Determination of tetraniliprole residues in animal derived foods by multi-plug filtration cleanup combined with HPLC-MS/MS
ObjectiveThis study aimed to develop a rapid and efficient method for quantifying tetraniliprole residues in animal-derived foods by combining multi-plug filtration cleanup (m-PFC) with high-performance liquid chromatography-mass spectrometry (HPLC-MS).MethodsSamples were extracted with acetonitrile...
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| Format: | Article |
| Language: | English |
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The Editorial Office of Food and Machinery
2024-10-01
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| Series: | Shipin yu jixie |
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| Online Access: | http://www.ifoodmm.com/spyjx/article/abstract/20241007?st=article_issue |
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| author | YUAN Liejiang WANG Xiu LI Zheng ZHU Li DENG Hang |
| author_facet | YUAN Liejiang WANG Xiu LI Zheng ZHU Li DENG Hang |
| author_sort | YUAN Liejiang |
| collection | DOAJ |
| description | ObjectiveThis study aimed to develop a rapid and efficient method for quantifying tetraniliprole residues in animal-derived foods by combining multi-plug filtration cleanup (m-PFC) with high-performance liquid chromatography-mass spectrometry (HPLC-MS).MethodsSamples were extracted with acetonitrile, followed by salting out using sodium chloride and anhydrous magnesium sulfate. The extracts were purified via m-PFC and analyzed using HPLC-MS with external standard calibration.ResultsThe method demonstrated a strong linear correlation between tetraniliprole concentration and response values over a range of 0.001 to 0.150 mg/L, with a coefficient of determination (R2) exceeding 0.999. The limit of quantification (LOQ) was 0.002 mg/kg. Average recovery rates ranged from 90.0% to 108.0%, with relative standard deviations between 1.10% and 4.89%, validated across a variety of matrices, including pork, beef, mutton, chicken, pork liver, beef liver, mutton liver, chicken liver, eggs and milk.ConclusionThe proposed method is rapid, straightforward, high sensitivity, and suitable for quantitative determination of tetraniliprole residues in animal-derived food. |
| format | Article |
| id | doaj-art-dae3fd3395d84f48a8fb39458e9347a9 |
| institution | DOAJ |
| issn | 1003-5788 |
| language | English |
| publishDate | 2024-10-01 |
| publisher | The Editorial Office of Food and Machinery |
| record_format | Article |
| series | Shipin yu jixie |
| spelling | doaj-art-dae3fd3395d84f48a8fb39458e9347a92025-08-20T02:59:19ZengThe Editorial Office of Food and MachineryShipin yu jixie1003-57882024-10-014010465210.13652/j.spjx.1003.5788.2024.808001003-5788（2024）10-0046-07Determination of tetraniliprole residues in animal derived foods by multi-plug filtration cleanup combined with HPLC-MS/MSYUAN Liejiang0WANG Xiu1LI Zheng2ZHU Li3DENG Hang4Hunan Provincial Institute of Product and Goods Quality Inspection, Changsha, Hunan410007, ChinaHunan Provincial Institute of Product and Goods Quality Inspection, Changsha, Hunan410007, ChinaHunan Provincial Institute of Product and Goods Quality Inspection, Changsha, Hunan410007, ChinaHunan Provincial Institute of Product and Goods Quality Inspection, Changsha, Hunan410007, ChinaHunan Provincial Institute of Product and Goods Quality Inspection, Changsha, Hunan410007, ChinaObjectiveThis study aimed to develop a rapid and efficient method for quantifying tetraniliprole residues in animal-derived foods by combining multi-plug filtration cleanup (m-PFC) with high-performance liquid chromatography-mass spectrometry (HPLC-MS).MethodsSamples were extracted with acetonitrile, followed by salting out using sodium chloride and anhydrous magnesium sulfate. The extracts were purified via m-PFC and analyzed using HPLC-MS with external standard calibration.ResultsThe method demonstrated a strong linear correlation between tetraniliprole concentration and response values over a range of 0.001 to 0.150 mg/L, with a coefficient of determination (R2) exceeding 0.999. The limit of quantification (LOQ) was 0.002 mg/kg. Average recovery rates ranged from 90.0% to 108.0%, with relative standard deviations between 1.10% and 4.89%, validated across a variety of matrices, including pork, beef, mutton, chicken, pork liver, beef liver, mutton liver, chicken liver, eggs and milk.ConclusionThe proposed method is rapid, straightforward, high sensitivity, and suitable for quantitative determination of tetraniliprole residues in animal-derived food.http://www.ifoodmm.com/spyjx/article/abstract/20241007?st=article_issuetetraniliprolemulti-plug filtration cleanup (m-pfc)hplc-ms/msanimal derived foods |
| spellingShingle | YUAN Liejiang WANG Xiu LI Zheng ZHU Li DENG Hang Determination of tetraniliprole residues in animal derived foods by multi-plug filtration cleanup combined with HPLC-MS/MS Shipin yu jixie tetraniliprole multi-plug filtration cleanup (m-pfc) hplc-ms/ms animal derived foods |
| title | Determination of tetraniliprole residues in animal derived foods by multi-plug filtration cleanup combined with HPLC-MS/MS |
| title_full | Determination of tetraniliprole residues in animal derived foods by multi-plug filtration cleanup combined with HPLC-MS/MS |
| title_fullStr | Determination of tetraniliprole residues in animal derived foods by multi-plug filtration cleanup combined with HPLC-MS/MS |
| title_full_unstemmed | Determination of tetraniliprole residues in animal derived foods by multi-plug filtration cleanup combined with HPLC-MS/MS |
| title_short | Determination of tetraniliprole residues in animal derived foods by multi-plug filtration cleanup combined with HPLC-MS/MS |
| title_sort | determination of tetraniliprole residues in animal derived foods by multi plug filtration cleanup combined with hplc ms ms |
| topic | tetraniliprole multi-plug filtration cleanup (m-pfc) hplc-ms/ms animal derived foods |
| url | http://www.ifoodmm.com/spyjx/article/abstract/20241007?st=article_issue |
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