Assessment of changes occurring in biochar/zeolite substrates used in the vegetation-activated sludge process in the treatment of leachate from landfills

Leachate management remains one of the key technological challenges in landfill operations. There is a growing need for methods that can effectively treat leachate directly at its source. One promising approach is the vegetation-activated sludge process (V-ASP), which integrates constructed wetlands...

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Main Authors: Aleksandra Wdowczyk, Agata Szymańska-Pulikowska, Jacek Chęcmanowski, Krzysztof Kierzek, Paweł Wiercik
Format: Article
Language:English
Published: Elsevier 2025-06-01
Series:Water Resources and Industry
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Online Access:http://www.sciencedirect.com/science/article/pii/S2212371725000046
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author Aleksandra Wdowczyk
Agata Szymańska-Pulikowska
Jacek Chęcmanowski
Krzysztof Kierzek
Paweł Wiercik
author_facet Aleksandra Wdowczyk
Agata Szymańska-Pulikowska
Jacek Chęcmanowski
Krzysztof Kierzek
Paweł Wiercik
author_sort Aleksandra Wdowczyk
collection DOAJ
description Leachate management remains one of the key technological challenges in landfill operations. There is a growing need for methods that can effectively treat leachate directly at its source. One promising approach is the vegetation-activated sludge process (V-ASP), which integrates constructed wetlands with conventional activated sludge treatment. Given the limited research on V-ASP systems, this study explored the potential of low-cost adsorbent materials—zeolite and sunflower husk biochar—to enhance leachate treatment. The absorption properties of these materials in various V-ASP configurations were analysed using Fourier Transform Infrared Spectroscopy (FTIR) and scanning electron microscope (SEM) to better understand the mechanisms involved in pollutant removal. For most of the parameters analysed (Chemical Oxygen Demand, total nitrogen, organic nitrogen, total phosphorus, nitrites, sulfates, chlorides, Zn, Cu, Ni), the best reductions were achieved with zeolite substrates at a hydraulic retention time (HRT) of 14 days. Ammonium nitrogen removal was highly efficient, maintaining rates between 99 % and 99.8 % throughout the entire experimental period. Total nitrogen removal varied, with a minimum reduction of 13.1 % and a maximum of over 74 %. FTIR spectra confirmed alterations in the functional groups and surface characteristics of zeolite and biochar, evidenced by shifts in the bands of functional groups due to absorption. These findings could help improve leachate management strategies and aid in designing treatment systems that can be deployed directly at landfill sites.
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spelling doaj-art-c32e45ed494946f28150dc60d9875da22025-08-20T02:02:24ZengElsevierWater Resources and Industry2212-37172025-06-013310028010.1016/j.wri.2025.100280Assessment of changes occurring in biochar/zeolite substrates used in the vegetation-activated sludge process in the treatment of leachate from landfillsAleksandra Wdowczyk0Agata Szymańska-Pulikowska1Jacek Chęcmanowski2Krzysztof Kierzek3Paweł Wiercik4Wrocław University of Environmental and Life Sciences, Department of Environmental Protection and Development, Pl. Grunwaldzki 24, 50–363, Wrocław, Poland; Corresponding author.Wrocław University of Environmental and Life Sciences, Institute of Environmental Engineering, Pl. Grunwaldzki 24, 50–363, Wrocław, PolandWrocław University of Science and Technology, Faculty of Chemistry, Department of Advanced Material Technologies, Wybrzeże Wyspiańskiego 27, 50-370, Wroclaw, PolandWrocław University of Science and Technology, Faculty of Chemistry, Department of Process Engineering and Technology of Polymer and Carbon Materials, Wybrzeże Wyspiańskiego 27, 50-370, Wroclaw, PolandWrocław University of Environmental and Life Sciences, Institute of Environmental Engineering, Pl. Grunwaldzki 24, 50–363, Wrocław, PolandLeachate management remains one of the key technological challenges in landfill operations. There is a growing need for methods that can effectively treat leachate directly at its source. One promising approach is the vegetation-activated sludge process (V-ASP), which integrates constructed wetlands with conventional activated sludge treatment. Given the limited research on V-ASP systems, this study explored the potential of low-cost adsorbent materials—zeolite and sunflower husk biochar—to enhance leachate treatment. The absorption properties of these materials in various V-ASP configurations were analysed using Fourier Transform Infrared Spectroscopy (FTIR) and scanning electron microscope (SEM) to better understand the mechanisms involved in pollutant removal. For most of the parameters analysed (Chemical Oxygen Demand, total nitrogen, organic nitrogen, total phosphorus, nitrites, sulfates, chlorides, Zn, Cu, Ni), the best reductions were achieved with zeolite substrates at a hydraulic retention time (HRT) of 14 days. Ammonium nitrogen removal was highly efficient, maintaining rates between 99 % and 99.8 % throughout the entire experimental period. Total nitrogen removal varied, with a minimum reduction of 13.1 % and a maximum of over 74 %. FTIR spectra confirmed alterations in the functional groups and surface characteristics of zeolite and biochar, evidenced by shifts in the bands of functional groups due to absorption. These findings could help improve leachate management strategies and aid in designing treatment systems that can be deployed directly at landfill sites.http://www.sciencedirect.com/science/article/pii/S2212371725000046Leachate treatmentSubstrateVegetation-activated sludge processFourier transform infrared spectroscopyScanning electron microscope
spellingShingle Aleksandra Wdowczyk
Agata Szymańska-Pulikowska
Jacek Chęcmanowski
Krzysztof Kierzek
Paweł Wiercik
Assessment of changes occurring in biochar/zeolite substrates used in the vegetation-activated sludge process in the treatment of leachate from landfills
Water Resources and Industry
Leachate treatment
Substrate
Vegetation-activated sludge process
Fourier transform infrared spectroscopy
Scanning electron microscope
title Assessment of changes occurring in biochar/zeolite substrates used in the vegetation-activated sludge process in the treatment of leachate from landfills
title_full Assessment of changes occurring in biochar/zeolite substrates used in the vegetation-activated sludge process in the treatment of leachate from landfills
title_fullStr Assessment of changes occurring in biochar/zeolite substrates used in the vegetation-activated sludge process in the treatment of leachate from landfills
title_full_unstemmed Assessment of changes occurring in biochar/zeolite substrates used in the vegetation-activated sludge process in the treatment of leachate from landfills
title_short Assessment of changes occurring in biochar/zeolite substrates used in the vegetation-activated sludge process in the treatment of leachate from landfills
title_sort assessment of changes occurring in biochar zeolite substrates used in the vegetation activated sludge process in the treatment of leachate from landfills
topic Leachate treatment
Substrate
Vegetation-activated sludge process
Fourier transform infrared spectroscopy
Scanning electron microscope
url http://www.sciencedirect.com/science/article/pii/S2212371725000046
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