Optimized Breakdown Strength and Crystal Structure for Boosting the Energy Storage Performance of Niobate-Based Glass Ceramics via a B-Site Substitution Strategy

Based on the B-site modification strategy, excellent energy storage properties were achieved in this work by substituting Nb with Ta of the same valence in niobate-based glass ceramics. Ta substitution was found to lead to the transformation of crystal structures, and the space point group evolved f...

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Main Authors: Kexin Gao, Fei Shang, Yaoyi Qin, Guohua Chen
Format: Article
Language:English
Published: MDPI AG 2025-05-01
Series:Crystals
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Online Access:https://www.mdpi.com/2073-4352/15/5/444
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author Kexin Gao
Fei Shang
Yaoyi Qin
Guohua Chen
author_facet Kexin Gao
Fei Shang
Yaoyi Qin
Guohua Chen
author_sort Kexin Gao
collection DOAJ
description Based on the B-site modification strategy, excellent energy storage properties were achieved in this work by substituting Nb with Ta of the same valence in niobate-based glass ceramics. Ta substitution was found to lead to the transformation of crystal structures, and the space point group evolved from the non-centrosymmetric P4bm to the centrosymmetric P4/mbm, resulting in a transition from relaxor ferroelectric to paraelectric glass ceramics. Furthermore, the addition of Ta led to a significant decrease in grain size and interfacial activation energy, as well as an increase in the optical band gap, resulting in a dramatic increase in BDS from 800 kV/cm to 1300 kV/cm. The KBSN-4.0mol%Ta<sub>2</sub>O<sub>5</sub> glass ceramic exhibited optimal energy storage properties, including a discharge energy density of ~5.62 J/cm<sup>3</sup> and a superfast discharge rate of ~9.7 ns, resulting in an ultrahigh discharge power density of about ~1296.9 MW/cm<sup>3</sup> at 1300 kV/cm. Furthermore, this KBSN-Ta glass ceramic also displayed good thermal stability over a temperature range of 20–120 °C, with the <i>W<sub>d</sub></i> decreasing by 9.0% at 600 kV/cm. B-site modification engineering in glass ceramics has proved to be an important way to effectively optimize energy storage performance.
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spelling doaj-art-dd02c6effb1d45e8a245a3382fd95e4e2025-08-20T01:56:31ZengMDPI AGCrystals2073-43522025-05-0115544410.3390/cryst15050444Optimized Breakdown Strength and Crystal Structure for Boosting the Energy Storage Performance of Niobate-Based Glass Ceramics via a B-Site Substitution StrategyKexin Gao0Fei Shang1Yaoyi Qin2Guohua Chen3Electronical Information Materials and Devices Engineering Research Center of Ministry of Education, Guangxi Key Laboratory of Information Materials, School of Material Science and Engineering, Guilin University of Electronic Technology, Guilin 541004, ChinaElectronical Information Materials and Devices Engineering Research Center of Ministry of Education, Guangxi Key Laboratory of Information Materials, School of Material Science and Engineering, Guilin University of Electronic Technology, Guilin 541004, ChinaElectronical Information Materials and Devices Engineering Research Center of Ministry of Education, Guangxi Key Laboratory of Information Materials, School of Material Science and Engineering, Guilin University of Electronic Technology, Guilin 541004, ChinaElectronical Information Materials and Devices Engineering Research Center of Ministry of Education, Guangxi Key Laboratory of Information Materials, School of Material Science and Engineering, Guilin University of Electronic Technology, Guilin 541004, ChinaBased on the B-site modification strategy, excellent energy storage properties were achieved in this work by substituting Nb with Ta of the same valence in niobate-based glass ceramics. Ta substitution was found to lead to the transformation of crystal structures, and the space point group evolved from the non-centrosymmetric P4bm to the centrosymmetric P4/mbm, resulting in a transition from relaxor ferroelectric to paraelectric glass ceramics. Furthermore, the addition of Ta led to a significant decrease in grain size and interfacial activation energy, as well as an increase in the optical band gap, resulting in a dramatic increase in BDS from 800 kV/cm to 1300 kV/cm. The KBSN-4.0mol%Ta<sub>2</sub>O<sub>5</sub> glass ceramic exhibited optimal energy storage properties, including a discharge energy density of ~5.62 J/cm<sup>3</sup> and a superfast discharge rate of ~9.7 ns, resulting in an ultrahigh discharge power density of about ~1296.9 MW/cm<sup>3</sup> at 1300 kV/cm. Furthermore, this KBSN-Ta glass ceramic also displayed good thermal stability over a temperature range of 20–120 °C, with the <i>W<sub>d</sub></i> decreasing by 9.0% at 600 kV/cm. B-site modification engineering in glass ceramics has proved to be an important way to effectively optimize energy storage performance.https://www.mdpi.com/2073-4352/15/5/444glass ceramicdielectric energy storageenergy densitypower densityB-site modification
spellingShingle Kexin Gao
Fei Shang
Yaoyi Qin
Guohua Chen
Optimized Breakdown Strength and Crystal Structure for Boosting the Energy Storage Performance of Niobate-Based Glass Ceramics via a B-Site Substitution Strategy
Crystals
glass ceramic
dielectric energy storage
energy density
power density
B-site modification
title Optimized Breakdown Strength and Crystal Structure for Boosting the Energy Storage Performance of Niobate-Based Glass Ceramics via a B-Site Substitution Strategy
title_full Optimized Breakdown Strength and Crystal Structure for Boosting the Energy Storage Performance of Niobate-Based Glass Ceramics via a B-Site Substitution Strategy
title_fullStr Optimized Breakdown Strength and Crystal Structure for Boosting the Energy Storage Performance of Niobate-Based Glass Ceramics via a B-Site Substitution Strategy
title_full_unstemmed Optimized Breakdown Strength and Crystal Structure for Boosting the Energy Storage Performance of Niobate-Based Glass Ceramics via a B-Site Substitution Strategy
title_short Optimized Breakdown Strength and Crystal Structure for Boosting the Energy Storage Performance of Niobate-Based Glass Ceramics via a B-Site Substitution Strategy
title_sort optimized breakdown strength and crystal structure for boosting the energy storage performance of niobate based glass ceramics via a b site substitution strategy
topic glass ceramic
dielectric energy storage
energy density
power density
B-site modification
url https://www.mdpi.com/2073-4352/15/5/444
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AT yaoyiqin optimizedbreakdownstrengthandcrystalstructureforboostingtheenergystorageperformanceofniobatebasedglassceramicsviaabsitesubstitutionstrategy
AT guohuachen optimizedbreakdownstrengthandcrystalstructureforboostingtheenergystorageperformanceofniobatebasedglassceramicsviaabsitesubstitutionstrategy