Study of the environmental pollutants of petroleum nature from spent refining water in Beiji refinery

In this research work, separation and identification of some petroleum components in wastewater in Beiji. The petroleum components and hydrocarbons were extracted from the wastewater by CCl4. The extract after evaporation of the solvent was fractionated using liquid-liquid extraction employing ethy...

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Main Author: Abid A. Erdini
Format: Article
Language:English
Published: Tikrit University 2023-02-01
Series:Tikrit Journal of Pure Science
Subjects:
Online Access:https://tjpsj.org/index.php/tjps/article/view/847
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author Abid A. Erdini
author_facet Abid A. Erdini
author_sort Abid A. Erdini
collection DOAJ
description In this research work, separation and identification of some petroleum components in wastewater in Beiji. The petroleum components and hydrocarbons were extracted from the wastewater by CCl4. The extract after evaporation of the solvent was fractionated using liquid-liquid extraction employing ethyl methyl ketone to remove paraffinic waxes-residual materials were redissolved in CCl4 to remove any contamination. The residue remained after the removal of the solvent was transferred quantitatively to prepacked silica gel column (100-120) mesh which was activated at 300 °C. Silica gel column was washed by using the following solvent: hexan, toluene, chloroform and ethanol. It was found apparent that the separated component were of paraffinic, aromatic and heterogenous, nature for the solvent mentioned above, respectively. The confirmation of such nature was performed by using infrared spectrophotometer technique
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spelling doaj-art-d9b0a664f1fd4c0a8a11a33329e1cc5f2025-08-20T02:36:23ZengTikrit UniversityTikrit Journal of Pure Science1813-16622415-17262023-02-0122810.25130/tjps.v22i8.847Study of the environmental pollutants of petroleum nature from spent refining water in Beiji refineryAbid A. Erdini In this research work, separation and identification of some petroleum components in wastewater in Beiji. The petroleum components and hydrocarbons were extracted from the wastewater by CCl4. The extract after evaporation of the solvent was fractionated using liquid-liquid extraction employing ethyl methyl ketone to remove paraffinic waxes-residual materials were redissolved in CCl4 to remove any contamination. The residue remained after the removal of the solvent was transferred quantitatively to prepacked silica gel column (100-120) mesh which was activated at 300 °C. Silica gel column was washed by using the following solvent: hexan, toluene, chloroform and ethanol. It was found apparent that the separated component were of paraffinic, aromatic and heterogenous, nature for the solvent mentioned above, respectively. The confirmation of such nature was performed by using infrared spectrophotometer technique https://tjpsj.org/index.php/tjps/article/view/847environmental pollutantspetroleum naturewaterBeiji refinery
spellingShingle Abid A. Erdini
Study of the environmental pollutants of petroleum nature from spent refining water in Beiji refinery
Tikrit Journal of Pure Science
environmental pollutants
petroleum nature
water
Beiji refinery
title Study of the environmental pollutants of petroleum nature from spent refining water in Beiji refinery
title_full Study of the environmental pollutants of petroleum nature from spent refining water in Beiji refinery
title_fullStr Study of the environmental pollutants of petroleum nature from spent refining water in Beiji refinery
title_full_unstemmed Study of the environmental pollutants of petroleum nature from spent refining water in Beiji refinery
title_short Study of the environmental pollutants of petroleum nature from spent refining water in Beiji refinery
title_sort study of the environmental pollutants of petroleum nature from spent refining water in beiji refinery
topic environmental pollutants
petroleum nature
water
Beiji refinery
url https://tjpsj.org/index.php/tjps/article/view/847
work_keys_str_mv AT abidaerdini studyoftheenvironmentalpollutantsofpetroleumnaturefromspentrefiningwaterinbeijirefinery