Quantification of Sensitization in Aluminum–Magnesium Alloys Through Frequency-Dependent Ultrasonic Attenuation

Aluminum–Magnesium (Al–Mg) alloys undergo sensitization, i.e., the precipitations of β-phase (Al<sub>2</sub>Mg<sub>3</sub>) at the grain boundaries, when exposed to elevated temperature. This microstructural change increases the susceptibility of Al–Mg alloys to intergranular...

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Main Authors: Songwei Wang, Haiying Huang
Format: Article
Language:English
Published: MDPI AG 2025-06-01
Series:Sensors
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Online Access:https://www.mdpi.com/1424-8220/25/13/3983
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author Songwei Wang
Haiying Huang
author_facet Songwei Wang
Haiying Huang
author_sort Songwei Wang
collection DOAJ
description Aluminum–Magnesium (Al–Mg) alloys undergo sensitization, i.e., the precipitations of β-phase (Al<sub>2</sub>Mg<sub>3</sub>) at the grain boundaries, when exposed to elevated temperature. This microstructural change increases the susceptibility of Al–Mg alloys to intergranular corrosion, exfoliation, and stress corrosion cracking. This study introduces a time-frequency analysis (TFA) technique to determine the frequency-dependent ultrasonic attenuation parameter and correlate the frequency-attenuation slope to the Degree of Sensitization (DoS) developed in heat-treated Al–Mg alloy samples. Broadband pitch-catch signal was generated using a laser ultrasonic testing (LUT) system, from which the narrowband pitch-catch signal at different frequencies can be digitally generated. The attenuation parameters of sensitized Al–Mg samples were determined from these narrowband pitch-catch signals using the primary pulse-first echo (PP-FE) method. By identifying the frequency range within which the attenuation parameter is linearly proportional to the frequency, the slopes of the frequency-attenuation relationship were determined and correlated with the DoS values of the sample plates. The experimental results validate that the frequency-attenuation slope has a higher sensitivity and lower scattering as compared to other conventional ultrasonic attenuation measurement techniques.
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spelling doaj-art-c2857a90e50d459ba8345dabf348d3f12025-08-20T03:28:58ZengMDPI AGSensors1424-82202025-06-012513398310.3390/s25133983Quantification of Sensitization in Aluminum–Magnesium Alloys Through Frequency-Dependent Ultrasonic AttenuationSongwei Wang0Haiying Huang1Department of Mechanical and Aerospace Engineering, University of Texas at Arlington, 500 W. First Street, Arlington, TX 76010, USADepartment of Mechanical and Aerospace Engineering, University of Texas at Arlington, 500 W. First Street, Arlington, TX 76010, USAAluminum–Magnesium (Al–Mg) alloys undergo sensitization, i.e., the precipitations of β-phase (Al<sub>2</sub>Mg<sub>3</sub>) at the grain boundaries, when exposed to elevated temperature. This microstructural change increases the susceptibility of Al–Mg alloys to intergranular corrosion, exfoliation, and stress corrosion cracking. This study introduces a time-frequency analysis (TFA) technique to determine the frequency-dependent ultrasonic attenuation parameter and correlate the frequency-attenuation slope to the Degree of Sensitization (DoS) developed in heat-treated Al–Mg alloy samples. Broadband pitch-catch signal was generated using a laser ultrasonic testing (LUT) system, from which the narrowband pitch-catch signal at different frequencies can be digitally generated. The attenuation parameters of sensitized Al–Mg samples were determined from these narrowband pitch-catch signals using the primary pulse-first echo (PP-FE) method. By identifying the frequency range within which the attenuation parameter is linearly proportional to the frequency, the slopes of the frequency-attenuation relationship were determined and correlated with the DoS values of the sample plates. The experimental results validate that the frequency-attenuation slope has a higher sensitivity and lower scattering as compared to other conventional ultrasonic attenuation measurement techniques.https://www.mdpi.com/1424-8220/25/13/3983Aluminum–Magnesium alloyfrequency-dependent attenuationlaser ultrasonic testingmaterial characterizationnon-destructive testingsensitization
spellingShingle Songwei Wang
Haiying Huang
Quantification of Sensitization in Aluminum–Magnesium Alloys Through Frequency-Dependent Ultrasonic Attenuation
Sensors
Aluminum–Magnesium alloy
frequency-dependent attenuation
laser ultrasonic testing
material characterization
non-destructive testing
sensitization
title Quantification of Sensitization in Aluminum–Magnesium Alloys Through Frequency-Dependent Ultrasonic Attenuation
title_full Quantification of Sensitization in Aluminum–Magnesium Alloys Through Frequency-Dependent Ultrasonic Attenuation
title_fullStr Quantification of Sensitization in Aluminum–Magnesium Alloys Through Frequency-Dependent Ultrasonic Attenuation
title_full_unstemmed Quantification of Sensitization in Aluminum–Magnesium Alloys Through Frequency-Dependent Ultrasonic Attenuation
title_short Quantification of Sensitization in Aluminum–Magnesium Alloys Through Frequency-Dependent Ultrasonic Attenuation
title_sort quantification of sensitization in aluminum magnesium alloys through frequency dependent ultrasonic attenuation
topic Aluminum–Magnesium alloy
frequency-dependent attenuation
laser ultrasonic testing
material characterization
non-destructive testing
sensitization
url https://www.mdpi.com/1424-8220/25/13/3983
work_keys_str_mv AT songweiwang quantificationofsensitizationinaluminummagnesiumalloysthroughfrequencydependentultrasonicattenuation
AT haiyinghuang quantificationofsensitizationinaluminummagnesiumalloysthroughfrequencydependentultrasonicattenuation