Synthesis, Characterization and Gas Sensor Application of New Composite Based on MWCNTs:CoPc:Metal Oxide
The synthesis of new substituted cobalt Phthalocyanine (CoPc) was carried out using starting materials Naphthalene-1,4,5, tetracarbonic acid dianhydride (NDI) employing dry process method. Metal oxides (MO) alloy of (60%Ni3O4 40%-Co3O4 ) have been functionalized with multiwall carbon nanotubes (F-MW...
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University of Baghdad, College of Science for Women
2021-06-01
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| Series: | مجلة بغداد للعلوم |
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| Online Access: | https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/5073 |
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| author | Mohanad Mousa Kareem Burak Yahya Kadem Emman J. Mohammad Abbas Jassim Atiyah |
| author_facet | Mohanad Mousa Kareem Burak Yahya Kadem Emman J. Mohammad Abbas Jassim Atiyah |
| author_sort | Mohanad Mousa Kareem |
| collection | DOAJ |
| description | The synthesis of new substituted cobalt Phthalocyanine (CoPc) was carried out using starting materials Naphthalene-1,4,5, tetracarbonic acid dianhydride (NDI) employing dry process method. Metal oxides (MO) alloy of (60%Ni3O4 40%-Co3O4 ) have been functionalized with multiwall carbon nanotubes (F-MWCNTs) to produce (F-MWCNTs/MO) nanocomposite (E2) and mixed with CoPc to yield (F-MWCNT/CoPc/MO) (E3). These composites were investigated using different analytical and spectrophotometric methods such as 1H-NMR (0-18 ppm), FTIR spectroscopy in the range of (400-4000cm-1), powder X-rays diffraction (PXRD, 2θ o = 10-80), Raman spectroscopy (0-4000 cm-1), and UV-Visible spectrophotometry (0-800 nm). Then the activity of these materials was investigated as a gas sensing of (Ammonia, Methanol and Acetone). For each case, 0.2 mg/.mL of the prepared Copc, Copc/MWCNT, Copc/MWCNTs–MO was dispersed in 1m of ammonia, methanol and acetone at 298K. The surface morphology of the prepared materials was heterogeneous. |
| format | Article |
| id | doaj-art-ce5bc84f9f75468a89b3283908636a3d |
| institution | Kabale University |
| issn | 2078-8665 2411-7986 |
| language | English |
| publishDate | 2021-06-01 |
| publisher | University of Baghdad, College of Science for Women |
| record_format | Article |
| series | مجلة بغداد للعلوم |
| spelling | doaj-art-ce5bc84f9f75468a89b3283908636a3d2025-08-20T03:38:43ZengUniversity of Baghdad, College of Science for Womenمجلة بغداد للعلوم2078-86652411-79862021-06-0118210.21123/bsj.2021.18.2.0384Synthesis, Characterization and Gas Sensor Application of New Composite Based on MWCNTs:CoPc:Metal OxideMohanad Mousa Kareem0Burak Yahya Kadem1Emman J. Mohammad2Abbas Jassim Atiyah3University of BabylonAl-Karkh University of ScienceUniversity of BabylonUniversity of BabylonThe synthesis of new substituted cobalt Phthalocyanine (CoPc) was carried out using starting materials Naphthalene-1,4,5, tetracarbonic acid dianhydride (NDI) employing dry process method. Metal oxides (MO) alloy of (60%Ni3O4 40%-Co3O4 ) have been functionalized with multiwall carbon nanotubes (F-MWCNTs) to produce (F-MWCNTs/MO) nanocomposite (E2) and mixed with CoPc to yield (F-MWCNT/CoPc/MO) (E3). These composites were investigated using different analytical and spectrophotometric methods such as 1H-NMR (0-18 ppm), FTIR spectroscopy in the range of (400-4000cm-1), powder X-rays diffraction (PXRD, 2θ o = 10-80), Raman spectroscopy (0-4000 cm-1), and UV-Visible spectrophotometry (0-800 nm). Then the activity of these materials was investigated as a gas sensing of (Ammonia, Methanol and Acetone). For each case, 0.2 mg/.mL of the prepared Copc, Copc/MWCNT, Copc/MWCNTs–MO was dispersed in 1m of ammonia, methanol and acetone at 298K. The surface morphology of the prepared materials was heterogeneous.https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/5073MWCNTs; Cobalt phthalocynanine; nanocomposite; gas sensing |
| spellingShingle | Mohanad Mousa Kareem Burak Yahya Kadem Emman J. Mohammad Abbas Jassim Atiyah Synthesis, Characterization and Gas Sensor Application of New Composite Based on MWCNTs:CoPc:Metal Oxide مجلة بغداد للعلوم MWCNTs; Cobalt phthalocynanine; nanocomposite; gas sensing |
| title | Synthesis, Characterization and Gas Sensor Application of New Composite Based on MWCNTs:CoPc:Metal Oxide |
| title_full | Synthesis, Characterization and Gas Sensor Application of New Composite Based on MWCNTs:CoPc:Metal Oxide |
| title_fullStr | Synthesis, Characterization and Gas Sensor Application of New Composite Based on MWCNTs:CoPc:Metal Oxide |
| title_full_unstemmed | Synthesis, Characterization and Gas Sensor Application of New Composite Based on MWCNTs:CoPc:Metal Oxide |
| title_short | Synthesis, Characterization and Gas Sensor Application of New Composite Based on MWCNTs:CoPc:Metal Oxide |
| title_sort | synthesis characterization and gas sensor application of new composite based on mwcnts copc metal oxide |
| topic | MWCNTs; Cobalt phthalocynanine; nanocomposite; gas sensing |
| url | https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/5073 |
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