Influence of carbonate apatite (CAp) addition on Mg-5Al-3Sn composites for potential biodegradable implant applications: A study of powder metallurgy combined with hot extrusion

Mg-5Al-3Sn alloy composites reinforced with carbonate apatite (CAp) have been successfully fabricated using the powder metallurgy method assisted by hot extrusion to find potential materials for biodegradable implant applications. Further tests such as corrosion, cytotoxicity, and others are still n...

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Main Authors: Sri Endah Susilowati, Fahamsyah Hamdan Latief, Iwan Setyadi, Didit Sumardiyanto, Suryadi Suryadi, I Nyoman Jujur, Mirza Wibisono
Format: Article
Language:English
Published: Elsevier 2025-03-01
Series:Results in Engineering
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Online Access:http://www.sciencedirect.com/science/article/pii/S2590123025005791
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author Sri Endah Susilowati
Fahamsyah Hamdan Latief
Iwan Setyadi
Didit Sumardiyanto
Suryadi Suryadi
I Nyoman Jujur
Mirza Wibisono
author_facet Sri Endah Susilowati
Fahamsyah Hamdan Latief
Iwan Setyadi
Didit Sumardiyanto
Suryadi Suryadi
I Nyoman Jujur
Mirza Wibisono
author_sort Sri Endah Susilowati
collection DOAJ
description Mg-5Al-3Sn alloy composites reinforced with carbonate apatite (CAp) have been successfully fabricated using the powder metallurgy method assisted by hot extrusion to find potential materials for biodegradable implant applications. Further tests such as corrosion, cytotoxicity, and others are still needed to evaluate the biocompatibility of the developed composites. The present results showed an increase in the maximum compressive strength of the composites by about 9 % for Mg-5Al-3Sn-1%CAp and 8 % for Mg-5Al-3Sn-2%CAp. Similarly, the average hardness of the composite with 1 % CAp increased slightly by 1.63 %, while that of the composite with 2 % CAp increased drastically by 33.4 %. Some factors contribute to the improvement of the mechanical properties of the composites. These include the hot extrusion process, which influences grain reduction; the precipitation of Mg17Al12 and Mg2Sn intermetallic phases along the grain boundaries; and the dispersion effect of CAp in the Mg-5Al-Sn alloy matrix. Generally, those factors restrict the dislocations' movement, thereby enhancing the compressive strength and hardness of Mg-5Al-3Sn/CAp composites.
format Article
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issn 2590-1230
language English
publishDate 2025-03-01
publisher Elsevier
record_format Article
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spelling doaj-art-cb8434eba9014479ad4201e9bfb48c7c2025-08-20T03:16:34ZengElsevierResults in Engineering2590-12302025-03-012510450210.1016/j.rineng.2025.104502Influence of carbonate apatite (CAp) addition on Mg-5Al-3Sn composites for potential biodegradable implant applications: A study of powder metallurgy combined with hot extrusionSri Endah Susilowati0Fahamsyah Hamdan Latief1Iwan Setyadi2Didit Sumardiyanto3Suryadi Suryadi4I Nyoman Jujur5Mirza Wibisono6Department of Mechanical Engineering, Faculty of Engineering and Informatics, Universitas 17 Agustus 1945, Jakarta,14350, Indonesia; Corresponding authors.Department of Mechanical Engineering, Faculty of Engineering and Science, Universitas Nasional, Jakarta, 12520, Indonesia; Corresponding authors.Research Center of Advanced Materials, National Research and Innovation Agency (BRIN), Puspiptek Area, South Tangerang, Banten, 15314, IndonesiaDepartment of Mechanical Engineering, Faculty of Engineering and Informatics, Universitas 17 Agustus 1945, Jakarta,14350, IndonesiaResearch Center of Advanced Materials, National Research and Innovation Agency (BRIN), Puspiptek Area, South Tangerang, Banten, 15314, IndonesiaResearch Center of Advanced Materials, National Research and Innovation Agency (BRIN), Puspiptek Area, South Tangerang, Banten, 15314, IndonesiaResearch Center of Advanced Materials, National Research and Innovation Agency (BRIN), Puspiptek Area, South Tangerang, Banten, 15314, IndonesiaMg-5Al-3Sn alloy composites reinforced with carbonate apatite (CAp) have been successfully fabricated using the powder metallurgy method assisted by hot extrusion to find potential materials for biodegradable implant applications. Further tests such as corrosion, cytotoxicity, and others are still needed to evaluate the biocompatibility of the developed composites. The present results showed an increase in the maximum compressive strength of the composites by about 9 % for Mg-5Al-3Sn-1%CAp and 8 % for Mg-5Al-3Sn-2%CAp. Similarly, the average hardness of the composite with 1 % CAp increased slightly by 1.63 %, while that of the composite with 2 % CAp increased drastically by 33.4 %. Some factors contribute to the improvement of the mechanical properties of the composites. These include the hot extrusion process, which influences grain reduction; the precipitation of Mg17Al12 and Mg2Sn intermetallic phases along the grain boundaries; and the dispersion effect of CAp in the Mg-5Al-Sn alloy matrix. Generally, those factors restrict the dislocations' movement, thereby enhancing the compressive strength and hardness of Mg-5Al-3Sn/CAp composites.http://www.sciencedirect.com/science/article/pii/S2590123025005791Mg-based compositesMechanical propertiesMicrostructureXRDBiodegradable implants
spellingShingle Sri Endah Susilowati
Fahamsyah Hamdan Latief
Iwan Setyadi
Didit Sumardiyanto
Suryadi Suryadi
I Nyoman Jujur
Mirza Wibisono
Influence of carbonate apatite (CAp) addition on Mg-5Al-3Sn composites for potential biodegradable implant applications: A study of powder metallurgy combined with hot extrusion
Results in Engineering
Mg-based composites
Mechanical properties
Microstructure
XRD
Biodegradable implants
title Influence of carbonate apatite (CAp) addition on Mg-5Al-3Sn composites for potential biodegradable implant applications: A study of powder metallurgy combined with hot extrusion
title_full Influence of carbonate apatite (CAp) addition on Mg-5Al-3Sn composites for potential biodegradable implant applications: A study of powder metallurgy combined with hot extrusion
title_fullStr Influence of carbonate apatite (CAp) addition on Mg-5Al-3Sn composites for potential biodegradable implant applications: A study of powder metallurgy combined with hot extrusion
title_full_unstemmed Influence of carbonate apatite (CAp) addition on Mg-5Al-3Sn composites for potential biodegradable implant applications: A study of powder metallurgy combined with hot extrusion
title_short Influence of carbonate apatite (CAp) addition on Mg-5Al-3Sn composites for potential biodegradable implant applications: A study of powder metallurgy combined with hot extrusion
title_sort influence of carbonate apatite cap addition on mg 5al 3sn composites for potential biodegradable implant applications a study of powder metallurgy combined with hot extrusion
topic Mg-based composites
Mechanical properties
Microstructure
XRD
Biodegradable implants
url http://www.sciencedirect.com/science/article/pii/S2590123025005791
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