Microstructure and mechanical properties of an oxide-dispersed ultrafine-grained maraging steel

A novel oxide-dispersed strengthened T250 maraging steel (ODS-T250 steel) was prepared by mechanical ball milling followed by hot isostatic pressing. Martensitic transformation behavior, ultrafine-grained martensite microstructure and tensile properties of the ODS-T250 steel were compared to its oxi...

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Main Authors: Bowen Shi, Tianyi Zeng, Nairong Tao, Xianbo Shi, Jiarong Zhang, Wei Wang, Sybrand van der Zwaag, Yiyin Shan, Wei Yan
Format: Article
Language:English
Published: Elsevier 2025-07-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425016382
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author Bowen Shi
Tianyi Zeng
Nairong Tao
Xianbo Shi
Jiarong Zhang
Wei Wang
Sybrand van der Zwaag
Yiyin Shan
Wei Yan
author_facet Bowen Shi
Tianyi Zeng
Nairong Tao
Xianbo Shi
Jiarong Zhang
Wei Wang
Sybrand van der Zwaag
Yiyin Shan
Wei Yan
author_sort Bowen Shi
collection DOAJ
description A novel oxide-dispersed strengthened T250 maraging steel (ODS-T250 steel) was prepared by mechanical ball milling followed by hot isostatic pressing. Martensitic transformation behavior, ultrafine-grained martensite microstructure and tensile properties of the ODS-T250 steel were compared to its oxide-free counterpart (T250 steel). The results indicated that ODS-T250 steel exhibited excellent microstructural thermal stability, maintaining an effective grain size of 0.348 μm even after quenching from 1200 °C, whereas T250 steel exhibited a much larger grain size of 5.473 μm. After quenching, the ODS-T250 steel showed significantly distinct variant selectivity, and its martensite morphology was unprecedented equiaxed structure rather than typical lath-type. Statistical analysis revealed that there was only a single variant formed when the prior austenite grain size (PAGS) was below 0.43 μm. Moreover, the martensite start (Ms) temperature of ODS-T250 steel was lower than the T250 steel due to its ultrafine PAGS and the dispersed oxide particles. The refinement of PAGS and the presence of oxide particles led to a simultaneous improvement in both strength and ductility of ODS-T250 steel.
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publishDate 2025-07-01
publisher Elsevier
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series Journal of Materials Research and Technology
spelling doaj-art-cab78be795d04f9caa60ec3a3124cd3d2025-08-20T03:31:28ZengElsevierJournal of Materials Research and Technology2238-78542025-07-01373075308810.1016/j.jmrt.2025.06.216Microstructure and mechanical properties of an oxide-dispersed ultrafine-grained maraging steelBowen Shi0Tianyi Zeng1Nairong Tao2Xianbo Shi3Jiarong Zhang4Wei Wang5Sybrand van der Zwaag6Yiyin Shan7Wei Yan8School of Materials Science and Engineering, Northeastern University, Shenyang, 110819, China; Shi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaSchool of Packaging and Materials Engineering, Hunan University of Technology, Zhuzhou, 412007, ChinaShenyang National Laboratory of Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaFaculty of Aerospace Engineering, Delft University of Technology, Delft, NetherlandsShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, China; Corresponding author. Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, China.A novel oxide-dispersed strengthened T250 maraging steel (ODS-T250 steel) was prepared by mechanical ball milling followed by hot isostatic pressing. Martensitic transformation behavior, ultrafine-grained martensite microstructure and tensile properties of the ODS-T250 steel were compared to its oxide-free counterpart (T250 steel). The results indicated that ODS-T250 steel exhibited excellent microstructural thermal stability, maintaining an effective grain size of 0.348 μm even after quenching from 1200 °C, whereas T250 steel exhibited a much larger grain size of 5.473 μm. After quenching, the ODS-T250 steel showed significantly distinct variant selectivity, and its martensite morphology was unprecedented equiaxed structure rather than typical lath-type. Statistical analysis revealed that there was only a single variant formed when the prior austenite grain size (PAGS) was below 0.43 μm. Moreover, the martensite start (Ms) temperature of ODS-T250 steel was lower than the T250 steel due to its ultrafine PAGS and the dispersed oxide particles. The refinement of PAGS and the presence of oxide particles led to a simultaneous improvement in both strength and ductility of ODS-T250 steel.http://www.sciencedirect.com/science/article/pii/S2238785425016382Maraging steelUltrafine grainsNano-oxidesVariant selectionMartensitic transformation
spellingShingle Bowen Shi
Tianyi Zeng
Nairong Tao
Xianbo Shi
Jiarong Zhang
Wei Wang
Sybrand van der Zwaag
Yiyin Shan
Wei Yan
Microstructure and mechanical properties of an oxide-dispersed ultrafine-grained maraging steel
Journal of Materials Research and Technology
Maraging steel
Ultrafine grains
Nano-oxides
Variant selection
Martensitic transformation
title Microstructure and mechanical properties of an oxide-dispersed ultrafine-grained maraging steel
title_full Microstructure and mechanical properties of an oxide-dispersed ultrafine-grained maraging steel
title_fullStr Microstructure and mechanical properties of an oxide-dispersed ultrafine-grained maraging steel
title_full_unstemmed Microstructure and mechanical properties of an oxide-dispersed ultrafine-grained maraging steel
title_short Microstructure and mechanical properties of an oxide-dispersed ultrafine-grained maraging steel
title_sort microstructure and mechanical properties of an oxide dispersed ultrafine grained maraging steel
topic Maraging steel
Ultrafine grains
Nano-oxides
Variant selection
Martensitic transformation
url http://www.sciencedirect.com/science/article/pii/S2238785425016382
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