Sn and Cu influence on Mg:Si ratios evolution in clusters based on DFT and its impact on precipitation hardening of pre-aged Al-1.0Mg-0.6Si alloys

Using atom probe tomography (APT), transmission electron microscopy (TEM), and hardness tests, the effect of Sn and Cu on the evolution of Mg:Si ratios in clusters and subsequent precipitation hardening behavior of pre-aged Al-1.0Mg-0.6Si alloys are investigated, and the underlying mechanism is reve...

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Main Authors: Fengkai Lu, Jianguo Tang, Wenbin Tu, Huijin Tao, Lingying Ye, Shengdan Liu, Xin Zhan, Lehang Ma, Xiyan Hu, Chenlu Yu
Format: Article
Language:English
Published: Elsevier 2024-11-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785424024086
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author Fengkai Lu
Jianguo Tang
Wenbin Tu
Huijin Tao
Lingying Ye
Shengdan Liu
Xin Zhan
Lehang Ma
Xiyan Hu
Chenlu Yu
author_facet Fengkai Lu
Jianguo Tang
Wenbin Tu
Huijin Tao
Lingying Ye
Shengdan Liu
Xin Zhan
Lehang Ma
Xiyan Hu
Chenlu Yu
author_sort Fengkai Lu
collection DOAJ
description Using atom probe tomography (APT), transmission electron microscopy (TEM), and hardness tests, the effect of Sn and Cu on the evolution of Mg:Si ratios in clusters and subsequent precipitation hardening behavior of pre-aged Al-1.0Mg-0.6Si alloys are investigated, and the underlying mechanism is revealed by density functional theory (DFT) calculation of interaction energy. It is shown that, the doping of Sn and/or Cu increases the average Mg:Si ratio in clusters. This increase is attributed to the strong interaction of Sn/Cu with Mg solutes, which enhances the binding of Mg to Si-rich clusters and results in a higher proportion of clusters with Mg:Si ratios near 1 (0.75–1.25). Consequently, the enhanced precipitation of β'' precipitates during artificial aging is observed in Sn and/or Cu doped alloys, due to the ease of clusters with Mg:Si ratios near 1 transform into β'' precipitates, leading to an improved hardening response. Notably, the combined doping of Sn and Cu exhibits the strongest aggregation tendency towards Mg solutes, yielding the most pronounced strengthening effects on precipitation and hardening response during artificial aging. Furthermore, a schematic model detailing the evolution of Mg:Si ratios in clusters is proposed, based on the APT results and DFT calculation of interaction energy.
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spelling doaj-art-c7dec11d0cb0469e86a6f03c741614cd2025-08-20T01:57:25ZengElsevierJournal of Materials Research and Technology2238-78542024-11-01334577458610.1016/j.jmrt.2024.10.138Sn and Cu influence on Mg:Si ratios evolution in clusters based on DFT and its impact on precipitation hardening of pre-aged Al-1.0Mg-0.6Si alloysFengkai Lu0Jianguo Tang1Wenbin Tu2Huijin Tao3Lingying Ye4Shengdan Liu5Xin Zhan6Lehang Ma7Xiyan Hu8Chenlu Yu9School of materials science and engineering, Central South University, Changsha, 410083, ChinaSchool of materials science and engineering, Central South University, Changsha, 410083, China; Corresponding author.Jiangxi Key Laboratory of Forming and Joining Technology for Aerospace Components, Nanchang Hangkong University, Nanchang, 330063, China; Corresponding author.School of materials science and engineering, Central South University, Changsha, 410083, ChinaSchool of materials science and engineering, Central South University, Changsha, 410083, ChinaSchool of materials science and engineering, Central South University, Changsha, 410083, ChinaSchool of materials science and engineering, Central South University, Changsha, 410083, ChinaSchool of materials science and engineering, Central South University, Changsha, 410083, ChinaSchool of materials science and engineering, Central South University, Changsha, 410083, ChinaSchool of materials science and engineering, Central South University, Changsha, 410083, ChinaUsing atom probe tomography (APT), transmission electron microscopy (TEM), and hardness tests, the effect of Sn and Cu on the evolution of Mg:Si ratios in clusters and subsequent precipitation hardening behavior of pre-aged Al-1.0Mg-0.6Si alloys are investigated, and the underlying mechanism is revealed by density functional theory (DFT) calculation of interaction energy. It is shown that, the doping of Sn and/or Cu increases the average Mg:Si ratio in clusters. This increase is attributed to the strong interaction of Sn/Cu with Mg solutes, which enhances the binding of Mg to Si-rich clusters and results in a higher proportion of clusters with Mg:Si ratios near 1 (0.75–1.25). Consequently, the enhanced precipitation of β'' precipitates during artificial aging is observed in Sn and/or Cu doped alloys, due to the ease of clusters with Mg:Si ratios near 1 transform into β'' precipitates, leading to an improved hardening response. Notably, the combined doping of Sn and Cu exhibits the strongest aggregation tendency towards Mg solutes, yielding the most pronounced strengthening effects on precipitation and hardening response during artificial aging. Furthermore, a schematic model detailing the evolution of Mg:Si ratios in clusters is proposed, based on the APT results and DFT calculation of interaction energy.http://www.sciencedirect.com/science/article/pii/S2238785424024086Atom probe tomographyPrecipitationDensity functional theoryClusteringMg:Si ratio
spellingShingle Fengkai Lu
Jianguo Tang
Wenbin Tu
Huijin Tao
Lingying Ye
Shengdan Liu
Xin Zhan
Lehang Ma
Xiyan Hu
Chenlu Yu
Sn and Cu influence on Mg:Si ratios evolution in clusters based on DFT and its impact on precipitation hardening of pre-aged Al-1.0Mg-0.6Si alloys
Journal of Materials Research and Technology
Atom probe tomography
Precipitation
Density functional theory
Clustering
Mg:Si ratio
title Sn and Cu influence on Mg:Si ratios evolution in clusters based on DFT and its impact on precipitation hardening of pre-aged Al-1.0Mg-0.6Si alloys
title_full Sn and Cu influence on Mg:Si ratios evolution in clusters based on DFT and its impact on precipitation hardening of pre-aged Al-1.0Mg-0.6Si alloys
title_fullStr Sn and Cu influence on Mg:Si ratios evolution in clusters based on DFT and its impact on precipitation hardening of pre-aged Al-1.0Mg-0.6Si alloys
title_full_unstemmed Sn and Cu influence on Mg:Si ratios evolution in clusters based on DFT and its impact on precipitation hardening of pre-aged Al-1.0Mg-0.6Si alloys
title_short Sn and Cu influence on Mg:Si ratios evolution in clusters based on DFT and its impact on precipitation hardening of pre-aged Al-1.0Mg-0.6Si alloys
title_sort sn and cu influence on mg si ratios evolution in clusters based on dft and its impact on precipitation hardening of pre aged al 1 0mg 0 6si alloys
topic Atom probe tomography
Precipitation
Density functional theory
Clustering
Mg:Si ratio
url http://www.sciencedirect.com/science/article/pii/S2238785424024086
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