UHPLC-MS/MS chemical profiling, preliminary toxicity, in vitro antioxidant potential and antimicrobial activity of Brachyotum naudinii Triana flowers

Chemical compounds of Brachyotum naudinii Triana flowers were analyzed using UHPLC-MS/MS. Anthocyanin dry extract was obtained by accelerated solvent extraction with 70% ethanol acidified with citric acid (pH 3.18) and then spray dried. Preliminary toxicity of anthocyanin extract was evaluated using...

Full description

Saved in:
Bibliographic Details
Main Authors: Marco Rolando Aronés Jara, Edgar Cárdenas Landeo, Kirianova Godoy Bautista, Eylen Almendra Ortiz Pérez, Juan Clímaco Paniagua Segovia, Hugo Roberto Luna Molero, Stephanny Massiel Barbarán Vilcatoma, Mónica Gómez Quispe, Edith Eveling Conislla Cáceres, Jesús Javier Paniagua Segovia, Anas Rashid, María Segunda Aurora Prado
Format: Article
Language:English
Published: Taylor & Francis Group 2024-12-01
Series:Journal of Taibah University for Science
Subjects:
Online Access:https://www.tandfonline.com/doi/10.1080/16583655.2024.2398230
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1850114883655303168
author Marco Rolando Aronés Jara
Edgar Cárdenas Landeo
Kirianova Godoy Bautista
Eylen Almendra Ortiz Pérez
Juan Clímaco Paniagua Segovia
Hugo Roberto Luna Molero
Stephanny Massiel Barbarán Vilcatoma
Mónica Gómez Quispe
Edith Eveling Conislla Cáceres
Jesús Javier Paniagua Segovia
Anas Rashid
María Segunda Aurora Prado
author_facet Marco Rolando Aronés Jara
Edgar Cárdenas Landeo
Kirianova Godoy Bautista
Eylen Almendra Ortiz Pérez
Juan Clímaco Paniagua Segovia
Hugo Roberto Luna Molero
Stephanny Massiel Barbarán Vilcatoma
Mónica Gómez Quispe
Edith Eveling Conislla Cáceres
Jesús Javier Paniagua Segovia
Anas Rashid
María Segunda Aurora Prado
author_sort Marco Rolando Aronés Jara
collection DOAJ
description Chemical compounds of Brachyotum naudinii Triana flowers were analyzed using UHPLC-MS/MS. Anthocyanin dry extract was obtained by accelerated solvent extraction with 70% ethanol acidified with citric acid (pH 3.18) and then spray dried. Preliminary toxicity of anthocyanin extract was evaluated using Artemia salina Leach, while its antioxidant capacity was measured by DPPH• and ABTS•+ methods, and reducing capacity was assessed using FRAP assay. Results showed the flowers comprise 39% tannins, 21% flavonol glycosides, 14% organic acids, 11% anthocyanins, 7% coumaric acid derivatives, 4% polar lipids, and 4% disaccharides. Anthocyanin extract exhibited moderate toxicity against Artemia salina (LC50 = 106.9 ± 9.9 µg mL−1) and showed inhibitory effects on DPPH• and ABTS•+ radicals, as well as reducing capacity in FRAP assay, though statistically different from Trolox (p < 0.05). The flowers have demonstrated antimicrobial activity against Staphylococcus aureus and are a source of novel anthocyanin compounds with antioxidant potential.
format Article
id doaj-art-ceffcde17aa8474689a0f0bfd4abf602
institution OA Journals
issn 1658-3655
language English
publishDate 2024-12-01
publisher Taylor & Francis Group
record_format Article
series Journal of Taibah University for Science
spelling doaj-art-ceffcde17aa8474689a0f0bfd4abf6022025-08-20T02:36:43ZengTaylor & Francis GroupJournal of Taibah University for Science1658-36552024-12-0118110.1080/16583655.2024.2398230UHPLC-MS/MS chemical profiling, preliminary toxicity, in vitro antioxidant potential and antimicrobial activity of Brachyotum naudinii Triana flowersMarco Rolando Aronés Jara0Edgar Cárdenas Landeo1Kirianova Godoy Bautista2Eylen Almendra Ortiz Pérez3Juan Clímaco Paniagua Segovia4Hugo Roberto Luna Molero5Stephanny Massiel Barbarán Vilcatoma6Mónica Gómez Quispe7Edith Eveling Conislla Cáceres8Jesús Javier Paniagua Segovia9Anas Rashid10María Segunda Aurora Prado11Professional School of Pharmacy and Biochemistry, Faculty of Health Sciences, National University of San Cristóbal of Huamanga, Ayacucho, PeruProfessional School of Pharmacy and Biochemistry, Faculty of Health Sciences, National University of San Cristóbal of Huamanga, Ayacucho, PeruProfessional School of Pharmacy and Biochemistry, Faculty of Health Sciences, National University of San Cristóbal of Huamanga, Ayacucho, PeruProfessional School of Pharmacy and Biochemistry, Faculty of Health Sciences, National University of San Cristóbal of Huamanga, Ayacucho, PeruProfessional School of Pharmacy and Biochemistry, Faculty of Health Sciences, National University of San Cristóbal of Huamanga, Ayacucho, PeruProfessional School of Pharmacy and Biochemistry, Faculty of Health Sciences, National University of San Cristóbal of Huamanga, Ayacucho, PeruProfessional School of Pharmacy and Biochemistry, Faculty of Health Sciences, National University of San Cristóbal of Huamanga, Ayacucho, PeruProfessional School of Pharmacy and Biochemistry, Faculty of Health Sciences, National University of San Cristóbal of Huamanga, Ayacucho, PeruProfessional School of Pharmacy and Biochemistry, Faculty of Health Sciences, National University of San Cristóbal of Huamanga, Ayacucho, PeruProfessional School of Engineering in Food Industries, Faculty of Chemical Engineering and Metallurgy, National University of San Cristóbal of Huamanga, Ayacucho, PeruDepartment of Neuroscience “Rita Levi Montalcini”, School of Medicine and Surgery, University of Torino, Torino, ItalyDepartment of Pharmacy, School of Pharmaceutical Sciences, University of São Paulo, São Paulo, BrazilChemical compounds of Brachyotum naudinii Triana flowers were analyzed using UHPLC-MS/MS. Anthocyanin dry extract was obtained by accelerated solvent extraction with 70% ethanol acidified with citric acid (pH 3.18) and then spray dried. Preliminary toxicity of anthocyanin extract was evaluated using Artemia salina Leach, while its antioxidant capacity was measured by DPPH• and ABTS•+ methods, and reducing capacity was assessed using FRAP assay. Results showed the flowers comprise 39% tannins, 21% flavonol glycosides, 14% organic acids, 11% anthocyanins, 7% coumaric acid derivatives, 4% polar lipids, and 4% disaccharides. Anthocyanin extract exhibited moderate toxicity against Artemia salina (LC50 = 106.9 ± 9.9 µg mL−1) and showed inhibitory effects on DPPH• and ABTS•+ radicals, as well as reducing capacity in FRAP assay, though statistically different from Trolox (p < 0.05). The flowers have demonstrated antimicrobial activity against Staphylococcus aureus and are a source of novel anthocyanin compounds with antioxidant potential.https://www.tandfonline.com/doi/10.1080/16583655.2024.2398230Melastomataceaeendemic species of rocky outcropsLC-MS/MSnew bioactive compoundsantioxidant potentialArtemia salina Leach
spellingShingle Marco Rolando Aronés Jara
Edgar Cárdenas Landeo
Kirianova Godoy Bautista
Eylen Almendra Ortiz Pérez
Juan Clímaco Paniagua Segovia
Hugo Roberto Luna Molero
Stephanny Massiel Barbarán Vilcatoma
Mónica Gómez Quispe
Edith Eveling Conislla Cáceres
Jesús Javier Paniagua Segovia
Anas Rashid
María Segunda Aurora Prado
UHPLC-MS/MS chemical profiling, preliminary toxicity, in vitro antioxidant potential and antimicrobial activity of Brachyotum naudinii Triana flowers
Journal of Taibah University for Science
Melastomataceae
endemic species of rocky outcrops
LC-MS/MS
new bioactive compounds
antioxidant potential
Artemia salina Leach
title UHPLC-MS/MS chemical profiling, preliminary toxicity, in vitro antioxidant potential and antimicrobial activity of Brachyotum naudinii Triana flowers
title_full UHPLC-MS/MS chemical profiling, preliminary toxicity, in vitro antioxidant potential and antimicrobial activity of Brachyotum naudinii Triana flowers
title_fullStr UHPLC-MS/MS chemical profiling, preliminary toxicity, in vitro antioxidant potential and antimicrobial activity of Brachyotum naudinii Triana flowers
title_full_unstemmed UHPLC-MS/MS chemical profiling, preliminary toxicity, in vitro antioxidant potential and antimicrobial activity of Brachyotum naudinii Triana flowers
title_short UHPLC-MS/MS chemical profiling, preliminary toxicity, in vitro antioxidant potential and antimicrobial activity of Brachyotum naudinii Triana flowers
title_sort uhplc ms ms chemical profiling preliminary toxicity in vitro antioxidant potential and antimicrobial activity of brachyotum naudinii triana flowers
topic Melastomataceae
endemic species of rocky outcrops
LC-MS/MS
new bioactive compounds
antioxidant potential
Artemia salina Leach
url https://www.tandfonline.com/doi/10.1080/16583655.2024.2398230
work_keys_str_mv AT marcorolandoaronesjara uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers
AT edgarcardenaslandeo uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers
AT kirianovagodoybautista uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers
AT eylenalmendraortizperez uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers
AT juanclimacopaniaguasegovia uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers
AT hugorobertolunamolero uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers
AT stephannymassielbarbaranvilcatoma uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers
AT monicagomezquispe uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers
AT edithevelingconisllacaceres uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers
AT jesusjavierpaniaguasegovia uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers
AT anasrashid uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers
AT mariasegundaauroraprado uhplcmsmschemicalprofilingpreliminarytoxicityinvitroantioxidantpotentialandantimicrobialactivityofbrachyotumnaudiniitrianaflowers