Purification of Crocin-I from Gardenia Yellow by Macroporous Resin Columns In-Series and Its Antidepressant-Like Effect

In this study, the purification of crocin-I from Gardenia yellow by macroporous resin columns in-series was systematically investigated. The in-series macroporous adsorption resins consisting of XAD 4 and XAD 1600N resins were selected on the basis of the evaluation of performance and separation cha...

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Main Authors: Yu Jiang, Susu Lin, Qiaoqiao Li, Yingpeng Tong, Ping Wang
Format: Article
Language:English
Published: Wiley 2022-01-01
Series:Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2022/7651553
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author Yu Jiang
Susu Lin
Qiaoqiao Li
Yingpeng Tong
Ping Wang
author_facet Yu Jiang
Susu Lin
Qiaoqiao Li
Yingpeng Tong
Ping Wang
author_sort Yu Jiang
collection DOAJ
description In this study, the purification of crocin-I from Gardenia yellow by macroporous resin columns in-series was systematically investigated. The in-series macroporous adsorption resins consisting of XAD 4 and XAD 1600N resins were selected on the basis of the evaluation of performance and separation characteristics of 17 kinds of resins, including the adsorption capacities, desorption ratio, and separation degree. According to the analysis results, the optimum conditions were as follows: bed volume ratio of XAD 4 and XAD 1600N resins, sample volume, flow rate, and methanol concentration were 3 : 1, 5 BV, 15 BV/h, and 70%, respectively (BV was the bed volume of XAD 4 resin). After one run treatment, the separation degree of crocin-I at 254 nm and 440 nm decreased from 1.92 to 0.08 (DC−254 nm) and from 0.71 to 0.36 (DC−440 nm), respectively. The results showed that the in-series macroporous resins revealed a high capacity in the purification of crocin-I. Meanwhile, in the animal experiment, the forced swimming tests were regulated by crocin-I and Gardenia yellow, which demonstrated that crocin-I was the main constituent of Gardenia yellow and had potential antidepressant biological activities.
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publishDate 2022-01-01
publisher Wiley
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spelling doaj-art-c4d40303d3d047289807e45180cf347f2025-08-20T02:18:47ZengWileyJournal of Chemistry2090-90712022-01-01202210.1155/2022/7651553Purification of Crocin-I from Gardenia Yellow by Macroporous Resin Columns In-Series and Its Antidepressant-Like EffectYu Jiang0Susu Lin1Qiaoqiao Li2Yingpeng Tong3Ping Wang4College of Pharmaceutical SciencesCollege of Pharmaceutical SciencesCollege of Pharmaceutical SciencesInstitute of Natural Medicine and Health ProductCollege of Pharmaceutical SciencesIn this study, the purification of crocin-I from Gardenia yellow by macroporous resin columns in-series was systematically investigated. The in-series macroporous adsorption resins consisting of XAD 4 and XAD 1600N resins were selected on the basis of the evaluation of performance and separation characteristics of 17 kinds of resins, including the adsorption capacities, desorption ratio, and separation degree. According to the analysis results, the optimum conditions were as follows: bed volume ratio of XAD 4 and XAD 1600N resins, sample volume, flow rate, and methanol concentration were 3 : 1, 5 BV, 15 BV/h, and 70%, respectively (BV was the bed volume of XAD 4 resin). After one run treatment, the separation degree of crocin-I at 254 nm and 440 nm decreased from 1.92 to 0.08 (DC−254 nm) and from 0.71 to 0.36 (DC−440 nm), respectively. The results showed that the in-series macroporous resins revealed a high capacity in the purification of crocin-I. Meanwhile, in the animal experiment, the forced swimming tests were regulated by crocin-I and Gardenia yellow, which demonstrated that crocin-I was the main constituent of Gardenia yellow and had potential antidepressant biological activities.http://dx.doi.org/10.1155/2022/7651553
spellingShingle Yu Jiang
Susu Lin
Qiaoqiao Li
Yingpeng Tong
Ping Wang
Purification of Crocin-I from Gardenia Yellow by Macroporous Resin Columns In-Series and Its Antidepressant-Like Effect
Journal of Chemistry
title Purification of Crocin-I from Gardenia Yellow by Macroporous Resin Columns In-Series and Its Antidepressant-Like Effect
title_full Purification of Crocin-I from Gardenia Yellow by Macroporous Resin Columns In-Series and Its Antidepressant-Like Effect
title_fullStr Purification of Crocin-I from Gardenia Yellow by Macroporous Resin Columns In-Series and Its Antidepressant-Like Effect
title_full_unstemmed Purification of Crocin-I from Gardenia Yellow by Macroporous Resin Columns In-Series and Its Antidepressant-Like Effect
title_short Purification of Crocin-I from Gardenia Yellow by Macroporous Resin Columns In-Series and Its Antidepressant-Like Effect
title_sort purification of crocin i from gardenia yellow by macroporous resin columns in series and its antidepressant like effect
url http://dx.doi.org/10.1155/2022/7651553
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AT qiaoqiaoli purificationofcrocinifromgardeniayellowbymacroporousresincolumnsinseriesanditsantidepressantlikeeffect
AT yingpengtong purificationofcrocinifromgardeniayellowbymacroporousresincolumnsinseriesanditsantidepressantlikeeffect
AT pingwang purificationofcrocinifromgardeniayellowbymacroporousresincolumnsinseriesanditsantidepressantlikeeffect