SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor
The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution....
Saved in:
| Main Authors: | , , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
University of Belgrade, Technical Faculty, Bor
2013-01-01
|
| Series: | Journal of Mining and Metallurgy. Section B: Metallurgy |
| Subjects: | |
| Online Access: | http://www.doiserbia.nb.rs/img/doi/1450-5339/2013/1450-53391200041D.pdf |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| _version_ | 1832569217577123840 |
|---|---|
| author | Dimitrijević R. Cvetković O. Miodragović Z. Simić M. Manojlović D. Jović V. |
| author_facet | Dimitrijević R. Cvetković O. Miodragović Z. Simić M. Manojlović D. Jović V. |
| author_sort | Dimitrijević R. |
| collection | DOAJ |
| description | The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM analysis revealed that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard. |
| format | Article |
| id | doaj-art-c4662feefe334781ae52b7ad6f4bf272 |
| institution | Kabale University |
| issn | 1450-5339 |
| language | English |
| publishDate | 2013-01-01 |
| publisher | University of Belgrade, Technical Faculty, Bor |
| record_format | Article |
| series | Journal of Mining and Metallurgy. Section B: Metallurgy |
| spelling | doaj-art-c4662feefe334781ae52b7ad6f4bf2722025-02-02T22:50:30ZengUniversity of Belgrade, Technical Faculty, BorJournal of Mining and Metallurgy. Section B: Metallurgy1450-53392013-01-01491919510.2298/JMMB120111041DSEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursorDimitrijević R.Cvetković O.Miodragović Z.Simić M.Manojlović D.Jović V.The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM analysis revealed that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard.http://www.doiserbia.nb.rs/img/doi/1450-5339/2013/1450-53391200041D.pdfAg nanoparticlesSphere shapedChemical depositionXRD techniqueSEM/EDX analysis |
| spellingShingle | Dimitrijević R. Cvetković O. Miodragović Z. Simić M. Manojlović D. Jović V. SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor Journal of Mining and Metallurgy. Section B: Metallurgy Ag nanoparticles Sphere shaped Chemical deposition XRD technique SEM/EDX analysis |
| title | SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor |
| title_full | SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor |
| title_fullStr | SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor |
| title_full_unstemmed | SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor |
| title_short | SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor |
| title_sort | sem edx and xrd characterization of silver nanocrystalline thin film prepared from organometallic solution precursor |
| topic | Ag nanoparticles Sphere shaped Chemical deposition XRD technique SEM/EDX analysis |
| url | http://www.doiserbia.nb.rs/img/doi/1450-5339/2013/1450-53391200041D.pdf |
| work_keys_str_mv | AT dimitrijevicr semedxandxrdcharacterizationofsilvernanocrystallinethinfilmpreparedfromorganometallicsolutionprecursor AT cvetkovico semedxandxrdcharacterizationofsilvernanocrystallinethinfilmpreparedfromorganometallicsolutionprecursor AT miodragovicz semedxandxrdcharacterizationofsilvernanocrystallinethinfilmpreparedfromorganometallicsolutionprecursor AT simicm semedxandxrdcharacterizationofsilvernanocrystallinethinfilmpreparedfromorganometallicsolutionprecursor AT manojlovicd semedxandxrdcharacterizationofsilvernanocrystallinethinfilmpreparedfromorganometallicsolutionprecursor AT jovicv semedxandxrdcharacterizationofsilvernanocrystallinethinfilmpreparedfromorganometallicsolutionprecursor |