Elevated temperature performance: Arc-jet testing of carbon fiber reinforced ZrB2 bars up to 2200 °C for strength retention assessment

For the first time, ultra-high temperature ceramic matrix composite bars were tested inside an arc-jet facility to investigate the impact of oxidation damage on strength retention. The composite bars, which were based on a ZrB2/SiC matrix reinforced with 45 vol% carbon fibers, were produced by slurr...

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Bibliographic Details
Main Authors: D. Sciti, A. Vinci, L. Zoli, P. Galizia, M. Mor, W. Fahrenholtz, S. Mungiguerra, R. Savino, A. M. Caporale, A. Airoldi
Format: Article
Language:English
Published: Tsinghua University Press 2025-02-01
Series:Journal of Advanced Ceramics
Subjects:
Online Access:https://www.sciopen.com/article/10.26599/JAC.2024.9221022
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Summary:For the first time, ultra-high temperature ceramic matrix composite bars were tested inside an arc-jet facility to investigate the impact of oxidation damage on strength retention. The composite bars, which were based on a ZrB2/SiC matrix reinforced with 45 vol% carbon fibers, were produced by slurry impregnation and sintering. The first batch was tested under 3-point (pt) bending, and two additional batches were exposed to plasma of dissociated air up to a temperature of 2200 °C for 2 min or 2.2 min and then subjected to 3-pt bending. More than 75% of the initial strength was retained even after repeated testing, demonstrating the durability and reusability of the material. Volatility diagrams were calculated to explain the oxide layering observed, while a numerical model was developed to correlate the experimental mechanical data with the elastic properties. The decrease of strength was attributed to a reduction of the cross section due to oxidation.
ISSN:2226-4108
2227-8508