Design, Synthesis and Structural Study of a <i>Bis</i>thiosemicarbazone Ligand Precursor of Metallosupramolecular Architectures

The increase in the investigation of different self-assembled architectures derived from thiosemicarbazone ligands can be attributed to the numerous functional metallosupramolecular architectures with practical applications that can be obtained. The potentially tetradentate organic <i>bis</...

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Bibliographic Details
Main Authors: Uxía Barreiro-Sisto, Isabel Velo-Heleno, Miguel Martínez-Calvo, Marcelino Maneiro, Sandra Fernández-Fariña
Format: Article
Language:English
Published: MDPI AG 2023-11-01
Series:Chemistry Proceedings
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Online Access:https://www.mdpi.com/2673-4583/14/1/3
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Summary:The increase in the investigation of different self-assembled architectures derived from thiosemicarbazone ligands can be attributed to the numerous functional metallosupramolecular architectures with practical applications that can be obtained. The potentially tetradentate organic <i>bis</i>thiosemicarbazone ligand H<sub>2</sub>L possesses two flexible bidentate [NS] domains separated by a short and rigid spacer, which could stabilize several metal ions and thus different metallosupramolecular architectures. H<sub>2</sub>L was prepared by the reaction between two equivalents of N-ethylhydrazinecarbothioamide and one equivalent of 1,1′,1″-(benzene-1,3,5-triyl)tris(ethan-1-one) and was fully studied using several techniques, including X-ray diffraction.
ISSN:2673-4583