Microwave Assisted Synthesis of Novel 1,2,3,4-Tetrahydrocarbazolyl thiazolidin-4-ones and Azetidin-2-ones and its Biological Behavior

A new family of 1,2,3,4 – tetrahydrocarbazolyl thiazolidin-4-ones (4a-e) and 1,2,3,4–tetrahydrocarbazolyl azetidin-2-ones (5a-e) were individually derived using N-[(α-substituted bezylidenehydrazino) acetyl] -1,2,3,4-tetra-hydrocarbazoles 3a-e by cyclization with thioglycolic acid and chloro- acetyl...

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Main Authors: T. Surendiran, S. Balasubramanian, Sivaraj D.
Format: Article
Language:English
Published: Wiley 2009-01-01
Series:E-Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2009/424172
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author T. Surendiran
S. Balasubramanian
Sivaraj D.
author_facet T. Surendiran
S. Balasubramanian
Sivaraj D.
author_sort T. Surendiran
collection DOAJ
description A new family of 1,2,3,4 – tetrahydrocarbazolyl thiazolidin-4-ones (4a-e) and 1,2,3,4–tetrahydrocarbazolyl azetidin-2-ones (5a-e) were individually derived using N-[(α-substituted bezylidenehydrazino) acetyl] -1,2,3,4-tetra-hydrocarbazoles 3a-e by cyclization with thioglycolic acid and chloro- acetylchloride respectively. The compounds (3a-e) were prepared by condensation of N-(hydrazinoacetyl) 1,2,3,4-tetrahydrocarbazole (2) with a series of aldehydes. The compound 2 was obtained by the hydrazinolysis of N-(chloroacetyl)-1,2,3,4-tetrahydrocarbazole (1). These products were characterized by IR, NMR, MASS spectra and by elemental analysis. All the titled compounds (4a-e) and 5(a-e) were screened for antibacterial and antifungal activities.
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spelling doaj-art-d14dda4d546a4366a7ce7e81b028d69c2025-08-20T03:24:01ZengWileyE-Journal of Chemistry0973-49452090-98102009-01-016S1S374S38010.1155/2009/424172Microwave Assisted Synthesis of Novel 1,2,3,4-Tetrahydrocarbazolyl thiazolidin-4-ones and Azetidin-2-ones and its Biological BehaviorT. Surendiran0S. Balasubramanian1Sivaraj D.2Research Department of Chemistry, Sathyabama University, Jeppiaar Nagar, Chennai, IndiaResearch Department of Chemistry, Mohamed Sathak A.J.College of Engineering, Chennai, IndiaEmirates Environmental Protection Company (EPO), Dubai, UAEA new family of 1,2,3,4 – tetrahydrocarbazolyl thiazolidin-4-ones (4a-e) and 1,2,3,4–tetrahydrocarbazolyl azetidin-2-ones (5a-e) were individually derived using N-[(α-substituted bezylidenehydrazino) acetyl] -1,2,3,4-tetra-hydrocarbazoles 3a-e by cyclization with thioglycolic acid and chloro- acetylchloride respectively. The compounds (3a-e) were prepared by condensation of N-(hydrazinoacetyl) 1,2,3,4-tetrahydrocarbazole (2) with a series of aldehydes. The compound 2 was obtained by the hydrazinolysis of N-(chloroacetyl)-1,2,3,4-tetrahydrocarbazole (1). These products were characterized by IR, NMR, MASS spectra and by elemental analysis. All the titled compounds (4a-e) and 5(a-e) were screened for antibacterial and antifungal activities.http://dx.doi.org/10.1155/2009/424172
spellingShingle T. Surendiran
S. Balasubramanian
Sivaraj D.
Microwave Assisted Synthesis of Novel 1,2,3,4-Tetrahydrocarbazolyl thiazolidin-4-ones and Azetidin-2-ones and its Biological Behavior
E-Journal of Chemistry
title Microwave Assisted Synthesis of Novel 1,2,3,4-Tetrahydrocarbazolyl thiazolidin-4-ones and Azetidin-2-ones and its Biological Behavior
title_full Microwave Assisted Synthesis of Novel 1,2,3,4-Tetrahydrocarbazolyl thiazolidin-4-ones and Azetidin-2-ones and its Biological Behavior
title_fullStr Microwave Assisted Synthesis of Novel 1,2,3,4-Tetrahydrocarbazolyl thiazolidin-4-ones and Azetidin-2-ones and its Biological Behavior
title_full_unstemmed Microwave Assisted Synthesis of Novel 1,2,3,4-Tetrahydrocarbazolyl thiazolidin-4-ones and Azetidin-2-ones and its Biological Behavior
title_short Microwave Assisted Synthesis of Novel 1,2,3,4-Tetrahydrocarbazolyl thiazolidin-4-ones and Azetidin-2-ones and its Biological Behavior
title_sort microwave assisted synthesis of novel 1 2 3 4 tetrahydrocarbazolyl thiazolidin 4 ones and azetidin 2 ones and its biological behavior
url http://dx.doi.org/10.1155/2009/424172
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AT sbalasubramanian microwaveassistedsynthesisofnovel1234tetrahydrocarbazolylthiazolidin4onesandazetidin2onesanditsbiologicalbehavior
AT sivarajd microwaveassistedsynthesisofnovel1234tetrahydrocarbazolylthiazolidin4onesandazetidin2onesanditsbiologicalbehavior