Thapsigargin triggers a non-apoptotic, caspase-independent programmed cell death in basophilic leukaemia cells

Abstract Thapsigargin (TG), a potent inhibitor of the sarco/endoplasmic reticulum Ca²⁺-ATPase (SERCA), is widely used to study intracellular Ca²⁺ homeostasis and has shown—along prodrug derivatives—promise as an anticancer agent. While TG is traditionally considered an inducer of apoptosis, the prec...

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Main Authors: Philip Steiner, Korollus Melek, Ancuela Andosch, Lena Wiesbauer, Anna Madlmayr, Michelle Duggan, Hubert H. Kerschbaum, Susanna Zierler
Format: Article
Language:English
Published: Nature Publishing Group 2025-07-01
Series:Cell Death Discovery
Online Access:https://doi.org/10.1038/s41420-025-02602-w
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author Philip Steiner
Korollus Melek
Ancuela Andosch
Lena Wiesbauer
Anna Madlmayr
Michelle Duggan
Hubert H. Kerschbaum
Susanna Zierler
author_facet Philip Steiner
Korollus Melek
Ancuela Andosch
Lena Wiesbauer
Anna Madlmayr
Michelle Duggan
Hubert H. Kerschbaum
Susanna Zierler
author_sort Philip Steiner
collection DOAJ
description Abstract Thapsigargin (TG), a potent inhibitor of the sarco/endoplasmic reticulum Ca²⁺-ATPase (SERCA), is widely used to study intracellular Ca²⁺ homeostasis and has shown—along prodrug derivatives—promise as an anticancer agent. While TG is traditionally considered an inducer of apoptosis, the precise mode of cell death it triggers remains incompletely defined. Here, we investigated the effects of TG on rat basophilic leukaemia (RBL-1) cells using advanced 2D and 3D transmission electron microscopy, confocal laser scanning microscopy, and functional cell death assays. TG treatment led to marked ultrastructural alterations, including pronounced ballooning of the perinuclear space, extensive vacuolization, mitochondrial enlargement and degradation, and structural anomalies of the endoplasmic reticulum. Notably, classical apoptotic features such as nuclear fragmentation, chromatin condensation and apoptotic body formation were absent. Functional assays revealed minimal caspase-3/7 activation and low Annexin V staining, indicating a caspase-independent, non-apoptotic form of programmed cell death (PCD). Morphological and quantitative analyses demonstrated that TG-induced cell death in RBL-1 cells closely resembles autosis, a non-apoptotic, autophagy-dependent PCD characterized by perinuclear space ballooning and increased autophagolysosome formation. These autosis-like features were also observed in TG-treated murine macrophages and human mast cells, suggesting a conserved mechanism across cell types. Digoxin, a Na⁺/K⁺-ATPase inhibitor, partially reversed TG-induced ultrastructural damage, supporting the involvement of Na⁺/K⁺-ATPase in this process. Ca²⁺ imaging confirmed that TG-induced cytosolic Ca²⁺ elevation is primarily driven by ER Ca²⁺ release, with extracellular Ca²⁺ amplifying the response. Our findings establish that TG induces a non-apoptotic, caspase-independent PCD matching autosis, challenging the prevailing view of TG as a classical apoptosis inducer. This insight has important implications for research on intracellular Ca2+ homeostasis as well as for the therapeutic exploitation of TG and its derivatives in targeting apoptosis-resistant cancer cells.
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spelling doaj-art-e04385669516498ba398cb0e272c4fc32025-08-20T03:45:45ZengNature Publishing GroupCell Death Discovery2058-77162025-07-0111111310.1038/s41420-025-02602-wThapsigargin triggers a non-apoptotic, caspase-independent programmed cell death in basophilic leukaemia cellsPhilip Steiner0Korollus Melek1Ancuela Andosch2Lena Wiesbauer3Anna Madlmayr4Michelle Duggan5Hubert H. Kerschbaum6Susanna Zierler7Institute of Pharmacology, Faculty of Medicine, Johannes Kepler University LinzInstitute of Biochemistry and Molecular Medicine, University of BernDepartment of Biosciences and Medical Biology, Paris Lodron University SalzburgInstitute of Pharmacology, Faculty of Medicine, Johannes Kepler University LinzInstitute of Pharmacology, Faculty of Medicine, Johannes Kepler University LinzInstitute of Pharmacology, Faculty of Medicine, Johannes Kepler University LinzDepartment of Biosciences and Medical Biology, Paris Lodron University SalzburgInstitute of Pharmacology, Faculty of Medicine, Johannes Kepler University LinzAbstract Thapsigargin (TG), a potent inhibitor of the sarco/endoplasmic reticulum Ca²⁺-ATPase (SERCA), is widely used to study intracellular Ca²⁺ homeostasis and has shown—along prodrug derivatives—promise as an anticancer agent. While TG is traditionally considered an inducer of apoptosis, the precise mode of cell death it triggers remains incompletely defined. Here, we investigated the effects of TG on rat basophilic leukaemia (RBL-1) cells using advanced 2D and 3D transmission electron microscopy, confocal laser scanning microscopy, and functional cell death assays. TG treatment led to marked ultrastructural alterations, including pronounced ballooning of the perinuclear space, extensive vacuolization, mitochondrial enlargement and degradation, and structural anomalies of the endoplasmic reticulum. Notably, classical apoptotic features such as nuclear fragmentation, chromatin condensation and apoptotic body formation were absent. Functional assays revealed minimal caspase-3/7 activation and low Annexin V staining, indicating a caspase-independent, non-apoptotic form of programmed cell death (PCD). Morphological and quantitative analyses demonstrated that TG-induced cell death in RBL-1 cells closely resembles autosis, a non-apoptotic, autophagy-dependent PCD characterized by perinuclear space ballooning and increased autophagolysosome formation. These autosis-like features were also observed in TG-treated murine macrophages and human mast cells, suggesting a conserved mechanism across cell types. Digoxin, a Na⁺/K⁺-ATPase inhibitor, partially reversed TG-induced ultrastructural damage, supporting the involvement of Na⁺/K⁺-ATPase in this process. Ca²⁺ imaging confirmed that TG-induced cytosolic Ca²⁺ elevation is primarily driven by ER Ca²⁺ release, with extracellular Ca²⁺ amplifying the response. Our findings establish that TG induces a non-apoptotic, caspase-independent PCD matching autosis, challenging the prevailing view of TG as a classical apoptosis inducer. This insight has important implications for research on intracellular Ca2+ homeostasis as well as for the therapeutic exploitation of TG and its derivatives in targeting apoptosis-resistant cancer cells.https://doi.org/10.1038/s41420-025-02602-w
spellingShingle Philip Steiner
Korollus Melek
Ancuela Andosch
Lena Wiesbauer
Anna Madlmayr
Michelle Duggan
Hubert H. Kerschbaum
Susanna Zierler
Thapsigargin triggers a non-apoptotic, caspase-independent programmed cell death in basophilic leukaemia cells
Cell Death Discovery
title Thapsigargin triggers a non-apoptotic, caspase-independent programmed cell death in basophilic leukaemia cells
title_full Thapsigargin triggers a non-apoptotic, caspase-independent programmed cell death in basophilic leukaemia cells
title_fullStr Thapsigargin triggers a non-apoptotic, caspase-independent programmed cell death in basophilic leukaemia cells
title_full_unstemmed Thapsigargin triggers a non-apoptotic, caspase-independent programmed cell death in basophilic leukaemia cells
title_short Thapsigargin triggers a non-apoptotic, caspase-independent programmed cell death in basophilic leukaemia cells
title_sort thapsigargin triggers a non apoptotic caspase independent programmed cell death in basophilic leukaemia cells
url https://doi.org/10.1038/s41420-025-02602-w
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