Effects of Nb–Ti double microalloying on the grain structure and precipitates of hot compressed FeCrAl alloys

Grain coarsening significantly weakens the strength and toughness of FeCrAl alloys at high temperatures. This study focused on the grain refinement behaviour of a Nb–Ti double-microalloyed FeCrAl alloy (Fe–18Cr–6Al‒0.2Ti‒0.2Nb) after hot compression, and the further development of recrystallization...

Full description

Saved in:
Bibliographic Details
Main Authors: Xing Fan, Fei Wang, Hongming Wang, Bowen Zhao, Runze Li, Jun Zhou
Format: Article
Language:English
Published: Elsevier 2025-03-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S223878542500016X
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1841526300997582848
author Xing Fan
Fei Wang
Hongming Wang
Bowen Zhao
Runze Li
Jun Zhou
author_facet Xing Fan
Fei Wang
Hongming Wang
Bowen Zhao
Runze Li
Jun Zhou
author_sort Xing Fan
collection DOAJ
description Grain coarsening significantly weakens the strength and toughness of FeCrAl alloys at high temperatures. This study focused on the grain refinement behaviour of a Nb–Ti double-microalloyed FeCrAl alloy (Fe–18Cr–6Al‒0.2Ti‒0.2Nb) after hot compression, and the further development of recrystallization grain size during heat treatment was also explored at temperatures of 1100 °C and 1250 °C for 1 and 6 h. Strain-induced Nb-rich and Ti-rich precipitates located at grain boundaries and/or subgrain boundaries influenced dynamic recrystallization during hot compression regardless of parameters such as the strain rate and initial grain size. Additionally, incomplete recrystallization was observed at 1100 °C, with a limited increase in the grain size and a decrease in the size and volume fraction of the Nb-rich and Ti-rich precipitates. Increasing the heating temperature accelerated discontinuous recrystallization, leading to a decrease in the internal dislocation density and hardness. This indicates that the addition of Nb and Ti significantly refined the recrystallized grain size while limiting their growth at high temperatures, which improved the mechanical properties of the Nb–Ti–FeCrAl alloy in high-temperature applications.
format Article
id doaj-art-c344bef82f154e4485982d456d905345
institution Kabale University
issn 2238-7854
language English
publishDate 2025-03-01
publisher Elsevier
record_format Article
series Journal of Materials Research and Technology
spelling doaj-art-c344bef82f154e4485982d456d9053452025-01-17T04:49:32ZengElsevierJournal of Materials Research and Technology2238-78542025-03-0135928941Effects of Nb–Ti double microalloying on the grain structure and precipitates of hot compressed FeCrAl alloysXing Fan0Fei Wang1Hongming Wang2Bowen Zhao3Runze Li4Jun Zhou5Jiangsu University, Zhenjiang 212013, ChinaJiangsu University, Zhenjiang 212013, China; Corresponding author.Jiangsu University, Zhenjiang 212013, ChinaJiangsu University, Zhenjiang 212013, ChinaJiangsu University, Zhenjiang 212013, ChinaChengdu State-owned Jinjiang Machine Factory, Chengdu 610043, ChinaGrain coarsening significantly weakens the strength and toughness of FeCrAl alloys at high temperatures. This study focused on the grain refinement behaviour of a Nb–Ti double-microalloyed FeCrAl alloy (Fe–18Cr–6Al‒0.2Ti‒0.2Nb) after hot compression, and the further development of recrystallization grain size during heat treatment was also explored at temperatures of 1100 °C and 1250 °C for 1 and 6 h. Strain-induced Nb-rich and Ti-rich precipitates located at grain boundaries and/or subgrain boundaries influenced dynamic recrystallization during hot compression regardless of parameters such as the strain rate and initial grain size. Additionally, incomplete recrystallization was observed at 1100 °C, with a limited increase in the grain size and a decrease in the size and volume fraction of the Nb-rich and Ti-rich precipitates. Increasing the heating temperature accelerated discontinuous recrystallization, leading to a decrease in the internal dislocation density and hardness. This indicates that the addition of Nb and Ti significantly refined the recrystallized grain size while limiting their growth at high temperatures, which improved the mechanical properties of the Nb–Ti–FeCrAl alloy in high-temperature applications.http://www.sciencedirect.com/science/article/pii/S223878542500016XHot compressionDouble microalloy controlMicroalloy precipitatesGrain growth
spellingShingle Xing Fan
Fei Wang
Hongming Wang
Bowen Zhao
Runze Li
Jun Zhou
Effects of Nb–Ti double microalloying on the grain structure and precipitates of hot compressed FeCrAl alloys
Journal of Materials Research and Technology
Hot compression
Double microalloy control
Microalloy precipitates
Grain growth
title Effects of Nb–Ti double microalloying on the grain structure and precipitates of hot compressed FeCrAl alloys
title_full Effects of Nb–Ti double microalloying on the grain structure and precipitates of hot compressed FeCrAl alloys
title_fullStr Effects of Nb–Ti double microalloying on the grain structure and precipitates of hot compressed FeCrAl alloys
title_full_unstemmed Effects of Nb–Ti double microalloying on the grain structure and precipitates of hot compressed FeCrAl alloys
title_short Effects of Nb–Ti double microalloying on the grain structure and precipitates of hot compressed FeCrAl alloys
title_sort effects of nb ti double microalloying on the grain structure and precipitates of hot compressed fecral alloys
topic Hot compression
Double microalloy control
Microalloy precipitates
Grain growth
url http://www.sciencedirect.com/science/article/pii/S223878542500016X
work_keys_str_mv AT xingfan effectsofnbtidoublemicroalloyingonthegrainstructureandprecipitatesofhotcompressedfecralalloys
AT feiwang effectsofnbtidoublemicroalloyingonthegrainstructureandprecipitatesofhotcompressedfecralalloys
AT hongmingwang effectsofnbtidoublemicroalloyingonthegrainstructureandprecipitatesofhotcompressedfecralalloys
AT bowenzhao effectsofnbtidoublemicroalloyingonthegrainstructureandprecipitatesofhotcompressedfecralalloys
AT runzeli effectsofnbtidoublemicroalloyingonthegrainstructureandprecipitatesofhotcompressedfecralalloys
AT junzhou effectsofnbtidoublemicroalloyingonthegrainstructureandprecipitatesofhotcompressedfecralalloys