Enhancing Ciprofloxacin Removal: Unveiling the Potential of Graphene Oxide Synthesized from Cassava Peels through Box-Behnken Design Optimization

The adsorption of ciprofloxacin from an aqueous solution using graphene oxide as an adsorbent derived from cassava peel waste using a modified Hummers method was described. The properties of the adsorbent were characterized using Fourier-Transform Infrared Spectroscopy, X-ray diffraction, Raman Spec...

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Main Authors: Rinawati Rinawati, Buhani Buhani, Widiarti Widiarti, Ahmad Isro, Elsa Fitrianingsih, Anisa Rahmawati, Agung Abadi Kiswandono, Fidelis Nitti
Format: Article
Language:English
Published: SDEWES Centre 2024-12-01
Series:Journal of Sustainable Development of Energy, Water and Environment Systems
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Online Access: http://www.sdewes.org/jsdewes/pid12.0516
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author Rinawati Rinawati
Buhani Buhani
Widiarti Widiarti
Ahmad Isro
Elsa Fitrianingsih
Anisa Rahmawati
Agung Abadi Kiswandono
Fidelis Nitti
author_facet Rinawati Rinawati
Buhani Buhani
Widiarti Widiarti
Ahmad Isro
Elsa Fitrianingsih
Anisa Rahmawati
Agung Abadi Kiswandono
Fidelis Nitti
author_sort Rinawati Rinawati
collection DOAJ
description The adsorption of ciprofloxacin from an aqueous solution using graphene oxide as an adsorbent derived from cassava peel waste using a modified Hummers method was described. The properties of the adsorbent were characterized using Fourier-Transform Infrared Spectroscopy, X-ray diffraction, Raman Spectroscopy and Scanning Electron Microscopy-Energy Dispersive X-ray techniques. The influence of the operational variables including potential of hydrogen, adsorbent mass, and contact time in the adsorption of ciprofloxacin was evaluated by response surface methodology. In particular, the interactions between the operational variables were evaluated using the Box-Behnken Design to determine the optimum conditions. The results indicated that the optimum conditions were achieved at pH 3, contact time of 20 minutes, using 35 mg of graphene oxide adsorbent, resulting in an adsorption efficiency of 91.71%. The results demonstrated that the graphene oxide material derived from cassava peel waste can be effectively used as an adsorbent for ciprofloxacin from aqueous solutions.
format Article
id doaj-art-c559a2207ad7430dadd5ed7c015bdfc4
institution OA Journals
issn 1848-9257
language English
publishDate 2024-12-01
publisher SDEWES Centre
record_format Article
series Journal of Sustainable Development of Energy, Water and Environment Systems
spelling doaj-art-c559a2207ad7430dadd5ed7c015bdfc42025-08-20T02:38:51ZengSDEWES CentreJournal of Sustainable Development of Energy, Water and Environment Systems1848-92572024-12-0112412010.13044/j.sdewes.d12.05161120516Enhancing Ciprofloxacin Removal: Unveiling the Potential of Graphene Oxide Synthesized from Cassava Peels through Box-Behnken Design OptimizationRinawati Rinawati0Buhani Buhani1Widiarti Widiarti2Ahmad Isro3Elsa Fitrianingsih4Anisa Rahmawati5Agung Abadi Kiswandono6Fidelis Nitti7 Universitas Lampung, Bandar Lampung, Indonesia Universitas Lampung, Bandar Lampung, Indonesia Universitas Lampung, Bandar Lampung, Indonesia Universitas Lampung, Bandar Lampung, Indonesia Universitas Lampung, Bandar Lampung, Indonesia Universitas Lampung, Bandar Lampung, Indonesia Universitas Lampung, Bandar Lampung, Indonesia University of Nusa Cendana, Kupang, Indonesia The adsorption of ciprofloxacin from an aqueous solution using graphene oxide as an adsorbent derived from cassava peel waste using a modified Hummers method was described. The properties of the adsorbent were characterized using Fourier-Transform Infrared Spectroscopy, X-ray diffraction, Raman Spectroscopy and Scanning Electron Microscopy-Energy Dispersive X-ray techniques. The influence of the operational variables including potential of hydrogen, adsorbent mass, and contact time in the adsorption of ciprofloxacin was evaluated by response surface methodology. In particular, the interactions between the operational variables were evaluated using the Box-Behnken Design to determine the optimum conditions. The results indicated that the optimum conditions were achieved at pH 3, contact time of 20 minutes, using 35 mg of graphene oxide adsorbent, resulting in an adsorption efficiency of 91.71%. The results demonstrated that the graphene oxide material derived from cassava peel waste can be effectively used as an adsorbent for ciprofloxacin from aqueous solutions. http://www.sdewes.org/jsdewes/pid12.0516 ciprofloxacin; adsorption; graphene oxide; cassava peel waste; box behnken design
spellingShingle Rinawati Rinawati
Buhani Buhani
Widiarti Widiarti
Ahmad Isro
Elsa Fitrianingsih
Anisa Rahmawati
Agung Abadi Kiswandono
Fidelis Nitti
Enhancing Ciprofloxacin Removal: Unveiling the Potential of Graphene Oxide Synthesized from Cassava Peels through Box-Behnken Design Optimization
Journal of Sustainable Development of Energy, Water and Environment Systems
ciprofloxacin; adsorption; graphene oxide; cassava peel waste; box behnken design
title Enhancing Ciprofloxacin Removal: Unveiling the Potential of Graphene Oxide Synthesized from Cassava Peels through Box-Behnken Design Optimization
title_full Enhancing Ciprofloxacin Removal: Unveiling the Potential of Graphene Oxide Synthesized from Cassava Peels through Box-Behnken Design Optimization
title_fullStr Enhancing Ciprofloxacin Removal: Unveiling the Potential of Graphene Oxide Synthesized from Cassava Peels through Box-Behnken Design Optimization
title_full_unstemmed Enhancing Ciprofloxacin Removal: Unveiling the Potential of Graphene Oxide Synthesized from Cassava Peels through Box-Behnken Design Optimization
title_short Enhancing Ciprofloxacin Removal: Unveiling the Potential of Graphene Oxide Synthesized from Cassava Peels through Box-Behnken Design Optimization
title_sort enhancing ciprofloxacin removal unveiling the potential of graphene oxide synthesized from cassava peels through box behnken design optimization
topic ciprofloxacin; adsorption; graphene oxide; cassava peel waste; box behnken design
url http://www.sdewes.org/jsdewes/pid12.0516
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