Achieving excellent strength-ductility synergy by adding carbon to a BCC structured low-cost Fe-based medium entropy alloy

The microstructure and tensile properties of C-doped Fe-based medium entropy alloys with a single BCC structure were studied in this work. The addition of 0.25 at.% and 0.5 at.% C induces a significant transformation of the Fe64Ni11Cr15Si7Al3 alloy from a single-phase BCC to a dual-phase FCC + BCC s...

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Main Authors: Chengfu Han, Zhenyu Du, Suo Zhang, Zhenyan Zhang, Shaojie Wu, Tan Wang, Yongfu Cai, Chen Chen, Ran Wei, Fushan Li
Format: Article
Language:English
Published: Elsevier 2025-05-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425011913
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author Chengfu Han
Zhenyu Du
Suo Zhang
Zhenyan Zhang
Shaojie Wu
Tan Wang
Yongfu Cai
Chen Chen
Ran Wei
Fushan Li
author_facet Chengfu Han
Zhenyu Du
Suo Zhang
Zhenyan Zhang
Shaojie Wu
Tan Wang
Yongfu Cai
Chen Chen
Ran Wei
Fushan Li
author_sort Chengfu Han
collection DOAJ
description The microstructure and tensile properties of C-doped Fe-based medium entropy alloys with a single BCC structure were studied in this work. The addition of 0.25 at.% and 0.5 at.% C induces a significant transformation of the Fe64Ni11Cr15Si7Al3 alloy from a single-phase BCC to a dual-phase FCC + BCC structure, accompanied by the precipitation of B2 (NiAl) nanoparticles within the BCC phase. Following thermomechanical treatment, the (Fe64Ni11Cr15Si7Al3)99.75C0.25 alloy shows excellent tensile properties at 77 K, achieving a yield strength (YS) of 1550 ± 34 MPa, ultimate tensile strength (UTS) of 1926 ± 33 MPa, and uniform elongation (UE) of 25 ± 6 %. These properties are attributed to ultrafine grains, carbon solution, high-density dislocations, B2 (NiAl) nano precipitates, and transformation - induced plasticity (TRIP). At 298 K, the same alloy retains substantial mechanical performance with a YS of 1054 ± 14 MPa, UTS of 1203 ± 6 MPa, and UE of 15 ± 1 %, without the TRIP effect. In contrast, the (Fe64Ni11Cr15Si7Al3)99.5C0.5 alloy exhibits sudden fracture at 77 K, likely due to carbide formation. This work provides a novel strategy for overcoming cold working challenges in single BCC alloys, thereby promoting their development and potential applications in structural materials.
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spelling doaj-art-c2bfe5a7cab24b058ef0789df5dfdf8c2025-08-20T01:50:49ZengElsevierJournal of Materials Research and Technology2238-78542025-05-01367913792410.1016/j.jmrt.2025.05.037Achieving excellent strength-ductility synergy by adding carbon to a BCC structured low-cost Fe-based medium entropy alloyChengfu Han0Zhenyu Du1Suo Zhang2Zhenyan Zhang3Shaojie Wu4Tan Wang5Yongfu Cai6Chen Chen7Ran Wei8Fushan Li9School of Materials Science and Engineering, Zhengzhou University, Zhengzhou, 450001, ChinaSchool of Materials Science and Engineering, Zhengzhou University, Zhengzhou, 450001, ChinaSchool of Materials Science and Engineering, Zhengzhou University, Zhengzhou, 450001, ChinaSchool of Materials Science and Engineering, Zhengzhou University, Zhengzhou, 450001, ChinaSchool of Materials Science and Engineering, Zhengzhou University, Zhengzhou, 450001, ChinaSchool of Materials Science and Engineering, Zhengzhou University, Zhengzhou, 450001, ChinaSchool of Materials Science and Engineering, Zhengzhou University, Zhengzhou, 450001, ChinaCorresponding author.; School of Materials Science and Engineering, Zhengzhou University, Zhengzhou, 450001, ChinaCorresponding author.; School of Materials Science and Engineering, Zhengzhou University, Zhengzhou, 450001, ChinaCorresponding author.; School of Materials Science and Engineering, Zhengzhou University, Zhengzhou, 450001, ChinaThe microstructure and tensile properties of C-doped Fe-based medium entropy alloys with a single BCC structure were studied in this work. The addition of 0.25 at.% and 0.5 at.% C induces a significant transformation of the Fe64Ni11Cr15Si7Al3 alloy from a single-phase BCC to a dual-phase FCC + BCC structure, accompanied by the precipitation of B2 (NiAl) nanoparticles within the BCC phase. Following thermomechanical treatment, the (Fe64Ni11Cr15Si7Al3)99.75C0.25 alloy shows excellent tensile properties at 77 K, achieving a yield strength (YS) of 1550 ± 34 MPa, ultimate tensile strength (UTS) of 1926 ± 33 MPa, and uniform elongation (UE) of 25 ± 6 %. These properties are attributed to ultrafine grains, carbon solution, high-density dislocations, B2 (NiAl) nano precipitates, and transformation - induced plasticity (TRIP). At 298 K, the same alloy retains substantial mechanical performance with a YS of 1054 ± 14 MPa, UTS of 1203 ± 6 MPa, and UE of 15 ± 1 %, without the TRIP effect. In contrast, the (Fe64Ni11Cr15Si7Al3)99.5C0.5 alloy exhibits sudden fracture at 77 K, likely due to carbide formation. This work provides a novel strategy for overcoming cold working challenges in single BCC alloys, thereby promoting their development and potential applications in structural materials.http://www.sciencedirect.com/science/article/pii/S2238785425011913C-dopingFe-based medium entropy alloyDual-phaseB2 precipitationsTensile properties
spellingShingle Chengfu Han
Zhenyu Du
Suo Zhang
Zhenyan Zhang
Shaojie Wu
Tan Wang
Yongfu Cai
Chen Chen
Ran Wei
Fushan Li
Achieving excellent strength-ductility synergy by adding carbon to a BCC structured low-cost Fe-based medium entropy alloy
Journal of Materials Research and Technology
C-doping
Fe-based medium entropy alloy
Dual-phase
B2 precipitations
Tensile properties
title Achieving excellent strength-ductility synergy by adding carbon to a BCC structured low-cost Fe-based medium entropy alloy
title_full Achieving excellent strength-ductility synergy by adding carbon to a BCC structured low-cost Fe-based medium entropy alloy
title_fullStr Achieving excellent strength-ductility synergy by adding carbon to a BCC structured low-cost Fe-based medium entropy alloy
title_full_unstemmed Achieving excellent strength-ductility synergy by adding carbon to a BCC structured low-cost Fe-based medium entropy alloy
title_short Achieving excellent strength-ductility synergy by adding carbon to a BCC structured low-cost Fe-based medium entropy alloy
title_sort achieving excellent strength ductility synergy by adding carbon to a bcc structured low cost fe based medium entropy alloy
topic C-doping
Fe-based medium entropy alloy
Dual-phase
B2 precipitations
Tensile properties
url http://www.sciencedirect.com/science/article/pii/S2238785425011913
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