Determination Micro Spectrohotometric of Pyridoxine Hydrochloride and Nicotinamide via Derivative Spectrophotometry First and Second
A simple, sensitive and accurate spectrophotometric method for determination of PYR.HCl and NTA in pure and pharmaceutical forms. The method based on group of known digital data used to separate the response signals for sample contains the two components without need to separating via first and sec...
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| Format: | Article |
| Language: | English |
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Tikrit University
2023-02-01
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| Series: | Tikrit Journal of Pure Science |
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| Online Access: | https://tjpsj.org/index.php/tjps/article/view/934 |
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| author | Mohammed Qasim Al-Sammaraee Khlaf Faris Al-Sammaraee |
| author_facet | Mohammed Qasim Al-Sammaraee Khlaf Faris Al-Sammaraee |
| author_sort | Mohammed Qasim Al-Sammaraee |
| collection | DOAJ |
| description |
A simple, sensitive and accurate spectrophotometric method for determination of PYR.HCl and NTA in pure and pharmaceutical forms. The method based on group of known digital data used to separate the response signals for sample contains the two components without need to separating via first and second derivative of spectra. The method obtained obeying to the Beers law in the concentration range between )5-45 µg.ml-1( for two components in the presence of PYR. HCl )15µg.ml-1( and NTA (5µg.ml-1) with another components at wavelength (210 nm ) respectively . The Rec % range was between ) 98.5354 - 103.4335 % (and RSD% (0.0864 - 0.1487 %), LOD) 1.0822 µg.ml-1, ( LOQ ( 3.6075 µg.ml-1 (PYR.HCl in presence of NTA, The Rec% range was between )96.1418 - 102.9273 % (and RSD% (0.2165–0.4933 % ), LOD (0.7273µg.ml-1 ,(LOQ (2.4252 µg.ml-1( NTA in presence of PYR. HCl .
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| format | Article |
| id | doaj-art-d0e05338402a4068942fb8603d2a8971 |
| institution | Kabale University |
| issn | 1813-1662 2415-1726 |
| language | English |
| publishDate | 2023-02-01 |
| publisher | Tikrit University |
| record_format | Article |
| series | Tikrit Journal of Pure Science |
| spelling | doaj-art-d0e05338402a4068942fb8603d2a89712025-08-20T03:28:59ZengTikrit UniversityTikrit Journal of Pure Science1813-16622415-17262023-02-01221210.25130/tjps.v22i12.934Determination Micro Spectrohotometric of Pyridoxine Hydrochloride and Nicotinamide via Derivative Spectrophotometry First and SecondMohammed Qasim Al-SammaraeeKhlaf Faris Al-Sammaraee A simple, sensitive and accurate spectrophotometric method for determination of PYR.HCl and NTA in pure and pharmaceutical forms. The method based on group of known digital data used to separate the response signals for sample contains the two components without need to separating via first and second derivative of spectra. The method obtained obeying to the Beers law in the concentration range between )5-45 µg.ml-1( for two components in the presence of PYR. HCl )15µg.ml-1( and NTA (5µg.ml-1) with another components at wavelength (210 nm ) respectively . The Rec % range was between ) 98.5354 - 103.4335 % (and RSD% (0.0864 - 0.1487 %), LOD) 1.0822 µg.ml-1, ( LOQ ( 3.6075 µg.ml-1 (PYR.HCl in presence of NTA, The Rec% range was between )96.1418 - 102.9273 % (and RSD% (0.2165–0.4933 % ), LOD (0.7273µg.ml-1 ,(LOQ (2.4252 µg.ml-1( NTA in presence of PYR. HCl . https://tjpsj.org/index.php/tjps/article/view/934derivative of spectraPyridoxine HydrochlorideNicotinamide |
| spellingShingle | Mohammed Qasim Al-Sammaraee Khlaf Faris Al-Sammaraee Determination Micro Spectrohotometric of Pyridoxine Hydrochloride and Nicotinamide via Derivative Spectrophotometry First and Second Tikrit Journal of Pure Science derivative of spectra Pyridoxine Hydrochloride Nicotinamide |
| title | Determination Micro Spectrohotometric of Pyridoxine Hydrochloride and Nicotinamide via Derivative Spectrophotometry First and Second |
| title_full | Determination Micro Spectrohotometric of Pyridoxine Hydrochloride and Nicotinamide via Derivative Spectrophotometry First and Second |
| title_fullStr | Determination Micro Spectrohotometric of Pyridoxine Hydrochloride and Nicotinamide via Derivative Spectrophotometry First and Second |
| title_full_unstemmed | Determination Micro Spectrohotometric of Pyridoxine Hydrochloride and Nicotinamide via Derivative Spectrophotometry First and Second |
| title_short | Determination Micro Spectrohotometric of Pyridoxine Hydrochloride and Nicotinamide via Derivative Spectrophotometry First and Second |
| title_sort | determination micro spectrohotometric of pyridoxine hydrochloride and nicotinamide via derivative spectrophotometry first and second |
| topic | derivative of spectra Pyridoxine Hydrochloride Nicotinamide |
| url | https://tjpsj.org/index.php/tjps/article/view/934 |
| work_keys_str_mv | AT mohammedqasimalsammaraee determinationmicrospectrohotometricofpyridoxinehydrochlorideandnicotinamideviaderivativespectrophotometryfirstandsecond AT khlaffarisalsammaraee determinationmicrospectrohotometricofpyridoxinehydrochlorideandnicotinamideviaderivativespectrophotometryfirstandsecond |