Dispersive Solid Phase Extraction for the Analysis of Veterinary Drugs Applied to Food Samples: A Review

To achieve analytical success, it is necessary to develop thorough clean-up procedures to extract analytes from the matrix. Dispersive solid phase extraction (DSPE) has been used as a pretreatment technique for the analysis of several compounds. This technique is based on the dispersion of a solid s...

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Main Authors: Gabriela Islas, Israel S. Ibarra, Prisciliano Hernandez, Jose M. Miranda, Alberto Cepeda
Format: Article
Language:English
Published: Wiley 2017-01-01
Series:International Journal of Analytical Chemistry
Online Access:http://dx.doi.org/10.1155/2017/8215271
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author Gabriela Islas
Israel S. Ibarra
Prisciliano Hernandez
Jose M. Miranda
Alberto Cepeda
author_facet Gabriela Islas
Israel S. Ibarra
Prisciliano Hernandez
Jose M. Miranda
Alberto Cepeda
author_sort Gabriela Islas
collection DOAJ
description To achieve analytical success, it is necessary to develop thorough clean-up procedures to extract analytes from the matrix. Dispersive solid phase extraction (DSPE) has been used as a pretreatment technique for the analysis of several compounds. This technique is based on the dispersion of a solid sorbent in liquid samples in the extraction isolation and clean-up of different analytes from complex matrices. DSPE has found a wide range of applications in several fields, and it is considered to be a selective, robust, and versatile technique. The applications of dispersive techniques in the analysis of veterinary drugs in different matrices involve magnetic sorbents, molecularly imprinted polymers, carbon-based nanomaterials, and the Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS) method. Techniques based on DSPE permit minimization of additional steps such as precipitation, centrifugation, and filtration, which decreases the manipulation of the sample. In this review, we describe the main procedures used for synthesis, characterization, and application of this pretreatment technique and how it has been applied to food analysis.
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spelling doaj-art-de124a3f477946718be0747ecb2ac8322025-08-20T02:21:20ZengWileyInternational Journal of Analytical Chemistry1687-87601687-87792017-01-01201710.1155/2017/82152718215271Dispersive Solid Phase Extraction for the Analysis of Veterinary Drugs Applied to Food Samples: A ReviewGabriela Islas0Israel S. Ibarra1Prisciliano Hernandez2Jose M. Miranda3Alberto Cepeda4Área Académica de Química, Universidad Autónoma del Estado de Hidalgo, Carretera Pachuca-Tulancingo Km 4.5, 42076 Pachuca, HGO, MexicoÁrea Académica de Química, Universidad Autónoma del Estado de Hidalgo, Carretera Pachuca-Tulancingo Km 4.5, 42076 Pachuca, HGO, MexicoÁrea de Energías, Universidad Politécnica de Francisco I. Madero, Domicilio Conocido, 42640 Tepatepec, HGO, MexicoDepartamento de Química Analítica, Nutrición y Bromatología, Facultad de Veterinaria, Universidade de Santiago de Compostela, Pabellón 4 Planta Baja, Campus Universitario, s/n, 27002 Lugo, SpainDepartamento de Química Analítica, Nutrición y Bromatología, Facultad de Veterinaria, Universidade de Santiago de Compostela, Pabellón 4 Planta Baja, Campus Universitario, s/n, 27002 Lugo, SpainTo achieve analytical success, it is necessary to develop thorough clean-up procedures to extract analytes from the matrix. Dispersive solid phase extraction (DSPE) has been used as a pretreatment technique for the analysis of several compounds. This technique is based on the dispersion of a solid sorbent in liquid samples in the extraction isolation and clean-up of different analytes from complex matrices. DSPE has found a wide range of applications in several fields, and it is considered to be a selective, robust, and versatile technique. The applications of dispersive techniques in the analysis of veterinary drugs in different matrices involve magnetic sorbents, molecularly imprinted polymers, carbon-based nanomaterials, and the Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS) method. Techniques based on DSPE permit minimization of additional steps such as precipitation, centrifugation, and filtration, which decreases the manipulation of the sample. In this review, we describe the main procedures used for synthesis, characterization, and application of this pretreatment technique and how it has been applied to food analysis.http://dx.doi.org/10.1155/2017/8215271
spellingShingle Gabriela Islas
Israel S. Ibarra
Prisciliano Hernandez
Jose M. Miranda
Alberto Cepeda
Dispersive Solid Phase Extraction for the Analysis of Veterinary Drugs Applied to Food Samples: A Review
International Journal of Analytical Chemistry
title Dispersive Solid Phase Extraction for the Analysis of Veterinary Drugs Applied to Food Samples: A Review
title_full Dispersive Solid Phase Extraction for the Analysis of Veterinary Drugs Applied to Food Samples: A Review
title_fullStr Dispersive Solid Phase Extraction for the Analysis of Veterinary Drugs Applied to Food Samples: A Review
title_full_unstemmed Dispersive Solid Phase Extraction for the Analysis of Veterinary Drugs Applied to Food Samples: A Review
title_short Dispersive Solid Phase Extraction for the Analysis of Veterinary Drugs Applied to Food Samples: A Review
title_sort dispersive solid phase extraction for the analysis of veterinary drugs applied to food samples a review
url http://dx.doi.org/10.1155/2017/8215271
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