Resveratrol-Loaded Dissolving Microneedles: Fabrication and <i>in vitro</i> Evaluation

Resveratrol (Res), an active ingredient derived from a multitude of plants, exhibits multiple pharmacological activities. However, its poor water solubility and low bioavailability present significant challenges to its clinical application. Our study aimed to improve the transdermal absorption of Re...

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Main Authors: Banghuai Xing, Qian Luo, Tiantian Gan, Yi Jin, Jianfang Feng, Meng Cheng, Liangxing Tu
Format: Article
Language:English
Published: Georg Thieme Verlag KG 2024-12-01
Series:Pharmaceutical Fronts
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Online Access:http://www.thieme-connect.de/DOI/DOI?10.1055/s-0044-1791832
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author Banghuai Xing
Qian Luo
Tiantian Gan
Yi Jin
Jianfang Feng
Meng Cheng
Liangxing Tu
author_facet Banghuai Xing
Qian Luo
Tiantian Gan
Yi Jin
Jianfang Feng
Meng Cheng
Liangxing Tu
author_sort Banghuai Xing
collection DOAJ
description Resveratrol (Res), an active ingredient derived from a multitude of plants, exhibits multiple pharmacological activities. However, its poor water solubility and low bioavailability present significant challenges to its clinical application. Our study aimed to improve the transdermal absorption of Res using dissolving microneedle (MN) technology, which could effectively overcome the stratum corneum barrier. Res-loaded dissolving microneedles (Res-MNs) were fabricated using polyvinyl pyrrolidone K90 (PVP K90) as the matrix material, and a two-step casting procedure was employed. The process was optimized using the Box–Behnken experimental design approach. The characteristics of Res-MNs in vitro, including morphology, solubility, safety evaluation, and skin permeation, were studied. The results showed that the optimum preparation conditions of Res-MNs were a centrifugation time of 10 minutes, a solvent concentration of 25%, and a prescription ratio (Res: matrix) of 0.375. The skin permeability of the Res-MNs was enhanced compared with Res suspension and Res gel. The cumulative release of Res-MNs in vitro was 75%, which was approximately 5 and 3 times that of the Res suspension group and Res gel group. These results suggest that dissolving MNs may represent a potential approach for enhancing the transdermal delivery of poorly absorbed drugs such as Res.
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language English
publishDate 2024-12-01
publisher Georg Thieme Verlag KG
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series Pharmaceutical Fronts
spelling doaj-art-c413d45fa5ff4aefb1ac53a1a83068252025-08-20T02:32:11ZengGeorg Thieme Verlag KGPharmaceutical Fronts2628-50882628-50962024-12-010604e439e44810.1055/s-0044-1791832Resveratrol-Loaded Dissolving Microneedles: Fabrication and <i>in vitro</i> EvaluationBanghuai Xing0Qian Luo1Tiantian Gan2Yi Jin3Jianfang Feng4Meng Cheng5Liangxing Tu6Division of Innovative Pharmaceutical Sciences, National Pharmaceutical Engineering Center for Solid Preparation in Chinese Herbal Medicine, Jiangxi University of Traditional Chinese Medicine, Nanchang, People's Republic of ChinaDivision of Innovative Pharmaceutical Sciences, National Pharmaceutical Engineering Center for Solid Preparation in Chinese Herbal Medicine, Jiangxi University of Traditional Chinese Medicine, Nanchang, People's Republic of ChinaDivision of Innovative Pharmaceutical Sciences, National Pharmaceutical Engineering Center for Solid Preparation in Chinese Herbal Medicine, Jiangxi University of Traditional Chinese Medicine, Nanchang, People's Republic of ChinaDivision of Innovative Pharmaceutical Sciences, National Pharmaceutical Engineering Center for Solid Preparation in Chinese Herbal Medicine, Jiangxi University of Traditional Chinese Medicine, Nanchang, People's Republic of ChinaDivision of Innovative Pharmaceutical Sciences, National Pharmaceutical Engineering Center for Solid Preparation in Chinese Herbal Medicine, Jiangxi University of Traditional Chinese Medicine, Nanchang, People's Republic of ChinaGCP Center, The Affiliated Hospital of Jiangxi University of Chinese Medicine, Nanchang, People's Republic of ChinaDivision of Innovative Pharmaceutical Sciences, National Pharmaceutical Engineering Center for Solid Preparation in Chinese Herbal Medicine, Jiangxi University of Traditional Chinese Medicine, Nanchang, People's Republic of ChinaResveratrol (Res), an active ingredient derived from a multitude of plants, exhibits multiple pharmacological activities. However, its poor water solubility and low bioavailability present significant challenges to its clinical application. Our study aimed to improve the transdermal absorption of Res using dissolving microneedle (MN) technology, which could effectively overcome the stratum corneum barrier. Res-loaded dissolving microneedles (Res-MNs) were fabricated using polyvinyl pyrrolidone K90 (PVP K90) as the matrix material, and a two-step casting procedure was employed. The process was optimized using the Box–Behnken experimental design approach. The characteristics of Res-MNs in vitro, including morphology, solubility, safety evaluation, and skin permeation, were studied. The results showed that the optimum preparation conditions of Res-MNs were a centrifugation time of 10 minutes, a solvent concentration of 25%, and a prescription ratio (Res: matrix) of 0.375. The skin permeability of the Res-MNs was enhanced compared with Res suspension and Res gel. The cumulative release of Res-MNs in vitro was 75%, which was approximately 5 and 3 times that of the Res suspension group and Res gel group. These results suggest that dissolving MNs may represent a potential approach for enhancing the transdermal delivery of poorly absorbed drugs such as Res.http://www.thieme-connect.de/DOI/DOI?10.1055/s-0044-1791832microneedletransdermalresveratrolabsorptionpolyvinylpyrrolidone K90
spellingShingle Banghuai Xing
Qian Luo
Tiantian Gan
Yi Jin
Jianfang Feng
Meng Cheng
Liangxing Tu
Resveratrol-Loaded Dissolving Microneedles: Fabrication and <i>in vitro</i> Evaluation
Pharmaceutical Fronts
microneedle
transdermal
resveratrol
absorption
polyvinylpyrrolidone K90
title Resveratrol-Loaded Dissolving Microneedles: Fabrication and <i>in vitro</i> Evaluation
title_full Resveratrol-Loaded Dissolving Microneedles: Fabrication and <i>in vitro</i> Evaluation
title_fullStr Resveratrol-Loaded Dissolving Microneedles: Fabrication and <i>in vitro</i> Evaluation
title_full_unstemmed Resveratrol-Loaded Dissolving Microneedles: Fabrication and <i>in vitro</i> Evaluation
title_short Resveratrol-Loaded Dissolving Microneedles: Fabrication and <i>in vitro</i> Evaluation
title_sort resveratrol loaded dissolving microneedles fabrication and i in vitro i evaluation
topic microneedle
transdermal
resveratrol
absorption
polyvinylpyrrolidone K90
url http://www.thieme-connect.de/DOI/DOI?10.1055/s-0044-1791832
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AT tiantiangan resveratrolloadeddissolvingmicroneedlesfabricationandiinvitroievaluation
AT yijin resveratrolloadeddissolvingmicroneedlesfabricationandiinvitroievaluation
AT jianfangfeng resveratrolloadeddissolvingmicroneedlesfabricationandiinvitroievaluation
AT mengcheng resveratrolloadeddissolvingmicroneedlesfabricationandiinvitroievaluation
AT liangxingtu resveratrolloadeddissolvingmicroneedlesfabricationandiinvitroievaluation