Study on properties of pre-alloy powder of TiNiHf high temperature shape memory alloy for additive manufacturing by preheating treatment

In this work, pre-alloyed powder high-temperature shape memory alloy (Ti30Ni50Hf20) for additive manufacturing was preheated at 300–800 °C and thermoscycled at 650 °C to examine the influence of preheating temperature and thermal cycle number on the phase composition and phase transformation behavio...

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Main Authors: M.C. Jiang, X.Y. Yang, M.C. Zhang, D.C. Ren, H.F. Nurly, Y. Liu, Y.S. Cai, H.B. Ji, J.F. Lei
Format: Article
Language:English
Published: Elsevier 2024-11-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785424024384
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author M.C. Jiang
X.Y. Yang
M.C. Zhang
D.C. Ren
H.F. Nurly
Y. Liu
Y.S. Cai
H.B. Ji
J.F. Lei
author_facet M.C. Jiang
X.Y. Yang
M.C. Zhang
D.C. Ren
H.F. Nurly
Y. Liu
Y.S. Cai
H.B. Ji
J.F. Lei
author_sort M.C. Jiang
collection DOAJ
description In this work, pre-alloyed powder high-temperature shape memory alloy (Ti30Ni50Hf20) for additive manufacturing was preheated at 300–800 °C and thermoscycled at 650 °C to examine the influence of preheating temperature and thermal cycle number on the phase composition and phase transformation behavior. The results showed that the H phase precipitation occurred in the matrix with the rising preheating temperature within 300–600 °C, and the phase transformation temperature of the pre-alloyed powders also increased. When the preheating temperature exceeded 600 °C, the H phase dissolved back into the matrix, and the phase transformation temperature decreased. A total of 50 thermal cycles were conducted on the pre-alloyed powders at 650 °C, and the phase transformation temperature and phase composition remained stable after cycling. It can be concluded that the preheating temperature greatly affected the phase composition and phase transformation behavior of Ti30Ni50Hf20 high-temperature shape memory alloy pre-alloyed powders, while the number of thermal cycles delivered a minor effect.
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issn 2238-7854
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publisher Elsevier
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series Journal of Materials Research and Technology
spelling doaj-art-cae4c260dddf476fbed8708611dbc5ea2025-08-20T02:39:03ZengElsevierJournal of Materials Research and Technology2238-78542024-11-01336422643310.1016/j.jmrt.2024.10.168Study on properties of pre-alloy powder of TiNiHf high temperature shape memory alloy for additive manufacturing by preheating treatmentM.C. Jiang0X.Y. Yang1M.C. Zhang2D.C. Ren3H.F. Nurly4Y. Liu5Y.S. Cai6H.B. Ji7J.F. Lei8School of Materials Science and Engineering, University of Science and Technology of China, Shenyang, 110016, China; Shi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaSchool of Materials Science and Engineering, University of Science and Technology of China, Shenyang, 110016, China; Shi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaSchool of Materials Science and Engineering, University of Science and Technology of China, Shenyang, 110016, China; Shi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, China; Corresponding author.Shi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, China; Corresponding author.Shi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, China; Corresponding author.Shi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaIn this work, pre-alloyed powder high-temperature shape memory alloy (Ti30Ni50Hf20) for additive manufacturing was preheated at 300–800 °C and thermoscycled at 650 °C to examine the influence of preheating temperature and thermal cycle number on the phase composition and phase transformation behavior. The results showed that the H phase precipitation occurred in the matrix with the rising preheating temperature within 300–600 °C, and the phase transformation temperature of the pre-alloyed powders also increased. When the preheating temperature exceeded 600 °C, the H phase dissolved back into the matrix, and the phase transformation temperature decreased. A total of 50 thermal cycles were conducted on the pre-alloyed powders at 650 °C, and the phase transformation temperature and phase composition remained stable after cycling. It can be concluded that the preheating temperature greatly affected the phase composition and phase transformation behavior of Ti30Ni50Hf20 high-temperature shape memory alloy pre-alloyed powders, while the number of thermal cycles delivered a minor effect.http://www.sciencedirect.com/science/article/pii/S2238785424024384TiNiHf high-temperature shape memory alloyPre-alloyed powderAdditive manufacturingHeat treatmentPhase transformation behavior
spellingShingle M.C. Jiang
X.Y. Yang
M.C. Zhang
D.C. Ren
H.F. Nurly
Y. Liu
Y.S. Cai
H.B. Ji
J.F. Lei
Study on properties of pre-alloy powder of TiNiHf high temperature shape memory alloy for additive manufacturing by preheating treatment
Journal of Materials Research and Technology
TiNiHf high-temperature shape memory alloy
Pre-alloyed powder
Additive manufacturing
Heat treatment
Phase transformation behavior
title Study on properties of pre-alloy powder of TiNiHf high temperature shape memory alloy for additive manufacturing by preheating treatment
title_full Study on properties of pre-alloy powder of TiNiHf high temperature shape memory alloy for additive manufacturing by preheating treatment
title_fullStr Study on properties of pre-alloy powder of TiNiHf high temperature shape memory alloy for additive manufacturing by preheating treatment
title_full_unstemmed Study on properties of pre-alloy powder of TiNiHf high temperature shape memory alloy for additive manufacturing by preheating treatment
title_short Study on properties of pre-alloy powder of TiNiHf high temperature shape memory alloy for additive manufacturing by preheating treatment
title_sort study on properties of pre alloy powder of tinihf high temperature shape memory alloy for additive manufacturing by preheating treatment
topic TiNiHf high-temperature shape memory alloy
Pre-alloyed powder
Additive manufacturing
Heat treatment
Phase transformation behavior
url http://www.sciencedirect.com/science/article/pii/S2238785424024384
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