Towards sustainable urea electro-oxidation: a thermodynamic and green chemistry evaluation of alternative pathways

This study presents a comparative thermodynamic analysis of various pathways for electrochemical hydrogen production coupled with the anodic oxidation of urea, offering a sustainable alternative to the conventional oxygen evolution reaction. For the first time, the feasibility and efficiency of thes...

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Main Author: Vyacheslav Protsenko
Format: Article
Language:English
Published: The Royal Society 2025-07-01
Series:Royal Society Open Science
Subjects:
Online Access:https://royalsocietypublishing.org/doi/10.1098/rsos.250156
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author Vyacheslav Protsenko
author_facet Vyacheslav Protsenko
author_sort Vyacheslav Protsenko
collection DOAJ
description This study presents a comparative thermodynamic analysis of various pathways for electrochemical hydrogen production coupled with the anodic oxidation of urea, offering a sustainable alternative to the conventional oxygen evolution reaction. For the first time, the feasibility and efficiency of these processes were evaluated using integrated green chemistry metrics, including atom economy and a newly proposed metric, electricity economy, which quantifies the theoretical minimum electrical energy required for the equilibrium formation of reaction products. The analysis demonstrated that urea-oxidation pathways generally require significantly less energy input than water electrolysis. Among the examined reactions, the oxidation of urea to gaseous nitrogen and carbonate ions was identified as the most efficient, with an electricity economy of –4650.83 J mol–1 and an atom economy of 6.4%. However, practical application is hindered by issues such as low product selectivity and high anodic potentials dictated by the redox thermodynamics of commonly used nickel-based catalysts. These findings underscore the need for next-generation electrocatalysts with enhanced selectivity and lower overpotentials to fully exploit the energetic advantages of urea oxidation for green hydrogen production.
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institution Kabale University
issn 2054-5703
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publisher The Royal Society
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series Royal Society Open Science
spelling doaj-art-ca7687ea02194fd79c43f61dcaf1db362025-08-20T03:31:24ZengThe Royal SocietyRoyal Society Open Science2054-57032025-07-0112710.1098/rsos.250156Towards sustainable urea electro-oxidation: a thermodynamic and green chemistry evaluation of alternative pathwaysVyacheslav Protsenko0Department of Physical Chemistry, Ukrainian State University of Science and Technologies, Dnipro, UkraineThis study presents a comparative thermodynamic analysis of various pathways for electrochemical hydrogen production coupled with the anodic oxidation of urea, offering a sustainable alternative to the conventional oxygen evolution reaction. For the first time, the feasibility and efficiency of these processes were evaluated using integrated green chemistry metrics, including atom economy and a newly proposed metric, electricity economy, which quantifies the theoretical minimum electrical energy required for the equilibrium formation of reaction products. The analysis demonstrated that urea-oxidation pathways generally require significantly less energy input than water electrolysis. Among the examined reactions, the oxidation of urea to gaseous nitrogen and carbonate ions was identified as the most efficient, with an electricity economy of –4650.83 J mol–1 and an atom economy of 6.4%. However, practical application is hindered by issues such as low product selectivity and high anodic potentials dictated by the redox thermodynamics of commonly used nickel-based catalysts. These findings underscore the need for next-generation electrocatalysts with enhanced selectivity and lower overpotentials to fully exploit the energetic advantages of urea oxidation for green hydrogen production.https://royalsocietypublishing.org/doi/10.1098/rsos.250156electrochemical hydrogen productionurea-oxidation reactiongreen chemistry metricselectricity economyelectrocatalyst development
spellingShingle Vyacheslav Protsenko
Towards sustainable urea electro-oxidation: a thermodynamic and green chemistry evaluation of alternative pathways
Royal Society Open Science
electrochemical hydrogen production
urea-oxidation reaction
green chemistry metrics
electricity economy
electrocatalyst development
title Towards sustainable urea electro-oxidation: a thermodynamic and green chemistry evaluation of alternative pathways
title_full Towards sustainable urea electro-oxidation: a thermodynamic and green chemistry evaluation of alternative pathways
title_fullStr Towards sustainable urea electro-oxidation: a thermodynamic and green chemistry evaluation of alternative pathways
title_full_unstemmed Towards sustainable urea electro-oxidation: a thermodynamic and green chemistry evaluation of alternative pathways
title_short Towards sustainable urea electro-oxidation: a thermodynamic and green chemistry evaluation of alternative pathways
title_sort towards sustainable urea electro oxidation a thermodynamic and green chemistry evaluation of alternative pathways
topic electrochemical hydrogen production
urea-oxidation reaction
green chemistry metrics
electricity economy
electrocatalyst development
url https://royalsocietypublishing.org/doi/10.1098/rsos.250156
work_keys_str_mv AT vyacheslavprotsenko towardssustainableureaelectrooxidationathermodynamicandgreenchemistryevaluationofalternativepathways