Comprehensive microstructural evolution analysis of AA5083-H116 alloy welded joints using pulsed GMAW and 80Ar19He1O2 shielding gas

This study investigates the microstructural evolution of AA5083-H116 butt-welded joints produced by automated pulsed GMAW (GMAW-P) with an 80Ar-19He–1O2 shielding gas under varying heat inputs. Multiscale characterization techniques—including optical and scanning electron microscopy, EBSD, XRD, and...

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Main Authors: Enrique Esteban Niebles-Nuñez, Jimy Unfried-Silgado, Jaime Elías Torres-Salcedo, Conrado R.M. Afonso, Antonio J. Ramírez
Format: Article
Language:English
Published: Elsevier 2025-09-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425019192
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author Enrique Esteban Niebles-Nuñez
Jimy Unfried-Silgado
Jaime Elías Torres-Salcedo
Conrado R.M. Afonso
Antonio J. Ramírez
author_facet Enrique Esteban Niebles-Nuñez
Jimy Unfried-Silgado
Jaime Elías Torres-Salcedo
Conrado R.M. Afonso
Antonio J. Ramírez
author_sort Enrique Esteban Niebles-Nuñez
collection DOAJ
description This study investigates the microstructural evolution of AA5083-H116 butt-welded joints produced by automated pulsed GMAW (GMAW-P) with an 80Ar-19He–1O2 shielding gas under varying heat inputs. Multiscale characterization techniques—including optical and scanning electron microscopy, EBSD, XRD, and transmission electron microscopy (TEM) along with automated crystallographic mapping (ASTAR), were used to assess recrystallization, phase transformations, and grain growth. The coarse-grained zone (GGZ) exhibited complete recrystallization and abnormal grain growth (14.2–18.6 μm), with low misorientation (≈2°) and dominant low-angle boundaries (<7°). The mixed grain zone (MGZ) showed partial recrystallization and subgrains, while the fine-grained zone (GFZ) displayed incipient recrystallization (2°–10°) and residual substructures near the base metal. The Al-FCC matrix retained Mg in solid solution, with secondary phases (Al(Fe,Mn), Al(Fe,Mn,Cr) and nanoscale precipitates (Al3Mg2, Al6(Mn,Fe)) at grain boundaries. Results demonstrate that heat input critically governs microstructural stability, dictating recrystallization kinetics and precipitate distribution. These findings enable optimized welding parameters to enhance joint performance in demanding naval, aerospace, and automotive applications.
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publishDate 2025-09-01
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spelling doaj-art-cff8b655d52e4dc884fc6ad88a2e6bc42025-08-20T03:59:22ZengElsevierJournal of Materials Research and Technology2238-78542025-09-01381263127510.1016/j.jmrt.2025.07.261Comprehensive microstructural evolution analysis of AA5083-H116 alloy welded joints using pulsed GMAW and 80Ar19He1O2 shielding gasEnrique Esteban Niebles-Nuñez0Jimy Unfried-Silgado1Jaime Elías Torres-Salcedo2Conrado R.M. Afonso3Antonio J. Ramírez4Programa de Ingeniería Mecánica, Facultad de ingeniería, Grupo de investigación IMTEF, Universidad Autónoma del Caribe, Barranquilla, 080020, ColombiaDepartamento de Ingeniería Mecánica. Grupo de investigación ICT. Universidad de Córdoba, Montería, 230002, ColombiaPrograma de Doctorado en Ingeniería Mecánica, Universidad del Norte, Barranquilla, 081001, ColombiaDepartamento de Engenharia de Materiais (DEMa), Universidade Federal de São Carlos (UFSCar), 13.565-905, São Carlos, SP, Brazil; Corresponding author.Welding Engineering Program, The Ohio State University Columbus, Columbus, OH, USAThis study investigates the microstructural evolution of AA5083-H116 butt-welded joints produced by automated pulsed GMAW (GMAW-P) with an 80Ar-19He–1O2 shielding gas under varying heat inputs. Multiscale characterization techniques—including optical and scanning electron microscopy, EBSD, XRD, and transmission electron microscopy (TEM) along with automated crystallographic mapping (ASTAR), were used to assess recrystallization, phase transformations, and grain growth. The coarse-grained zone (GGZ) exhibited complete recrystallization and abnormal grain growth (14.2–18.6 μm), with low misorientation (≈2°) and dominant low-angle boundaries (<7°). The mixed grain zone (MGZ) showed partial recrystallization and subgrains, while the fine-grained zone (GFZ) displayed incipient recrystallization (2°–10°) and residual substructures near the base metal. The Al-FCC matrix retained Mg in solid solution, with secondary phases (Al(Fe,Mn), Al(Fe,Mn,Cr) and nanoscale precipitates (Al3Mg2, Al6(Mn,Fe)) at grain boundaries. Results demonstrate that heat input critically governs microstructural stability, dictating recrystallization kinetics and precipitate distribution. These findings enable optimized welding parameters to enhance joint performance in demanding naval, aerospace, and automotive applications.http://www.sciencedirect.com/science/article/pii/S2238785425019192AA5083-H116 welded jointsGMAW-PMicrostructural evolutionRecrystallization and grain growthIntermetallic precipitates
spellingShingle Enrique Esteban Niebles-Nuñez
Jimy Unfried-Silgado
Jaime Elías Torres-Salcedo
Conrado R.M. Afonso
Antonio J. Ramírez
Comprehensive microstructural evolution analysis of AA5083-H116 alloy welded joints using pulsed GMAW and 80Ar19He1O2 shielding gas
Journal of Materials Research and Technology
AA5083-H116 welded joints
GMAW-P
Microstructural evolution
Recrystallization and grain growth
Intermetallic precipitates
title Comprehensive microstructural evolution analysis of AA5083-H116 alloy welded joints using pulsed GMAW and 80Ar19He1O2 shielding gas
title_full Comprehensive microstructural evolution analysis of AA5083-H116 alloy welded joints using pulsed GMAW and 80Ar19He1O2 shielding gas
title_fullStr Comprehensive microstructural evolution analysis of AA5083-H116 alloy welded joints using pulsed GMAW and 80Ar19He1O2 shielding gas
title_full_unstemmed Comprehensive microstructural evolution analysis of AA5083-H116 alloy welded joints using pulsed GMAW and 80Ar19He1O2 shielding gas
title_short Comprehensive microstructural evolution analysis of AA5083-H116 alloy welded joints using pulsed GMAW and 80Ar19He1O2 shielding gas
title_sort comprehensive microstructural evolution analysis of aa5083 h116 alloy welded joints using pulsed gmaw and 80ar19he1o2 shielding gas
topic AA5083-H116 welded joints
GMAW-P
Microstructural evolution
Recrystallization and grain growth
Intermetallic precipitates
url http://www.sciencedirect.com/science/article/pii/S2238785425019192
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