A Comparative Study of the Effect of MgO and CaCO3 as Support Materials in the Synthesis of Carbon Nanotubes with Fe/Co as Catalyst

A comparative study of the effect of magnesium oxide and calcium carbonate as support material in the synthesis of carbon nanotubes using the catalyst Fe/Co is presented. The synthesized carbon nanotubes were characterized with Raman spectroscopy, scanning electron spectroscopy (SEM), high-resolutio...

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Main Authors: Ezekiel D. Dikio, Albert J. Kupeta, Force T. Thema
Format: Article
Language:English
Published: Wiley 2014-01-01
Series:Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2014/641823
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author Ezekiel D. Dikio
Albert J. Kupeta
Force T. Thema
author_facet Ezekiel D. Dikio
Albert J. Kupeta
Force T. Thema
author_sort Ezekiel D. Dikio
collection DOAJ
description A comparative study of the effect of magnesium oxide and calcium carbonate as support material in the synthesis of carbon nanotubes using the catalyst Fe/Co is presented. The synthesized carbon nanotubes were characterized with Raman spectroscopy, scanning electron spectroscopy (SEM), high-resolution transmission electron microscopy (HRTEM), X-ray diffraction spectroscopy (XRD), and energy dispersive spectroscopy (EDS). The morphology of the carbon nanotubes synthesized with magnesium oxide as support material gives rise to carbon nanotubes with consistent and well-defined structure unlike that synthesized with calcium carbonate. The ID/IG ratio of synthesized carbon nanotubes (CNTs) was 0.8544 for magnesium oxide supported compared to 0.8501 for calcium carbonate supported carbon nanotube.
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issn 2090-9063
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publishDate 2014-01-01
publisher Wiley
record_format Article
series Journal of Chemistry
spelling doaj-art-ca95dc4cfe8649dbb69eb0603240503e2025-02-03T01:12:13ZengWileyJournal of Chemistry2090-90632090-90712014-01-01201410.1155/2014/641823641823A Comparative Study of the Effect of MgO and CaCO3 as Support Materials in the Synthesis of Carbon Nanotubes with Fe/Co as CatalystEzekiel D. Dikio0Albert J. Kupeta1Force T. Thema2Applied Chemistry and Nanoscience Laboratory, Department of Chemistry, Vaal University of Technology, P.O. Box X012, Vanderbijlpark 1911, South AfricaApplied Chemistry and Nanoscience Laboratory, Department of Chemistry, Vaal University of Technology, P.O. Box X012, Vanderbijlpark 1911, South AfricaApplied Chemistry and Nanoscience Laboratory, Department of Chemistry, Vaal University of Technology, P.O. Box X012, Vanderbijlpark 1911, South AfricaA comparative study of the effect of magnesium oxide and calcium carbonate as support material in the synthesis of carbon nanotubes using the catalyst Fe/Co is presented. The synthesized carbon nanotubes were characterized with Raman spectroscopy, scanning electron spectroscopy (SEM), high-resolution transmission electron microscopy (HRTEM), X-ray diffraction spectroscopy (XRD), and energy dispersive spectroscopy (EDS). The morphology of the carbon nanotubes synthesized with magnesium oxide as support material gives rise to carbon nanotubes with consistent and well-defined structure unlike that synthesized with calcium carbonate. The ID/IG ratio of synthesized carbon nanotubes (CNTs) was 0.8544 for magnesium oxide supported compared to 0.8501 for calcium carbonate supported carbon nanotube.http://dx.doi.org/10.1155/2014/641823
spellingShingle Ezekiel D. Dikio
Albert J. Kupeta
Force T. Thema
A Comparative Study of the Effect of MgO and CaCO3 as Support Materials in the Synthesis of Carbon Nanotubes with Fe/Co as Catalyst
Journal of Chemistry
title A Comparative Study of the Effect of MgO and CaCO3 as Support Materials in the Synthesis of Carbon Nanotubes with Fe/Co as Catalyst
title_full A Comparative Study of the Effect of MgO and CaCO3 as Support Materials in the Synthesis of Carbon Nanotubes with Fe/Co as Catalyst
title_fullStr A Comparative Study of the Effect of MgO and CaCO3 as Support Materials in the Synthesis of Carbon Nanotubes with Fe/Co as Catalyst
title_full_unstemmed A Comparative Study of the Effect of MgO and CaCO3 as Support Materials in the Synthesis of Carbon Nanotubes with Fe/Co as Catalyst
title_short A Comparative Study of the Effect of MgO and CaCO3 as Support Materials in the Synthesis of Carbon Nanotubes with Fe/Co as Catalyst
title_sort comparative study of the effect of mgo and caco3 as support materials in the synthesis of carbon nanotubes with fe co as catalyst
url http://dx.doi.org/10.1155/2014/641823
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