A Ternary Catalytic System for the Room Temperature Suzuki-Miyaura Reaction in Water

The formation of Pd(0) in the absence of any classical reducing agent in a medium containing Mg2+/Al3+ layered double hydroxide (LDH) and N,N-dimethylformamide was evidenced. XRD analysis showed the presence of crystalline phases of palladium in the Pd/LDH composite. Suzuki-Miyaura reactions in aque...

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Main Authors: Aires da Conceição Silva, Jaqueline Dias Senra, Andréa Luzia Ferreira de Souza, Luiz Fernando Brum Malta
Format: Article
Language:English
Published: Wiley 2013-01-01
Series:The Scientific World Journal
Online Access:http://dx.doi.org/10.1155/2013/456789
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author Aires da Conceição Silva
Jaqueline Dias Senra
Andréa Luzia Ferreira de Souza
Luiz Fernando Brum Malta
author_facet Aires da Conceição Silva
Jaqueline Dias Senra
Andréa Luzia Ferreira de Souza
Luiz Fernando Brum Malta
author_sort Aires da Conceição Silva
collection DOAJ
description The formation of Pd(0) in the absence of any classical reducing agent in a medium containing Mg2+/Al3+ layered double hydroxide (LDH) and N,N-dimethylformamide was evidenced. XRD analysis showed the presence of crystalline phases of palladium in the Pd/LDH composite. Suzuki-Miyaura reactions in aqueous medium were carried out at room temperature, and good yields were obtained with bromoarenes and iodoarenes using the ternary system LDH-Pd-CD (cyclodextrin) as catalyst.
format Article
id doaj-art-c4449e53ece84953981dc3ca04562a8b
institution DOAJ
issn 1537-744X
language English
publishDate 2013-01-01
publisher Wiley
record_format Article
series The Scientific World Journal
spelling doaj-art-c4449e53ece84953981dc3ca04562a8b2025-08-20T03:04:59ZengWileyThe Scientific World Journal1537-744X2013-01-01201310.1155/2013/456789456789A Ternary Catalytic System for the Room Temperature Suzuki-Miyaura Reaction in WaterAires da Conceição Silva0Jaqueline Dias Senra1Andréa Luzia Ferreira de Souza2Luiz Fernando Brum Malta3Instituto de Química, Universidade Federal do Rio de Janeiro, CT Bloco A Lab 641, 21941-909 Rio de Janeiro, RJ, BrazilNúcleo de Pesquisas de Produtos Naturais, Universidade Federal do Rio de Janeiro, CCS Bloco H, 21941-614 Rio de Janeiro, RJ, BrazilInstituto de Química, Universidade Federal do Rio de Janeiro, 27930-560 Macaé, RJ, BrazilInstituto de Química, Universidade Federal do Rio de Janeiro, CT Bloco A Lab 641, 21941-909 Rio de Janeiro, RJ, BrazilThe formation of Pd(0) in the absence of any classical reducing agent in a medium containing Mg2+/Al3+ layered double hydroxide (LDH) and N,N-dimethylformamide was evidenced. XRD analysis showed the presence of crystalline phases of palladium in the Pd/LDH composite. Suzuki-Miyaura reactions in aqueous medium were carried out at room temperature, and good yields were obtained with bromoarenes and iodoarenes using the ternary system LDH-Pd-CD (cyclodextrin) as catalyst.http://dx.doi.org/10.1155/2013/456789
spellingShingle Aires da Conceição Silva
Jaqueline Dias Senra
Andréa Luzia Ferreira de Souza
Luiz Fernando Brum Malta
A Ternary Catalytic System for the Room Temperature Suzuki-Miyaura Reaction in Water
The Scientific World Journal
title A Ternary Catalytic System for the Room Temperature Suzuki-Miyaura Reaction in Water
title_full A Ternary Catalytic System for the Room Temperature Suzuki-Miyaura Reaction in Water
title_fullStr A Ternary Catalytic System for the Room Temperature Suzuki-Miyaura Reaction in Water
title_full_unstemmed A Ternary Catalytic System for the Room Temperature Suzuki-Miyaura Reaction in Water
title_short A Ternary Catalytic System for the Room Temperature Suzuki-Miyaura Reaction in Water
title_sort ternary catalytic system for the room temperature suzuki miyaura reaction in water
url http://dx.doi.org/10.1155/2013/456789
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