PREPARATION OF B-T-S SEMICONDUCTORS BY USING SOLID STATE REACTION AND STUDYING ITS STRUCTURAL AND PHYSICAL PROPERTIES

In this study, the ceramic compound BaTi(1-x)SnxO3 was prepared at (x=0, 0.05, 0.1, 0.15, 0.2) and doped with SiO2 and Y2O3 for all concentrations by using solid state reaction at 1150 oC and sintering time of 6h. Structural properties were studied before and after adding SiO2 and Y2O3 by using X-r...

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Main Authors: Ali Fuad Khairy, Khalid Hamdi Rzej, Abdul Hameed Mahdi Al-Saraf
Format: Article
Language:English
Published: Tikrit University 2023-02-01
Series:Tikrit Journal of Pure Science
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Online Access:https://tjpsj.org/index.php/tjps/article/view/1066
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author Ali Fuad Khairy
Khalid Hamdi Rzej
Abdul Hameed Mahdi Al-Saraf
author_facet Ali Fuad Khairy
Khalid Hamdi Rzej
Abdul Hameed Mahdi Al-Saraf
author_sort Ali Fuad Khairy
collection DOAJ
description In this study, the ceramic compound BaTi(1-x)SnxO3 was prepared at (x=0, 0.05, 0.1, 0.15, 0.2) and doped with SiO2 and Y2O3 for all concentrations by using solid state reaction at 1150 oC and sintering time of 6h. Structural properties were studied before and after adding SiO2 and Y2O3 by using X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and Energy dispersive X-ray (EDX). It is found that the compound BaTi(1-x)SnxO3 has tetragonal structure for all concentration except at (x=0.2) which has cubic structure. After adding SiO2 and Y2O3, the peaks height was increased especially at (110). Physical properties were studied before and after adding SiO2 and Y2O3 by measuring density, porosity and absorbency. It is found that the density was increased while the porosity and absorbency were decreased as concentration increased. The electrical properties were studied such as alternate electric conductivity, dielectric constant and dielectric loss coefficient. It is found that the alternate electric conductivity was increased as frequency increased and the highest value of dielectric constant at frequency (100 Hz) and (x=0.05) after adding SiO2 and Y2O3 was (0.301). It is clear that the adding of SiO2 and Y2O3 enhanced the dielectric properties of  BaTi(1-x)SnxO3.  
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spelling doaj-art-cd0139554b3f4ff4b9c49ccb0fc8d5e62025-08-20T02:36:31ZengTikrit UniversityTikrit Journal of Pure Science1813-16622415-17262023-02-0121410.25130/tjps.v21i4.1066PREPARATION OF B-T-S SEMICONDUCTORS BY USING SOLID STATE REACTION AND STUDYING ITS STRUCTURAL AND PHYSICAL PROPERTIESAli Fuad KhairyKhalid Hamdi RzejAbdul Hameed Mahdi Al-Saraf In this study, the ceramic compound BaTi(1-x)SnxO3 was prepared at (x=0, 0.05, 0.1, 0.15, 0.2) and doped with SiO2 and Y2O3 for all concentrations by using solid state reaction at 1150 oC and sintering time of 6h. Structural properties were studied before and after adding SiO2 and Y2O3 by using X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and Energy dispersive X-ray (EDX). It is found that the compound BaTi(1-x)SnxO3 has tetragonal structure for all concentration except at (x=0.2) which has cubic structure. After adding SiO2 and Y2O3, the peaks height was increased especially at (110). Physical properties were studied before and after adding SiO2 and Y2O3 by measuring density, porosity and absorbency. It is found that the density was increased while the porosity and absorbency were decreased as concentration increased. The electrical properties were studied such as alternate electric conductivity, dielectric constant and dielectric loss coefficient. It is found that the alternate electric conductivity was increased as frequency increased and the highest value of dielectric constant at frequency (100 Hz) and (x=0.05) after adding SiO2 and Y2O3 was (0.301). It is clear that the adding of SiO2 and Y2O3 enhanced the dielectric properties of  BaTi(1-x)SnxO3.   https://tjpsj.org/index.php/tjps/article/view/1066B-T-S SEMICONDUCTORSSTATE REACTIONPHYSICAL PROPERTIES
spellingShingle Ali Fuad Khairy
Khalid Hamdi Rzej
Abdul Hameed Mahdi Al-Saraf
PREPARATION OF B-T-S SEMICONDUCTORS BY USING SOLID STATE REACTION AND STUDYING ITS STRUCTURAL AND PHYSICAL PROPERTIES
Tikrit Journal of Pure Science
B-T-S SEMICONDUCTORS
STATE REACTION
PHYSICAL PROPERTIES
title PREPARATION OF B-T-S SEMICONDUCTORS BY USING SOLID STATE REACTION AND STUDYING ITS STRUCTURAL AND PHYSICAL PROPERTIES
title_full PREPARATION OF B-T-S SEMICONDUCTORS BY USING SOLID STATE REACTION AND STUDYING ITS STRUCTURAL AND PHYSICAL PROPERTIES
title_fullStr PREPARATION OF B-T-S SEMICONDUCTORS BY USING SOLID STATE REACTION AND STUDYING ITS STRUCTURAL AND PHYSICAL PROPERTIES
title_full_unstemmed PREPARATION OF B-T-S SEMICONDUCTORS BY USING SOLID STATE REACTION AND STUDYING ITS STRUCTURAL AND PHYSICAL PROPERTIES
title_short PREPARATION OF B-T-S SEMICONDUCTORS BY USING SOLID STATE REACTION AND STUDYING ITS STRUCTURAL AND PHYSICAL PROPERTIES
title_sort preparation of b t s semiconductors by using solid state reaction and studying its structural and physical properties
topic B-T-S SEMICONDUCTORS
STATE REACTION
PHYSICAL PROPERTIES
url https://tjpsj.org/index.php/tjps/article/view/1066
work_keys_str_mv AT alifuadkhairy preparationofbtssemiconductorsbyusingsolidstatereactionandstudyingitsstructuralandphysicalproperties
AT khalidhamdirzej preparationofbtssemiconductorsbyusingsolidstatereactionandstudyingitsstructuralandphysicalproperties
AT abdulhameedmahdialsaraf preparationofbtssemiconductorsbyusingsolidstatereactionandstudyingitsstructuralandphysicalproperties