Synthesis and characterization of Azo derivatives containing pyrazole ring
This research included the preparation of new pyrazole derivatives from the condensation of the benzoyl acetone with carboxylic acid hydrazide in ethanol as a solvent. The reaction included two steps from the tetra surfaces nucleophilic addition and cyclisation process in second step. The pyrazole...
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| Format: | Article |
| Language: | English |
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Tikrit University
2023-02-01
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| Series: | Tikrit Journal of Pure Science |
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| Online Access: | https://tjpsj.org/index.php/tjps/article/view/1114 |
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| author | Ibtisam Taufek Ameen Gazwan Hassan Al-Soumadaiy Khudhair. Aba'as Khudhair |
| author_facet | Ibtisam Taufek Ameen Gazwan Hassan Al-Soumadaiy Khudhair. Aba'as Khudhair |
| author_sort | Ibtisam Taufek Ameen |
| collection | DOAJ |
| description |
This research included the preparation of new pyrazole derivatives from the condensation of the benzoyl acetone with carboxylic acid hydrazide in ethanol as a solvent. The reaction included two steps from the tetra surfaces nucleophilic addition and cyclisation process in second step. The pyrazole derivatives products were reacted with Diazonium salts.
The prepared compounds were characterized by infrared, Nuclear Magnatic resonance spectroscopy and the completing of the reaction was checking by the TLC.
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| format | Article |
| id | doaj-art-c63f3365808342f4a888afb3d16ccbb5 |
| institution | OA Journals |
| issn | 1813-1662 2415-1726 |
| language | English |
| publishDate | 2023-02-01 |
| publisher | Tikrit University |
| record_format | Article |
| series | Tikrit Journal of Pure Science |
| spelling | doaj-art-c63f3365808342f4a888afb3d16ccbb52025-08-20T02:36:27ZengTikrit UniversityTikrit Journal of Pure Science1813-16622415-17262023-02-0121710.25130/tjps.v21i7.1114Synthesis and characterization of Azo derivatives containing pyrazole ringIbtisam Taufek AmeenGazwan Hassan Al-SoumadaiyKhudhair. Aba'as Khudhair This research included the preparation of new pyrazole derivatives from the condensation of the benzoyl acetone with carboxylic acid hydrazide in ethanol as a solvent. The reaction included two steps from the tetra surfaces nucleophilic addition and cyclisation process in second step. The pyrazole derivatives products were reacted with Diazonium salts. The prepared compounds were characterized by infrared, Nuclear Magnatic resonance spectroscopy and the completing of the reaction was checking by the TLC. https://tjpsj.org/index.php/tjps/article/view/1114PyrazoleAzo dyesNucleophilic addition |
| spellingShingle | Ibtisam Taufek Ameen Gazwan Hassan Al-Soumadaiy Khudhair. Aba'as Khudhair Synthesis and characterization of Azo derivatives containing pyrazole ring Tikrit Journal of Pure Science Pyrazole Azo dyes Nucleophilic addition |
| title | Synthesis and characterization of Azo derivatives containing pyrazole ring |
| title_full | Synthesis and characterization of Azo derivatives containing pyrazole ring |
| title_fullStr | Synthesis and characterization of Azo derivatives containing pyrazole ring |
| title_full_unstemmed | Synthesis and characterization of Azo derivatives containing pyrazole ring |
| title_short | Synthesis and characterization of Azo derivatives containing pyrazole ring |
| title_sort | synthesis and characterization of azo derivatives containing pyrazole ring |
| topic | Pyrazole Azo dyes Nucleophilic addition |
| url | https://tjpsj.org/index.php/tjps/article/view/1114 |
| work_keys_str_mv | AT ibtisamtaufekameen synthesisandcharacterizationofazoderivativescontainingpyrazolering AT gazwanhassanalsoumadaiy synthesisandcharacterizationofazoderivativescontainingpyrazolering AT khudhairabaaskhudhair synthesisandcharacterizationofazoderivativescontainingpyrazolering |