Size Dependent Compressive Strength of FIB Machined Single Crystal Manganese Pillars

The deformation behavior of single crystals of manganese pillars generated by focused ion beam (FIB), with diameters ranging from ~1 m to ~4.5 m, has been studied as a function of specimen size using micropillar compression at ambient temperature. The manganese pillars were...

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Main Authors: Halil Yılmaz, Bülent Alkan, Hasan Feyzi Budak
Format: Article
Language:English
Published: Hitit University 2024-03-01
Series:Hittite Journal of Science and Engineering
Online Access:https://dergipark.org.tr/en/doi/10.17350/HJSE19030000330
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author Halil Yılmaz
Bülent Alkan
Hasan Feyzi Budak
author_facet Halil Yılmaz
Bülent Alkan
Hasan Feyzi Budak
author_sort Halil Yılmaz
collection DOAJ
description The deformation behavior of single crystals of manganese pillars generated by focused ion beam (FIB), with diameters ranging from ~1 m to ~4.5 m, has been studied as a function of specimen size using micropillar compression at ambient temperature. The manganese pillars were machined from randomly chosen larger grains of polycrystalline metal. At ambient temperature, single crystals of manganese display chaotic slip planes emerging on the sample surface and brittle plastic deformation when the sample size is decreased to the micrometer scale. The manganese pillars reached very high flow stresses in the range of 4-5.6 GPa. The stress-strain curves of all tested manganese pillars demonstrated significant work hardening and smooth flow behavior, with strains up to 8-10%. After 10% strain, however, the flow stresses remained constant with no work hardening. As previously reported, the manganese pillars with undetermined orientation demonstrated a less pronounced size effect (-0.14) by the size effect exponent of BCC pillars.
format Article
id doaj-art-d736eee1b3f547ef943f9b6e3db573a5
institution Kabale University
issn 2148-4171
language English
publishDate 2024-03-01
publisher Hitit University
record_format Article
series Hittite Journal of Science and Engineering
spelling doaj-art-d736eee1b3f547ef943f9b6e3db573a52025-01-12T07:13:56ZengHitit UniversityHittite Journal of Science and Engineering2148-41712024-03-01111414710.17350/HJSE19030000330150 Size Dependent Compressive Strength of FIB Machined Single Crystal Manganese Pillars Halil Yılmaz0https://orcid.org/0000-0003-3585-0665Bülent Alkan1https://orcid.org/0000-0003-1048-7986Hasan Feyzi Budak2https://orcid.org/0000-0002-7993-2059MUŞ ALPARSLAN ÜNİVERSİTESİ, TEKNİK BİLİMLER MESLEK YÜKSEKOKULU, MAKİNE VE METAL TEKNOLOJİLERİ BÖLÜMÜHITIT UNIVERSITY, FACULTY OF ENGINEERING, DEPARTMENT OF METALLURGICAL AND MATERIALS ENGINEERINGATATURK UNIVERSITY, EAST ANATOLIA HIGH TECHNOLOGY APPLICATION AND RESEARCH CENTER The deformation behavior of single crystals of manganese pillars generated by focused ion beam (FIB), with diameters ranging from ~1 m to ~4.5 m, has been studied as a function of specimen size using micropillar compression at ambient temperature. The manganese pillars were machined from randomly chosen larger grains of polycrystalline metal. At ambient temperature, single crystals of manganese display chaotic slip planes emerging on the sample surface and brittle plastic deformation when the sample size is decreased to the micrometer scale. The manganese pillars reached very high flow stresses in the range of 4-5.6 GPa. The stress-strain curves of all tested manganese pillars demonstrated significant work hardening and smooth flow behavior, with strains up to 8-10%. After 10% strain, however, the flow stresses remained constant with no work hardening. As previously reported, the manganese pillars with undetermined orientation demonstrated a less pronounced size effect (-0.14) by the size effect exponent of BCC pillars.https://dergipark.org.tr/en/doi/10.17350/HJSE19030000330
spellingShingle Halil Yılmaz
Bülent Alkan
Hasan Feyzi Budak
Size Dependent Compressive Strength of FIB Machined Single Crystal Manganese Pillars
Hittite Journal of Science and Engineering
title Size Dependent Compressive Strength of FIB Machined Single Crystal Manganese Pillars
title_full Size Dependent Compressive Strength of FIB Machined Single Crystal Manganese Pillars
title_fullStr Size Dependent Compressive Strength of FIB Machined Single Crystal Manganese Pillars
title_full_unstemmed Size Dependent Compressive Strength of FIB Machined Single Crystal Manganese Pillars
title_short Size Dependent Compressive Strength of FIB Machined Single Crystal Manganese Pillars
title_sort size dependent compressive strength of fib machined single crystal manganese pillars
url https://dergipark.org.tr/en/doi/10.17350/HJSE19030000330
work_keys_str_mv AT halilyılmaz sizedependentcompressivestrengthoffibmachinedsinglecrystalmanganesepillars
AT bulentalkan sizedependentcompressivestrengthoffibmachinedsinglecrystalmanganesepillars
AT hasanfeyzibudak sizedependentcompressivestrengthoffibmachinedsinglecrystalmanganesepillars