Improvement of Electrochromic Stability of Viologen‐Based Ionic Gel by Layered Metal–Organic Frameworks

Abstract Metal–organic frameworks (MOFs) fulfill the requirements of electrochromic (EC) materials due to their unique 3D pore structure, excellent thermal stability, and outstanding processing and electrochemical properties. Viologens, a class of cationic organic molecules with remarkable redox pro...

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Main Authors: Huan Jiang, Yujiao Li, Fangfang Liu, Chenhao Wang, Liping Sheng, Jianfang Wang, Cheng‐an Tao
Format: Article
Language:English
Published: Wiley-VCH 2025-06-01
Series:Advanced Materials Interfaces
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Online Access:https://doi.org/10.1002/admi.202500078
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author Huan Jiang
Yujiao Li
Fangfang Liu
Chenhao Wang
Liping Sheng
Jianfang Wang
Cheng‐an Tao
author_facet Huan Jiang
Yujiao Li
Fangfang Liu
Chenhao Wang
Liping Sheng
Jianfang Wang
Cheng‐an Tao
author_sort Huan Jiang
collection DOAJ
description Abstract Metal–organic frameworks (MOFs) fulfill the requirements of electrochromic (EC) materials due to their unique 3D pore structure, excellent thermal stability, and outstanding processing and electrochemical properties. Viologens, a class of cationic organic molecules with remarkable redox properties, are a type of EC material with exceptional characteristics. In this study, ionic gel electrochromic materials are prepared by hybridizing zirconyl imine (ZrTCA) MOFs with ethyl viologen bis (trifluoromethane sulfonyl) imide (EV[TFSI]2) in varying proportions, and ionic gel electrochromic devices (ECDs) are constructed. The results indicate that the incorporation of layered zirconium‐based MOFs not only enriches the color states of the ionic gel ECDs but also transforms them from transparent to reflective displays. Compared to pure EV[TFSI]2 ECDs, those doped with zirconium MOFs exhibit a more uniform coloring state, shorter coloring time, higher coloration efficiency, and better cycle stability. This is attributed to the good chemical stability and efficient ion migration channels provided by the porous framework structure of zirconium‐based MOFs. Notably, the MOFs:EV[TFSI]2 (0.5:1) ECDs display a synergistic effect, with the redox cycle stabilizing for ≈1100 cycles and color bleaching kinetic stability tested up to 1600 switches, experiencing only a 9% reduction in ΔT, demonstrating significantly enhanced durability and stability compared to pure EV[TFSI]2 ECDs.
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spelling doaj-art-da03888c72d344a28fe6dabaab54115b2025-08-20T03:27:51ZengWiley-VCHAdvanced Materials Interfaces2196-73502025-06-011212n/an/a10.1002/admi.202500078Improvement of Electrochromic Stability of Viologen‐Based Ionic Gel by Layered Metal–Organic FrameworksHuan Jiang0Yujiao Li1Fangfang Liu2Chenhao Wang3Liping Sheng4Jianfang Wang5Cheng‐an Tao6College of Science National University of Defense Technology Changsha 410073 P. R. ChinaCollege of Science National University of Defense Technology Changsha 410073 P. R. ChinaCollege of Science National University of Defense Technology Changsha 410073 P. R. ChinaCollege of Science National University of Defense Technology Changsha 410073 P. R. ChinaCollege of Chemistry and Chemical Engineering Hunan Normal University Changsha 410081 P. R. ChinaCollege of Science National University of Defense Technology Changsha 410073 P. R. ChinaCollege of Science National University of Defense Technology Changsha 410073 P. R. ChinaAbstract Metal–organic frameworks (MOFs) fulfill the requirements of electrochromic (EC) materials due to their unique 3D pore structure, excellent thermal stability, and outstanding processing and electrochemical properties. Viologens, a class of cationic organic molecules with remarkable redox properties, are a type of EC material with exceptional characteristics. In this study, ionic gel electrochromic materials are prepared by hybridizing zirconyl imine (ZrTCA) MOFs with ethyl viologen bis (trifluoromethane sulfonyl) imide (EV[TFSI]2) in varying proportions, and ionic gel electrochromic devices (ECDs) are constructed. The results indicate that the incorporation of layered zirconium‐based MOFs not only enriches the color states of the ionic gel ECDs but also transforms them from transparent to reflective displays. Compared to pure EV[TFSI]2 ECDs, those doped with zirconium MOFs exhibit a more uniform coloring state, shorter coloring time, higher coloration efficiency, and better cycle stability. This is attributed to the good chemical stability and efficient ion migration channels provided by the porous framework structure of zirconium‐based MOFs. Notably, the MOFs:EV[TFSI]2 (0.5:1) ECDs display a synergistic effect, with the redox cycle stabilizing for ≈1100 cycles and color bleaching kinetic stability tested up to 1600 switches, experiencing only a 9% reduction in ΔT, demonstrating significantly enhanced durability and stability compared to pure EV[TFSI]2 ECDs.https://doi.org/10.1002/admi.202500078electrochromismethyl viologenionogelmetal–organic frameworks
spellingShingle Huan Jiang
Yujiao Li
Fangfang Liu
Chenhao Wang
Liping Sheng
Jianfang Wang
Cheng‐an Tao
Improvement of Electrochromic Stability of Viologen‐Based Ionic Gel by Layered Metal–Organic Frameworks
Advanced Materials Interfaces
electrochromism
ethyl viologen
ionogel
metal–organic frameworks
title Improvement of Electrochromic Stability of Viologen‐Based Ionic Gel by Layered Metal–Organic Frameworks
title_full Improvement of Electrochromic Stability of Viologen‐Based Ionic Gel by Layered Metal–Organic Frameworks
title_fullStr Improvement of Electrochromic Stability of Viologen‐Based Ionic Gel by Layered Metal–Organic Frameworks
title_full_unstemmed Improvement of Electrochromic Stability of Viologen‐Based Ionic Gel by Layered Metal–Organic Frameworks
title_short Improvement of Electrochromic Stability of Viologen‐Based Ionic Gel by Layered Metal–Organic Frameworks
title_sort improvement of electrochromic stability of viologen based ionic gel by layered metal organic frameworks
topic electrochromism
ethyl viologen
ionogel
metal–organic frameworks
url https://doi.org/10.1002/admi.202500078
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AT chenhaowang improvementofelectrochromicstabilityofviologenbasedionicgelbylayeredmetalorganicframeworks
AT lipingsheng improvementofelectrochromicstabilityofviologenbasedionicgelbylayeredmetalorganicframeworks
AT jianfangwang improvementofelectrochromicstabilityofviologenbasedionicgelbylayeredmetalorganicframeworks
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