Comprehensive Study of the Gas Volume and Composition Produced by Different 3–230 Ah Lithium Iron Phosphate (LFP) Cells Failed Using External Heat, Overcharge and Nail Penetration Under Air and Inert Atmospheres

This paper reports on the failure of cells with lithium iron phosphate (LFP) chemistry tested under a range of conditions to understand their effect on the volume and composition of gas generated. Cells of the following formats, 26,650, pouch, and prismatic, and capacities ranging from 3 to 230 Ah,...

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Main Authors: Gemma E. Howard, Jonathan E. H. Buston, Jason Gill, Steven L. Goddard, Jack W. Mellor, Philip A. P. Reeve
Format: Article
Language:English
Published: MDPI AG 2025-07-01
Series:Batteries
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Online Access:https://www.mdpi.com/2313-0105/11/7/267
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author Gemma E. Howard
Jonathan E. H. Buston
Jason Gill
Steven L. Goddard
Jack W. Mellor
Philip A. P. Reeve
author_facet Gemma E. Howard
Jonathan E. H. Buston
Jason Gill
Steven L. Goddard
Jack W. Mellor
Philip A. P. Reeve
author_sort Gemma E. Howard
collection DOAJ
description This paper reports on the failure of cells with lithium iron phosphate (LFP) chemistry tested under a range of conditions to understand their effect on the volume and composition of gas generated. Cells of the following formats, 26,650, pouch, and prismatic, and capacities ranging from 3 to 230 Ah, were subjected to external heat, overcharge, and nail penetration tests. Gas volume was calculated, and the following gases analysed: H<sub>2</sub>, CO<sub>2</sub>, CO, CH<sub>4</sub>, C<sub>2</sub>H<sub>4</sub>, C<sub>2</sub>H<sub>6</sub>, C<sub>3</sub>H<sub>6</sub>, and C<sub>3</sub>H<sub>8</sub>. Cells that failed via external heating under inert conditions (N<sub>2</sub> or Ar atmosphere) at 100% state of charge (SoC) typically generated 0.7 L/Ah of gas; overcharged cells, 0.11–0.68 L/Ah; and nail penetration between 0.3 and 0.5 L/Ah. In general, for all test configurations, regardless of atmosphere, the total gas volume contained a 40% concentration of H<sub>2</sub>, 15% of CO<sub>2</sub>, and the remaining gas consisted of varying concentrations of CO and flammable hydrocarbons. This demonstrates that despite differences in gas volume, the failure gas composition of LFP cells remains similar.
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institution Kabale University
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publishDate 2025-07-01
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spelling doaj-art-cbb5e49fd49647ad8f730baba3a6930e2025-08-20T03:58:31ZengMDPI AGBatteries2313-01052025-07-0111726710.3390/batteries11070267Comprehensive Study of the Gas Volume and Composition Produced by Different 3–230 Ah Lithium Iron Phosphate (LFP) Cells Failed Using External Heat, Overcharge and Nail Penetration Under Air and Inert AtmospheresGemma E. Howard0Jonathan E. H. Buston1Jason Gill2Steven L. Goddard3Jack W. Mellor4Philip A. P. Reeve5HSE Science and Research Centre, Harpur Hill, Buxton Derbyshire SK17 9JN, UKHSE Science and Research Centre, Harpur Hill, Buxton Derbyshire SK17 9JN, UKHSE Science and Research Centre, Harpur Hill, Buxton Derbyshire SK17 9JN, UKHSE Science and Research Centre, Harpur Hill, Buxton Derbyshire SK17 9JN, UKHSE Science and Research Centre, Harpur Hill, Buxton Derbyshire SK17 9JN, UKHSE Science and Research Centre, Harpur Hill, Buxton Derbyshire SK17 9JN, UKThis paper reports on the failure of cells with lithium iron phosphate (LFP) chemistry tested under a range of conditions to understand their effect on the volume and composition of gas generated. Cells of the following formats, 26,650, pouch, and prismatic, and capacities ranging from 3 to 230 Ah, were subjected to external heat, overcharge, and nail penetration tests. Gas volume was calculated, and the following gases analysed: H<sub>2</sub>, CO<sub>2</sub>, CO, CH<sub>4</sub>, C<sub>2</sub>H<sub>4</sub>, C<sub>2</sub>H<sub>6</sub>, C<sub>3</sub>H<sub>6</sub>, and C<sub>3</sub>H<sub>8</sub>. Cells that failed via external heating under inert conditions (N<sub>2</sub> or Ar atmosphere) at 100% state of charge (SoC) typically generated 0.7 L/Ah of gas; overcharged cells, 0.11–0.68 L/Ah; and nail penetration between 0.3 and 0.5 L/Ah. In general, for all test configurations, regardless of atmosphere, the total gas volume contained a 40% concentration of H<sub>2</sub>, 15% of CO<sub>2</sub>, and the remaining gas consisted of varying concentrations of CO and flammable hydrocarbons. This demonstrates that despite differences in gas volume, the failure gas composition of LFP cells remains similar.https://www.mdpi.com/2313-0105/11/7/267Li-ionlithium iron phosphate (LFP)gas analysisgas volume22,650pouch cell
spellingShingle Gemma E. Howard
Jonathan E. H. Buston
Jason Gill
Steven L. Goddard
Jack W. Mellor
Philip A. P. Reeve
Comprehensive Study of the Gas Volume and Composition Produced by Different 3–230 Ah Lithium Iron Phosphate (LFP) Cells Failed Using External Heat, Overcharge and Nail Penetration Under Air and Inert Atmospheres
Batteries
Li-ion
lithium iron phosphate (LFP)
gas analysis
gas volume
22,650
pouch cell
title Comprehensive Study of the Gas Volume and Composition Produced by Different 3–230 Ah Lithium Iron Phosphate (LFP) Cells Failed Using External Heat, Overcharge and Nail Penetration Under Air and Inert Atmospheres
title_full Comprehensive Study of the Gas Volume and Composition Produced by Different 3–230 Ah Lithium Iron Phosphate (LFP) Cells Failed Using External Heat, Overcharge and Nail Penetration Under Air and Inert Atmospheres
title_fullStr Comprehensive Study of the Gas Volume and Composition Produced by Different 3–230 Ah Lithium Iron Phosphate (LFP) Cells Failed Using External Heat, Overcharge and Nail Penetration Under Air and Inert Atmospheres
title_full_unstemmed Comprehensive Study of the Gas Volume and Composition Produced by Different 3–230 Ah Lithium Iron Phosphate (LFP) Cells Failed Using External Heat, Overcharge and Nail Penetration Under Air and Inert Atmospheres
title_short Comprehensive Study of the Gas Volume and Composition Produced by Different 3–230 Ah Lithium Iron Phosphate (LFP) Cells Failed Using External Heat, Overcharge and Nail Penetration Under Air and Inert Atmospheres
title_sort comprehensive study of the gas volume and composition produced by different 3 230 ah lithium iron phosphate lfp cells failed using external heat overcharge and nail penetration under air and inert atmospheres
topic Li-ion
lithium iron phosphate (LFP)
gas analysis
gas volume
22,650
pouch cell
url https://www.mdpi.com/2313-0105/11/7/267
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