, but there are relatively few studies exploring the aroma changes during its cooking process using different detection methods. The aroma of <i>T. matsutake</i> soup was analyzed and compared using electronic nose (E-nose) analysis, headspace gas chromatography-ion mobility spectrometry (HS-GC-IMS), and headspace-solid-phase microextraction-gas chromatography-mass spectrometry (HS-SPME-GC-MS). A significant effect of cooking time on the overall aroma profile of <i>T. matsutake</i> soup was identified through E-nose analysis. By HS-GC-IMS and HS-SPME-GC-MS analysis, 51 volatile aroma compounds were detected, with alcohols and aldehydes identified as the main aroma substances. Based on the relative odor activity value (ROAV) and multivariate statistical analysis, 1-octen-3-ol, 1-octanol, methyl cinnamate, and 2-pentyl furan were determined to be the key aroma compounds in the cooking process. We observed that shorter cooking time preserved the mushroom aroma of <i>T. matsutake</i> soup most effectively. These findings can be utilized for the industrial production of <i>T. matsutake</i> soup and for optimization of its key aroma components.
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spelling doaj-art-e2863f89eb2340b4a3bc62f69738ee942025-08-20T02:24:46ZengMDPI AGFoods2304-81582025-04-01149147810.3390/foods14091478Comprehensive Characterization and Comparison of Aroma Profiles of <i>Tricholoma matsutake</i> Soup During the Cooking Process by HS-GC-IMS and HS-SPME-GC-MSNi-Na Yan0Cheng-Jian Xu1Shuang-Li Xiong2Xiang Li3Si-Yu Gu4Zhong-Yan Zhu5Yang Liu6Nan Zhu7Yu Zhou8Hang Xiao9Key Laboratory of Sichuan Cuisine Artificial Intelligence, Sichuan Tourism University, Chengdu 610100, ChinaKey Laboratory of Sichuan Cuisine Artificial Intelligence, Sichuan Tourism University, Chengdu 610100, ChinaKey Laboratory of Sichuan Cuisine Artificial Intelligence, Sichuan Tourism University, Chengdu 610100, ChinaKey Laboratory of Sichuan Cuisine Artificial Intelligence, Sichuan Tourism University, Chengdu 610100, ChinaKey Laboratory of Sichuan Cuisine Artificial Intelligence, Sichuan Tourism University, Chengdu 610100, ChinaKey Laboratory of Sichuan Cuisine Artificial Intelligence, Sichuan Tourism University, Chengdu 610100, ChinaKey Laboratory of Sichuan Cuisine Artificial Intelligence, Sichuan Tourism University, Chengdu 610100, ChinaKey Laboratory of Sichuan Cuisine Artificial Intelligence, Sichuan Tourism University, Chengdu 610100, ChinaKey Laboratory of Sichuan Cuisine Artificial Intelligence, Sichuan Tourism University, Chengdu 610100, ChinaDepartment of Food Science, University of Massachusetts, Amherst, MA 01003, USAMany scholars have studied <i>Tricholoma matsutake</i> soup, but there are relatively few studies exploring the aroma changes during its cooking process using different detection methods. The aroma of <i>T. matsutake</i> soup was analyzed and compared using electronic nose (E-nose) analysis, headspace gas chromatography-ion mobility spectrometry (HS-GC-IMS), and headspace-solid-phase microextraction-gas chromatography-mass spectrometry (HS-SPME-GC-MS). A significant effect of cooking time on the overall aroma profile of <i>T. matsutake</i> soup was identified through E-nose analysis. By HS-GC-IMS and HS-SPME-GC-MS analysis, 51 volatile aroma compounds were detected, with alcohols and aldehydes identified as the main aroma substances. Based on the relative odor activity value (ROAV) and multivariate statistical analysis, 1-octen-3-ol, 1-octanol, methyl cinnamate, and 2-pentyl furan were determined to be the key aroma compounds in the cooking process. We observed that shorter cooking time preserved the mushroom aroma of <i>T. matsutake</i> soup most effectively. These findings can be utilized for the industrial production of <i>T. matsutake</i> soup and for optimization of its key aroma components.https://www.mdpi.com/2304-8158/14/9/1478<i>Tricholoma matsutake</i>HS-GC-IMSHS-SPME-GC-MSROAVvolatile compounds
spellingShingle Ni-Na Yan
Cheng-Jian Xu
Shuang-Li Xiong
Xiang Li
Si-Yu Gu
Zhong-Yan Zhu
Yang Liu
Nan Zhu
Yu Zhou
Hang Xiao
Comprehensive Characterization and Comparison of Aroma Profiles of <i>Tricholoma matsutake</i> Soup During the Cooking Process by HS-GC-IMS and HS-SPME-GC-MS
Foods
<i>Tricholoma matsutake</i>
HS-GC-IMS
HS-SPME-GC-MS
ROAV
volatile compounds
title Comprehensive Characterization and Comparison of Aroma Profiles of <i>Tricholoma matsutake</i> Soup During the Cooking Process by HS-GC-IMS and HS-SPME-GC-MS
title_full Comprehensive Characterization and Comparison of Aroma Profiles of <i>Tricholoma matsutake</i> Soup During the Cooking Process by HS-GC-IMS and HS-SPME-GC-MS
title_fullStr Comprehensive Characterization and Comparison of Aroma Profiles of <i>Tricholoma matsutake</i> Soup During the Cooking Process by HS-GC-IMS and HS-SPME-GC-MS
title_full_unstemmed Comprehensive Characterization and Comparison of Aroma Profiles of <i>Tricholoma matsutake</i> Soup During the Cooking Process by HS-GC-IMS and HS-SPME-GC-MS
title_short Comprehensive Characterization and Comparison of Aroma Profiles of <i>Tricholoma matsutake</i> Soup During the Cooking Process by HS-GC-IMS and HS-SPME-GC-MS
title_sort comprehensive characterization and comparison of aroma profiles of i tricholoma matsutake i soup during the cooking process by hs gc ims and hs spme gc ms
topic <i>Tricholoma matsutake</i>
HS-GC-IMS
HS-SPME-GC-MS
ROAV
volatile compounds
url https://www.mdpi.com/2304-8158/14/9/1478
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