Microwave Extraction of Gallic Acid Equivalent of Total Flavonoids from Nigella sativa

Unfortunately, cancer is the most widespread disease in worldwide. Colorectal cancer is declared as the third most common cancer type. The usage of controlled-drug-releasing capsules for treating the cancer diseases has becoming more and more popular in the whole world. In the production of drug raw...

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Main Authors: Burcu Özturk, Sibel Yiğitarslan
Format: Article
Language:English
Published: izzet kara 2017-12-01
Series:International Journal of Secondary Metabolite
Subjects:
Online Access:https://dergipark.org.tr/tr/pub/ijsm/issue/32131/363838?publisher=ijate
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author Burcu Özturk
Sibel Yiğitarslan
author_facet Burcu Özturk
Sibel Yiğitarslan
author_sort Burcu Özturk
collection DOAJ
description Unfortunately, cancer is the most widespread disease in worldwide. Colorectal cancer is declared as the third most common cancer type. The usage of controlled-drug-releasing capsules for treating the cancer diseases has becoming more and more popular in the whole world. In the production of drug raw material, the first operation is an extraction of the phytochemicals from the herbal plant. The yield of the extraction operation is an important step for the economical and efficient production of such capsules. Thus the aim of this study was to optimize the microwave extraction of total flavonoids from Nigella sativa with methanol by using Response Surface Methodology based on Box-Behnken design. Microwave extraction experiments had been carried out with the parameters of microwave power, solid/liquid ratio and the and the application time. The optimum values were determined as 0.62 kW, 1/(47) g/mL, and 10.84 second, respectively. According to the quadratic surface of the extraction yield depending on those parameters, 309.60 mg/100g of gallic acid equivalent of total flavonoids can be obtained at the optimum conditions. As a result of the statistical analysis, this function was found as capable of expressing the effect of the parameters on the amount of total flavonoid production in industry. Nowadays, drying of the extracts and loading of the aqueous solutions of them into the prebiotic-coated probiotic capsules have been under consideration.
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spelling doaj-art-ce89ede21e2e4ef8a94f83b8dafc49c92025-08-20T02:19:30Zengizzet karaInternational Journal of Secondary Metabolite2148-69052017-12-0143, Special Issue 111712410.21448/ijsm.363838618Microwave Extraction of Gallic Acid Equivalent of Total Flavonoids from Nigella sativaBurcu ÖzturkSibel YiğitarslanUnfortunately, cancer is the most widespread disease in worldwide. Colorectal cancer is declared as the third most common cancer type. The usage of controlled-drug-releasing capsules for treating the cancer diseases has becoming more and more popular in the whole world. In the production of drug raw material, the first operation is an extraction of the phytochemicals from the herbal plant. The yield of the extraction operation is an important step for the economical and efficient production of such capsules. Thus the aim of this study was to optimize the microwave extraction of total flavonoids from Nigella sativa with methanol by using Response Surface Methodology based on Box-Behnken design. Microwave extraction experiments had been carried out with the parameters of microwave power, solid/liquid ratio and the and the application time. The optimum values were determined as 0.62 kW, 1/(47) g/mL, and 10.84 second, respectively. According to the quadratic surface of the extraction yield depending on those parameters, 309.60 mg/100g of gallic acid equivalent of total flavonoids can be obtained at the optimum conditions. As a result of the statistical analysis, this function was found as capable of expressing the effect of the parameters on the amount of total flavonoid production in industry. Nowadays, drying of the extracts and loading of the aqueous solutions of them into the prebiotic-coated probiotic capsules have been under consideration.https://dergipark.org.tr/tr/pub/ijsm/issue/32131/363838?publisher=ijatenigella sativaextractionflavonoidresponse surface methodology
spellingShingle Burcu Özturk
Sibel Yiğitarslan
Microwave Extraction of Gallic Acid Equivalent of Total Flavonoids from Nigella sativa
International Journal of Secondary Metabolite
nigella sativa
extraction
flavonoid
response surface methodology
title Microwave Extraction of Gallic Acid Equivalent of Total Flavonoids from Nigella sativa
title_full Microwave Extraction of Gallic Acid Equivalent of Total Flavonoids from Nigella sativa
title_fullStr Microwave Extraction of Gallic Acid Equivalent of Total Flavonoids from Nigella sativa
title_full_unstemmed Microwave Extraction of Gallic Acid Equivalent of Total Flavonoids from Nigella sativa
title_short Microwave Extraction of Gallic Acid Equivalent of Total Flavonoids from Nigella sativa
title_sort microwave extraction of gallic acid equivalent of total flavonoids from nigella sativa
topic nigella sativa
extraction
flavonoid
response surface methodology
url https://dergipark.org.tr/tr/pub/ijsm/issue/32131/363838?publisher=ijate
work_keys_str_mv AT burcuozturk microwaveextractionofgallicacidequivalentoftotalflavonoidsfromnigellasativa
AT sibelyigitarslan microwaveextractionofgallicacidequivalentoftotalflavonoidsfromnigellasativa