Simultaneous value-added utilization of photogenerated electrons and holes on Pd/TiO2

Abstract The biggest challenge facing the advancement of photocatalytic technology so far is how to achieve the simultaneous and efficient utilization of photogenerated electrons and holes for dual value-added chemicals. Here we show that Pd/TiO2 with electronic metal-support interaction realizes ph...

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Main Authors: Boxin Liu, Zhuofeng Hu, Yanfang Li, Xin Tan, Jinhua Ye, Tao Yu
Format: Article
Language:English
Published: Nature Portfolio 2025-07-01
Series:Nature Communications
Online Access:https://doi.org/10.1038/s41467-025-61223-0
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author Boxin Liu
Zhuofeng Hu
Yanfang Li
Xin Tan
Jinhua Ye
Tao Yu
author_facet Boxin Liu
Zhuofeng Hu
Yanfang Li
Xin Tan
Jinhua Ye
Tao Yu
author_sort Boxin Liu
collection DOAJ
description Abstract The biggest challenge facing the advancement of photocatalytic technology so far is how to achieve the simultaneous and efficient utilization of photogenerated electrons and holes for dual value-added chemicals. Here we show that Pd/TiO2 with electronic metal-support interaction realizes photocatalytic H2O2 evolution coupled with furfural selective oxidation to furoic acid. We demonstrate that the electronic structure of Pd is modulated to form Pdδ+ active sites and upshifted d-band center via electronic metal-support interaction, enhancing O2 adsorption and H2O2 evolution performance, and the photogenerated holes from TiO2 oxidize furfural undergoing the Aldehyde-Water Shift to furoic acid by sequential breaking of O-H and C-H bonds. The optimal Pd/TiO2 achieves H2O2 and furoic acid evolution rates of 3672.31 and 4529.08 μM h−1 with furfural conversion of 92.66% and furoic acid selectivity of 97.82%. Our work provides a promising approach for enhancing synergistic photosynthesis of dual value-added chemicals, thus advancing carbon neutrality goals.
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institution Kabale University
issn 2041-1723
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series Nature Communications
spelling doaj-art-c9ca4f47397442b78bb563d18c745f612025-08-20T03:37:37ZengNature PortfolioNature Communications2041-17232025-07-0116111310.1038/s41467-025-61223-0Simultaneous value-added utilization of photogenerated electrons and holes on Pd/TiO2Boxin Liu0Zhuofeng Hu1Yanfang Li2Xin Tan3Jinhua Ye4Tao Yu5School of Environmental Science and Engineering, Tianjin UniversitySchool of Environmental Science and Engineering, Guangdong Provincial Key Laboratory of Environmental Pollution Control and Remediation Technology, Sun Yat-sen UniversitySchool of Environmental Science and Engineering, Tianjin UniversitySchool of Environmental Science and Engineering, Tianjin UniversityResearch Center for Solar Driven Carbon Neutrality, Hebei UniversitySchool of Chemical Engineering and Technology, Tianjin UniversityAbstract The biggest challenge facing the advancement of photocatalytic technology so far is how to achieve the simultaneous and efficient utilization of photogenerated electrons and holes for dual value-added chemicals. Here we show that Pd/TiO2 with electronic metal-support interaction realizes photocatalytic H2O2 evolution coupled with furfural selective oxidation to furoic acid. We demonstrate that the electronic structure of Pd is modulated to form Pdδ+ active sites and upshifted d-band center via electronic metal-support interaction, enhancing O2 adsorption and H2O2 evolution performance, and the photogenerated holes from TiO2 oxidize furfural undergoing the Aldehyde-Water Shift to furoic acid by sequential breaking of O-H and C-H bonds. The optimal Pd/TiO2 achieves H2O2 and furoic acid evolution rates of 3672.31 and 4529.08 μM h−1 with furfural conversion of 92.66% and furoic acid selectivity of 97.82%. Our work provides a promising approach for enhancing synergistic photosynthesis of dual value-added chemicals, thus advancing carbon neutrality goals.https://doi.org/10.1038/s41467-025-61223-0
spellingShingle Boxin Liu
Zhuofeng Hu
Yanfang Li
Xin Tan
Jinhua Ye
Tao Yu
Simultaneous value-added utilization of photogenerated electrons and holes on Pd/TiO2
Nature Communications
title Simultaneous value-added utilization of photogenerated electrons and holes on Pd/TiO2
title_full Simultaneous value-added utilization of photogenerated electrons and holes on Pd/TiO2
title_fullStr Simultaneous value-added utilization of photogenerated electrons and holes on Pd/TiO2
title_full_unstemmed Simultaneous value-added utilization of photogenerated electrons and holes on Pd/TiO2
title_short Simultaneous value-added utilization of photogenerated electrons and holes on Pd/TiO2
title_sort simultaneous value added utilization of photogenerated electrons and holes on pd tio2
url https://doi.org/10.1038/s41467-025-61223-0
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AT zhuofenghu simultaneousvalueaddedutilizationofphotogeneratedelectronsandholesonpdtio2
AT yanfangli simultaneousvalueaddedutilizationofphotogeneratedelectronsandholesonpdtio2
AT xintan simultaneousvalueaddedutilizationofphotogeneratedelectronsandholesonpdtio2
AT jinhuaye simultaneousvalueaddedutilizationofphotogeneratedelectronsandholesonpdtio2
AT taoyu simultaneousvalueaddedutilizationofphotogeneratedelectronsandholesonpdtio2