An experimental study to investigate the role of pyrolysis reaction on in-situ hydrogen generation from sandstone oil reservoirs

In-situ combustion gasification (ISCG) is a technology in the field pilot stage used for hydrogen generation from oil reservoirs. ISCG is implemented by injecting an oxidant (pure oxygen, air, …) into the reservoir to trigger in-situ chemical reactions responsible for hydrogen generation. Pyrolysis...

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Main Authors: Mohamed Abdalsalam Hanfi, Olalekan Saheed Alade, Abdulkadir Tanimu, Mohamed Mahmoud, Sulaiman A. Alarifi
Format: Article
Language:English
Published: KeAi Communications Co., Ltd. 2025-06-01
Series:Petroleum
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Online Access:http://www.sciencedirect.com/science/article/pii/S2405656125000355
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author Mohamed Abdalsalam Hanfi
Olalekan Saheed Alade
Abdulkadir Tanimu
Mohamed Mahmoud
Sulaiman A. Alarifi
author_facet Mohamed Abdalsalam Hanfi
Olalekan Saheed Alade
Abdulkadir Tanimu
Mohamed Mahmoud
Sulaiman A. Alarifi
author_sort Mohamed Abdalsalam Hanfi
collection DOAJ
description In-situ combustion gasification (ISCG) is a technology in the field pilot stage used for hydrogen generation from oil reservoirs. ISCG is implemented by injecting an oxidant (pure oxygen, air, …) into the reservoir to trigger in-situ chemical reactions responsible for hydrogen generation. Pyrolysis reaction is one of the significant reactions triggered by in-situ combustion (ISC). This study used a fixed-bed micro-activity test (MAT) unit to investigate hydrogen generation from crude oil through pyrolysis. Crude oil pyrolysis experiments were conducted in the MAT unit under different temperatures (300 °C, 400 °C, 500 °C, 600 °C), atmospheric pressure, and under a flow of a nitrogen gas. The results showed that the threshold initiation temperature of hydrogen generation and coke formation was about 500 °C. The experiments demonstrated that the introduced sandstone enhanced hydrogen generation and coke formation at high temperatures. The maximum volume of hydrogen generated with sandstone effect reached 8.15 mL at 600 °C, while that without sandstone was only 6.39 mL at 600 °C. The study provides deep insights into the in-situ hydrogen generation from crude oil through pyrolysis. In addition, the obtained data of various pyrolysis products provide a comprehensive representation of crude oil pyrolysis that could promote the existing reaction models of in-situ hydrogen generation from the gasification of crude oil. The findings demonstrate the potential of adopting pyrolysis of crude oil for direct hydrogen generation from reservoirs.
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spelling doaj-art-d2276e360ce241b8b83df3ac1ca814732025-08-20T02:35:22ZengKeAi Communications Co., Ltd.Petroleum2405-65612025-06-0111336637610.1016/j.petlm.2025.05.002An experimental study to investigate the role of pyrolysis reaction on in-situ hydrogen generation from sandstone oil reservoirsMohamed Abdalsalam Hanfi0Olalekan Saheed Alade1Abdulkadir Tanimu2Mohamed Mahmoud3Sulaiman A. Alarifi4Department of Petroleum Engineering, King Fahd University of Petroleum & Minerals (KFUPM), Dhahran, 31261, Saudi ArabiaCenter for Integrative Petroleum Research (CIPR), King Fahd University of Petroleum & Minerals, Dhahran, 31261, Saudi ArabiaInterdisciplinary Research Center for Refining and Advanced Chemicals, Research Institute, King Fahd University of Petroleum and Minerals, Dhahran 31261, Saudi ArabiaDepartment of Petroleum Engineering, King Fahd University of Petroleum & Minerals (KFUPM), Dhahran, 31261, Saudi ArabiaDepartment of Petroleum Engineering, King Fahd University of Petroleum & Minerals (KFUPM), Dhahran, 31261, Saudi Arabia; Corresponding author.In-situ combustion gasification (ISCG) is a technology in the field pilot stage used for hydrogen generation from oil reservoirs. ISCG is implemented by injecting an oxidant (pure oxygen, air, …) into the reservoir to trigger in-situ chemical reactions responsible for hydrogen generation. Pyrolysis reaction is one of the significant reactions triggered by in-situ combustion (ISC). This study used a fixed-bed micro-activity test (MAT) unit to investigate hydrogen generation from crude oil through pyrolysis. Crude oil pyrolysis experiments were conducted in the MAT unit under different temperatures (300 °C, 400 °C, 500 °C, 600 °C), atmospheric pressure, and under a flow of a nitrogen gas. The results showed that the threshold initiation temperature of hydrogen generation and coke formation was about 500 °C. The experiments demonstrated that the introduced sandstone enhanced hydrogen generation and coke formation at high temperatures. The maximum volume of hydrogen generated with sandstone effect reached 8.15 mL at 600 °C, while that without sandstone was only 6.39 mL at 600 °C. The study provides deep insights into the in-situ hydrogen generation from crude oil through pyrolysis. In addition, the obtained data of various pyrolysis products provide a comprehensive representation of crude oil pyrolysis that could promote the existing reaction models of in-situ hydrogen generation from the gasification of crude oil. The findings demonstrate the potential of adopting pyrolysis of crude oil for direct hydrogen generation from reservoirs.http://www.sciencedirect.com/science/article/pii/S2405656125000355Hydrogen generationCrude oilIn-situ pyrolysisSandstone mineralogyPyrolysis products
spellingShingle Mohamed Abdalsalam Hanfi
Olalekan Saheed Alade
Abdulkadir Tanimu
Mohamed Mahmoud
Sulaiman A. Alarifi
An experimental study to investigate the role of pyrolysis reaction on in-situ hydrogen generation from sandstone oil reservoirs
Petroleum
Hydrogen generation
Crude oil
In-situ pyrolysis
Sandstone mineralogy
Pyrolysis products
title An experimental study to investigate the role of pyrolysis reaction on in-situ hydrogen generation from sandstone oil reservoirs
title_full An experimental study to investigate the role of pyrolysis reaction on in-situ hydrogen generation from sandstone oil reservoirs
title_fullStr An experimental study to investigate the role of pyrolysis reaction on in-situ hydrogen generation from sandstone oil reservoirs
title_full_unstemmed An experimental study to investigate the role of pyrolysis reaction on in-situ hydrogen generation from sandstone oil reservoirs
title_short An experimental study to investigate the role of pyrolysis reaction on in-situ hydrogen generation from sandstone oil reservoirs
title_sort experimental study to investigate the role of pyrolysis reaction on in situ hydrogen generation from sandstone oil reservoirs
topic Hydrogen generation
Crude oil
In-situ pyrolysis
Sandstone mineralogy
Pyrolysis products
url http://www.sciencedirect.com/science/article/pii/S2405656125000355
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