The Effect of Water on the Tin Electrodeposition from [Bmim]HSO4 Ionic Liquid

The electrodeposition of tin from SnO in ionic liquid 1-butyl-3-methylimidazolium hydrogen sulfate ([Bmim]HSO4) in the presence of water at different cathodic potential was investigated. With the addition of water to [Bmim]HSO4 ionic liquid, the electrochemical window of the electrolyte decreases an...

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Main Authors: Jie Tang, DongLiang Lv, CunYing Xu, YiXin Hua, QiBo Zhang, PingZhao Niu, XiaoLin Zhu
Format: Article
Language:English
Published: Wiley 2018-01-01
Series:International Journal of Electrochemistry
Online Access:http://dx.doi.org/10.1155/2018/1210394
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author Jie Tang
DongLiang Lv
CunYing Xu
YiXin Hua
QiBo Zhang
PingZhao Niu
XiaoLin Zhu
author_facet Jie Tang
DongLiang Lv
CunYing Xu
YiXin Hua
QiBo Zhang
PingZhao Niu
XiaoLin Zhu
author_sort Jie Tang
collection DOAJ
description The electrodeposition of tin from SnO in ionic liquid 1-butyl-3-methylimidazolium hydrogen sulfate ([Bmim]HSO4) in the presence of water at different cathodic potential was investigated. With the addition of water to [Bmim]HSO4 ionic liquid, the electrochemical window of the electrolyte decreases and the reduction potential of Sn(II) positively shifts. The water content of ionic liquid electrolyte has a distinct effect on morphology of the deposits. As water content increased from 0 to 50% (v/v), the morphology of deposits varies from granular to hexagonal rod-like, then to hollow tubular, and finally to wire-like. The XRD phase analysis showed that both Sn and CuSn alloys were deposited in ionic liquid/water mixtures. However, in dried ionic liquids only Cu3Sn was obtained, surprisingly. The difference in the structure might be attributed to the various interactions of the ions with the Cu substrate. In addition, the deposition potential was found to play a significant role in the morphology of deposits.
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id doaj-art-c12c49294aee42ed8f5cfccf5d64b48a
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issn 2090-3529
2090-3537
language English
publishDate 2018-01-01
publisher Wiley
record_format Article
series International Journal of Electrochemistry
spelling doaj-art-c12c49294aee42ed8f5cfccf5d64b48a2025-08-20T02:19:23ZengWileyInternational Journal of Electrochemistry2090-35292090-35372018-01-01201810.1155/2018/12103941210394The Effect of Water on the Tin Electrodeposition from [Bmim]HSO4 Ionic LiquidJie Tang0DongLiang Lv1CunYing Xu2YiXin Hua3QiBo Zhang4PingZhao Niu5XiaoLin Zhu6Department of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, ChinaDepartment of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, ChinaDepartment of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, ChinaDepartment of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, ChinaDepartment of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, ChinaDepartment of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, ChinaDepartment of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, ChinaThe electrodeposition of tin from SnO in ionic liquid 1-butyl-3-methylimidazolium hydrogen sulfate ([Bmim]HSO4) in the presence of water at different cathodic potential was investigated. With the addition of water to [Bmim]HSO4 ionic liquid, the electrochemical window of the electrolyte decreases and the reduction potential of Sn(II) positively shifts. The water content of ionic liquid electrolyte has a distinct effect on morphology of the deposits. As water content increased from 0 to 50% (v/v), the morphology of deposits varies from granular to hexagonal rod-like, then to hollow tubular, and finally to wire-like. The XRD phase analysis showed that both Sn and CuSn alloys were deposited in ionic liquid/water mixtures. However, in dried ionic liquids only Cu3Sn was obtained, surprisingly. The difference in the structure might be attributed to the various interactions of the ions with the Cu substrate. In addition, the deposition potential was found to play a significant role in the morphology of deposits.http://dx.doi.org/10.1155/2018/1210394
spellingShingle Jie Tang
DongLiang Lv
CunYing Xu
YiXin Hua
QiBo Zhang
PingZhao Niu
XiaoLin Zhu
The Effect of Water on the Tin Electrodeposition from [Bmim]HSO4 Ionic Liquid
International Journal of Electrochemistry
title The Effect of Water on the Tin Electrodeposition from [Bmim]HSO4 Ionic Liquid
title_full The Effect of Water on the Tin Electrodeposition from [Bmim]HSO4 Ionic Liquid
title_fullStr The Effect of Water on the Tin Electrodeposition from [Bmim]HSO4 Ionic Liquid
title_full_unstemmed The Effect of Water on the Tin Electrodeposition from [Bmim]HSO4 Ionic Liquid
title_short The Effect of Water on the Tin Electrodeposition from [Bmim]HSO4 Ionic Liquid
title_sort effect of water on the tin electrodeposition from bmim hso4 ionic liquid
url http://dx.doi.org/10.1155/2018/1210394
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