Effect of Surface Treatments on the Repair of a Hybrid Ceramic through the Microtensile Test

Abstract This study evaluated the microtensile bond strength between a hybrid ceramic and a composite resin under different surface treatments and aging. Hybrid ceramic blocks were divided into five groups based on surface treatment and thermocycling: HF: 5% hydrofluoric acid; HFS: hydrofluoric acid...

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Main Authors: Cristiane Mayumi Inagati, Jonas V. M. Rodrigues, Manassés T. V. Grangeiro, Natália R. Rossi, Lilian C. Anami, Guilherme de S. F. A. Saavedra, Rodrigo O. de Assunção e Souza, Renata M. de M. Marinho
Format: Article
Language:English
Published: Associação Brasileira de Cerâmica 2025-03-01
Series:Cerâmica
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Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132025000100306&lng=en&tlng=en
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author Cristiane Mayumi Inagati
Jonas V. M. Rodrigues
Manassés T. V. Grangeiro
Natália R. Rossi
Lilian C. Anami
Guilherme de S. F. A. Saavedra
Rodrigo O. de Assunção e Souza
Renata M. de M. Marinho
author_facet Cristiane Mayumi Inagati
Jonas V. M. Rodrigues
Manassés T. V. Grangeiro
Natália R. Rossi
Lilian C. Anami
Guilherme de S. F. A. Saavedra
Rodrigo O. de Assunção e Souza
Renata M. de M. Marinho
author_sort Cristiane Mayumi Inagati
collection DOAJ
description Abstract This study evaluated the microtensile bond strength between a hybrid ceramic and a composite resin under different surface treatments and aging. Hybrid ceramic blocks were divided into five groups based on surface treatment and thermocycling: HF: 5% hydrofluoric acid; HFS: hydrofluoric acid and silane; A110S: sandblasting with aluminum oxide and silicatization; A50: aluminum oxide particle blasting; R: roughening. All samples were cemented to composite resin. After 24-hour storage in distilled water at 37ºC, the blocks were cut into sticks and tested immediately or after 10,000 cycles. Microtensile bond strength was tested using a universal testing machine. Failure modes were visualized and classified as cohesive, adhesive, and predominantly adhesive. Statistical differences were found between groups for surface treatment and thermocycling (p<0.05). Hybrid ceramics showed higher bond strength when etched with hydrofluoric acid and silanized, but bond strength decreased after thermocycling in all groups.
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publishDate 2025-03-01
publisher Associação Brasileira de Cerâmica
record_format Article
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spelling doaj-art-cb2c68b1d9424812a5b15b3e42e4e4e42025-08-20T02:26:01ZengAssociação Brasileira de CerâmicaCerâmica1678-45532025-03-017110.1590/vaab72881Effect of Surface Treatments on the Repair of a Hybrid Ceramic through the Microtensile TestCristiane Mayumi Inagatihttps://orcid.org/0000-0003-1758-1924Jonas V. M. RodriguesManassés T. V. GrangeiroNatália R. RossiLilian C. AnamiGuilherme de S. F. A. SaavedraRodrigo O. de Assunção e SouzaRenata M. de M. MarinhoAbstract This study evaluated the microtensile bond strength between a hybrid ceramic and a composite resin under different surface treatments and aging. Hybrid ceramic blocks were divided into five groups based on surface treatment and thermocycling: HF: 5% hydrofluoric acid; HFS: hydrofluoric acid and silane; A110S: sandblasting with aluminum oxide and silicatization; A50: aluminum oxide particle blasting; R: roughening. All samples were cemented to composite resin. After 24-hour storage in distilled water at 37ºC, the blocks were cut into sticks and tested immediately or after 10,000 cycles. Microtensile bond strength was tested using a universal testing machine. Failure modes were visualized and classified as cohesive, adhesive, and predominantly adhesive. Statistical differences were found between groups for surface treatment and thermocycling (p<0.05). Hybrid ceramics showed higher bond strength when etched with hydrofluoric acid and silanized, but bond strength decreased after thermocycling in all groups.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132025000100306&lng=en&tlng=enadhesioncomposite resinshybrid ceramicmicrotensile bond strengthsurface treatment
spellingShingle Cristiane Mayumi Inagati
Jonas V. M. Rodrigues
Manassés T. V. Grangeiro
Natália R. Rossi
Lilian C. Anami
Guilherme de S. F. A. Saavedra
Rodrigo O. de Assunção e Souza
Renata M. de M. Marinho
Effect of Surface Treatments on the Repair of a Hybrid Ceramic through the Microtensile Test
Cerâmica
adhesion
composite resins
hybrid ceramic
microtensile bond strength
surface treatment
title Effect of Surface Treatments on the Repair of a Hybrid Ceramic through the Microtensile Test
title_full Effect of Surface Treatments on the Repair of a Hybrid Ceramic through the Microtensile Test
title_fullStr Effect of Surface Treatments on the Repair of a Hybrid Ceramic through the Microtensile Test
title_full_unstemmed Effect of Surface Treatments on the Repair of a Hybrid Ceramic through the Microtensile Test
title_short Effect of Surface Treatments on the Repair of a Hybrid Ceramic through the Microtensile Test
title_sort effect of surface treatments on the repair of a hybrid ceramic through the microtensile test
topic adhesion
composite resins
hybrid ceramic
microtensile bond strength
surface treatment
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132025000100306&lng=en&tlng=en
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