The Influence of Synthesis Temperature on the Structure, Composition and Magnetic Properties of Nanocomposites NiCo/C

By method of IR-pyrolysis the precursor of polyacrylonitrile and compounds of cobalt and nickel metalcarbon nanocomposites were obtained, representing nanoparticles of alloy NiCo, dispersed in nanocrystalline carbon matrix. NiCo / C nanocomposites are ferromagnets. Magnetization and the coercive for...

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Main Authors: D.G. Muratov, L.V. Kozhitov, S.G. Emelyanov, E.V. Yakushko, M.F. Bulatov
Format: Article
Language:English
Published: Sumy State University 2015-12-01
Series:Журнал нано- та електронної фізики
Subjects:
Online Access:http://jnep.sumdu.edu.ua/download/numbers/2015/4/articles/jnep_2015_V7_04071.pdf
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author D.G. Muratov
L.V. Kozhitov
S.G. Emelyanov
E.V. Yakushko
M.F. Bulatov
author_facet D.G. Muratov
L.V. Kozhitov
S.G. Emelyanov
E.V. Yakushko
M.F. Bulatov
author_sort D.G. Muratov
collection DOAJ
description By method of IR-pyrolysis the precursor of polyacrylonitrile and compounds of cobalt and nickel metalcarbon nanocomposites were obtained, representing nanoparticles of alloy NiCo, dispersed in nanocrystalline carbon matrix. NiCo / C nanocomposites are ferromagnets. Magnetization and the coercive force depends on the size and composition of the alloy nanoparticles NiCo. The average size of metal nanoparticles is determined by the synthesis temperature and in range of 350-800 °C is 10-80 nm, respectively. According to the results of TEM it was detected that with increasing synthesis temperature the maximum synthesis of nanoparticles size distribution shifts to larger sizes. The magnetization and coercivity depend on the size and composition of the nanoparticles of alloy NiCo. With increasing synthesis temperature from 350 to 800 °C the magnetization increases from 0.055 to 17 A·m2/kg.
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issn 2077-6772
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publisher Sumy State University
record_format Article
series Журнал нано- та електронної фізики
spelling doaj-art-e1aba99e7b9043e388b38c7d4211abef2025-08-20T03:24:52ZengSumy State UniversityЖурнал нано- та електронної фізики2077-67722015-12-017404071-104071-4The Influence of Synthesis Temperature on the Structure, Composition and Magnetic Properties of Nanocomposites NiCo/CD.G. Muratov0L.V. Kozhitov1S.G. Emelyanov2E.V. Yakushko3M.F. Bulatov4National University of Science and Technology «MISiS», 4, Leninsky Pr., 119049 Moscow, RussiaNational University of Science and Technology «MISiS», 4, Leninsky Pr., 119049 Moscow, RussiaSouth-West State University, 94, 50 let Oktyabrya St., 305040 Kursk, RussiaNational University of Science and Technology «MISiS», 4, Leninsky Pr., 119049 Moscow, RussiaFederal State Research and Design Institute of Rare Metal Industry, 5-1, B. Tolmachevsky Lane, Moscow, RussiaBy method of IR-pyrolysis the precursor of polyacrylonitrile and compounds of cobalt and nickel metalcarbon nanocomposites were obtained, representing nanoparticles of alloy NiCo, dispersed in nanocrystalline carbon matrix. NiCo / C nanocomposites are ferromagnets. Magnetization and the coercive force depends on the size and composition of the alloy nanoparticles NiCo. The average size of metal nanoparticles is determined by the synthesis temperature and in range of 350-800 °C is 10-80 nm, respectively. According to the results of TEM it was detected that with increasing synthesis temperature the maximum synthesis of nanoparticles size distribution shifts to larger sizes. The magnetization and coercivity depend on the size and composition of the nanoparticles of alloy NiCo. With increasing synthesis temperature from 350 to 800 °C the magnetization increases from 0.055 to 17 A·m2/kg.http://jnep.sumdu.edu.ua/download/numbers/2015/4/articles/jnep_2015_V7_04071.pdfMetal-carbon nanocompositesNanoparticles NiCoMagnetic properties of nanoparticlesIR-heatin
spellingShingle D.G. Muratov
L.V. Kozhitov
S.G. Emelyanov
E.V. Yakushko
M.F. Bulatov
The Influence of Synthesis Temperature on the Structure, Composition and Magnetic Properties of Nanocomposites NiCo/C
Журнал нано- та електронної фізики
Metal-carbon nanocomposites
Nanoparticles NiCo
Magnetic properties of nanoparticles
IR-heatin
title The Influence of Synthesis Temperature on the Structure, Composition and Magnetic Properties of Nanocomposites NiCo/C
title_full The Influence of Synthesis Temperature on the Structure, Composition and Magnetic Properties of Nanocomposites NiCo/C
title_fullStr The Influence of Synthesis Temperature on the Structure, Composition and Magnetic Properties of Nanocomposites NiCo/C
title_full_unstemmed The Influence of Synthesis Temperature on the Structure, Composition and Magnetic Properties of Nanocomposites NiCo/C
title_short The Influence of Synthesis Temperature on the Structure, Composition and Magnetic Properties of Nanocomposites NiCo/C
title_sort influence of synthesis temperature on the structure composition and magnetic properties of nanocomposites nico c
topic Metal-carbon nanocomposites
Nanoparticles NiCo
Magnetic properties of nanoparticles
IR-heatin
url http://jnep.sumdu.edu.ua/download/numbers/2015/4/articles/jnep_2015_V7_04071.pdf
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