Oxide tribolayer effects on fretting wear of steel under variable displacement amplitude

Most of the studies in the literature dealing with fretting have focused on wear mechanisms without considering the formation of oxide layers, whose nature can vary depending on the displacement amplitude and the material pairing. This omission limits the understanding of how different fretting cond...

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Main Authors: Roderick Jacques, Abdeljalil Jourani, Salima Bouvier, Yan-Ming Chen
Format: Article
Language:English
Published: Elsevier 2025-09-01
Series:Results in Engineering
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Online Access:http://www.sciencedirect.com/science/article/pii/S2590123025027124
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author Roderick Jacques
Abdeljalil Jourani
Salima Bouvier
Yan-Ming Chen
author_facet Roderick Jacques
Abdeljalil Jourani
Salima Bouvier
Yan-Ming Chen
author_sort Roderick Jacques
collection DOAJ
description Most of the studies in the literature dealing with fretting have focused on wear mechanisms without considering the formation of oxide layers, whose nature can vary depending on the displacement amplitude and the material pairing. This omission limits the understanding of how different fretting conditions influence surface transformations and ultimately affect wear behavior. This study investigates the wear mechanisms and oxide layer formation in two steel-steel tribosystems, 100Cr6/100Cr6 and 20MnCr5/100Cr6. A parametric approach was adopted, varying displacement amplitudes from 20 to 200 µm under a constant normal load of 10 N, to elucidate the roles of the third body, oxidation, and debris ejection on fretting wear. Friction behavior and electrical contact resistance were monitored in real-time to assess the evolution of contact conditions. Surface characterization was conducted using SEM, Energy dispersive X-ray (EDX), FIB-TEM, and Transmission Kikuchi diffraction (TKD) to analyze wear morphologies and oxide layer composition. The results reveal that although both material pairs developed oxide-based tribolayers at increased amplitudes, only the 20MnCr5/100Cr6 pair exhibited a notable reduction in wear volume between amplitudes of 50 µm and 100 µm. This reduction was attributed to the formation of a more effective third-body layer. Furthermore, TKD analysis demonstrated that magnetite-rich oxide layers formed at 50 µm displacement amplitude in the 100Cr6/100Cr6 pair were more compact and protective compared to the hematite-dominated layers observed at higher amplitudes. These findings underscore the critical influence of material pairing and displacement amplitude on the stability and protective effectiveness of oxide layers in fretting conditions.
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spelling doaj-art-d3fdd123c3be4a3f960e4251b1cf7ace2025-08-22T04:57:22ZengElsevierResults in Engineering2590-12302025-09-012710664510.1016/j.rineng.2025.106645Oxide tribolayer effects on fretting wear of steel under variable displacement amplitudeRoderick Jacques0Abdeljalil Jourani1Salima Bouvier2Yan-Ming Chen3Technical Center of Mechanical Industries (Cetim), 60304 Senlis, France; Université de technologie de Compiègne, Roberval (Mechanics, energy and electricity), Centre de recherche Royallieu - CS 60 319 - 60 203 Compiègne Cedex, FranceUniversité de technologie de Compiègne, Roberval (Mechanics, energy and electricity), Centre de recherche Royallieu - CS 60 319 - 60 203 Compiègne Cedex, France; Corresponding author.Université de technologie de Compiègne, Roberval (Mechanics, energy and electricity), Centre de recherche Royallieu - CS 60 319 - 60 203 Compiègne Cedex, FranceTechnical Center of Mechanical Industries (Cetim), 60304 Senlis, FranceMost of the studies in the literature dealing with fretting have focused on wear mechanisms without considering the formation of oxide layers, whose nature can vary depending on the displacement amplitude and the material pairing. This omission limits the understanding of how different fretting conditions influence surface transformations and ultimately affect wear behavior. This study investigates the wear mechanisms and oxide layer formation in two steel-steel tribosystems, 100Cr6/100Cr6 and 20MnCr5/100Cr6. A parametric approach was adopted, varying displacement amplitudes from 20 to 200 µm under a constant normal load of 10 N, to elucidate the roles of the third body, oxidation, and debris ejection on fretting wear. Friction behavior and electrical contact resistance were monitored in real-time to assess the evolution of contact conditions. Surface characterization was conducted using SEM, Energy dispersive X-ray (EDX), FIB-TEM, and Transmission Kikuchi diffraction (TKD) to analyze wear morphologies and oxide layer composition. The results reveal that although both material pairs developed oxide-based tribolayers at increased amplitudes, only the 20MnCr5/100Cr6 pair exhibited a notable reduction in wear volume between amplitudes of 50 µm and 100 µm. This reduction was attributed to the formation of a more effective third-body layer. Furthermore, TKD analysis demonstrated that magnetite-rich oxide layers formed at 50 µm displacement amplitude in the 100Cr6/100Cr6 pair were more compact and protective compared to the hematite-dominated layers observed at higher amplitudes. These findings underscore the critical influence of material pairing and displacement amplitude on the stability and protective effectiveness of oxide layers in fretting conditions.http://www.sciencedirect.com/science/article/pii/S2590123025027124FrettingSteelOxidationWear mechanismMetallurgical analysis
spellingShingle Roderick Jacques
Abdeljalil Jourani
Salima Bouvier
Yan-Ming Chen
Oxide tribolayer effects on fretting wear of steel under variable displacement amplitude
Results in Engineering
Fretting
Steel
Oxidation
Wear mechanism
Metallurgical analysis
title Oxide tribolayer effects on fretting wear of steel under variable displacement amplitude
title_full Oxide tribolayer effects on fretting wear of steel under variable displacement amplitude
title_fullStr Oxide tribolayer effects on fretting wear of steel under variable displacement amplitude
title_full_unstemmed Oxide tribolayer effects on fretting wear of steel under variable displacement amplitude
title_short Oxide tribolayer effects on fretting wear of steel under variable displacement amplitude
title_sort oxide tribolayer effects on fretting wear of steel under variable displacement amplitude
topic Fretting
Steel
Oxidation
Wear mechanism
Metallurgical analysis
url http://www.sciencedirect.com/science/article/pii/S2590123025027124
work_keys_str_mv AT roderickjacques oxidetribolayereffectsonfrettingwearofsteelundervariabledisplacementamplitude
AT abdeljaliljourani oxidetribolayereffectsonfrettingwearofsteelundervariabledisplacementamplitude
AT salimabouvier oxidetribolayereffectsonfrettingwearofsteelundervariabledisplacementamplitude
AT yanmingchen oxidetribolayereffectsonfrettingwearofsteelundervariabledisplacementamplitude