Unexpected texture transition induced by grain growth during static annealing of a dilute Mg-1Al alloy

Conventional rolled Mg-Al alloy sheets typically exhibit strong basal textures that remain and may even strengthen after recrystallization annealing due to the preferential growth of basal-oriented grains, resulting in poor formability at room temperature. Therefore, the knowledge of recrystallizati...

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Main Authors: Meng-Na Zhang, Hai-Long Jia, Xiao Ma, Lei Zhao, Zhi-Gang Li, Min Zha
Format: Article
Language:English
Published: KeAi Communications Co., Ltd. 2025-03-01
Series:Journal of Magnesium and Alloys
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Online Access:http://www.sciencedirect.com/science/article/pii/S221395672400135X
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Summary:Conventional rolled Mg-Al alloy sheets typically exhibit strong basal textures that remain and may even strengthen after recrystallization annealing due to the preferential growth of basal-oriented grains, resulting in poor formability at room temperature. Therefore, the knowledge of recrystallization and grain growth is critical for modifying textures of Mg-Al alloy sheets. The static recrystallization and texture evolution in a cold-rolled dilute Mg-1Al (wt.%) alloy during various annealed temperatures ranging from 300 °C to 450 °C, have been investigated using the quasi in-situ electron backscatter diffraction (EBSD) method. The as-rolled Mg-1Al alloy shows a dominant basal texture, which weakens and broadens in the rolling direction (RD) during the subsequent annealing, accompanied by the formation of 〈101¯0〉 texture component. Particularly, the 〈101¯0〉 texture component is more pronounced after annealing at high temperatures. The quasi in-situ EBSD results show that recrystallized grains are mainly induced by shear bands, which exhibit a wide spectrum of orientations with c-axis tilt angles ranging 20°-45° from the normal direction (ND). Orientations of shear band-induced recrystallized grains are retained during the entire recrystallization process, resulting in a reduction in the texture intensity. Moreover, recrystallized grains belonging to the 〈101¯0〉 texture component grow preferentially compared to those with other orientations, which is attributed to low energy grain boundaries, especially grain boundaries with ∼30° misorientation angles. Furthermore, the high temperature annealing facilitates the rapid growth of grain boundaries having a 30° misorientation angle, leading to the occurrence of distinct 〈101¯0〉 texture after annealing at 450 °C for 1 h. The results provide insights for texture modification of rare earth-free low-alloyed Mg alloys by controlling annealing parameters.
ISSN:2213-9567