Comparative assessment of calcium aluminate cement and potassium-metakaolin-based geopolymer as binders in high-alumina refractories

Abstract This investigation demonstrated the effects of calcium aluminate cement’s total or partial replacement with a potassium-metakaolin-based geopolymeric binder (K-GP) in high-alumina castables. Experimental measurements were conducted to analyze the produced samples’ processing, microstructure...

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Main Authors: B. P. Bezerra, A. P. Luz
Format: Article
Language:English
Published: Associação Brasileira de Cerâmica 2025-03-01
Series:Cerâmica
Subjects:
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132025000100307&tlng=en
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author B. P. Bezerra
A. P. Luz
author_facet B. P. Bezerra
A. P. Luz
author_sort B. P. Bezerra
collection DOAJ
description Abstract This investigation demonstrated the effects of calcium aluminate cement’s total or partial replacement with a potassium-metakaolin-based geopolymeric binder (K-GP) in high-alumina castables. Experimental measurements were conducted to analyze the produced samples’ processing, microstructure, and properties after curing and firing (800-1400 °C). The results highlighted K-GP as a viable binder option for producing cement-free refractories. After firing at 1100-1400 °C, the improved properties of geopolymer-bonded refractories were attributed to their complex resultant microstructure, comprising alumina particles strongly adhered by a glassy phase and contained randomly distributed clusters of kaliophilite and/or leucite grains within the ceramic matrix. After firing at 1250 °C, the samples exhibited a promising set of properties: high thermal shock resistance, modulus of rupture of 17.01 MPa, Young’s modulus of 67.15 GPa, porosity of 16.85%, density of 2.87 g/cm³, and linear shrinkage of 0.33%. These properties are suitable for applications at intermediate temperatures (i.e., petrochemical and non-ferrous industries).
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language English
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publisher Associação Brasileira de Cerâmica
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spelling doaj-art-c07fe3bc3cbb4b62ba016bc9f3f118c32025-08-20T02:53:44ZengAssociação Brasileira de CerâmicaCerâmica1678-45532025-03-017110.1590/mkwv7164Comparative assessment of calcium aluminate cement and potassium-metakaolin-based geopolymer as binders in high-alumina refractoriesB. P. BezerraA. P. Luzhttps://orcid.org/0000-0002-5941-5388Abstract This investigation demonstrated the effects of calcium aluminate cement’s total or partial replacement with a potassium-metakaolin-based geopolymeric binder (K-GP) in high-alumina castables. Experimental measurements were conducted to analyze the produced samples’ processing, microstructure, and properties after curing and firing (800-1400 °C). The results highlighted K-GP as a viable binder option for producing cement-free refractories. After firing at 1100-1400 °C, the improved properties of geopolymer-bonded refractories were attributed to their complex resultant microstructure, comprising alumina particles strongly adhered by a glassy phase and contained randomly distributed clusters of kaliophilite and/or leucite grains within the ceramic matrix. After firing at 1250 °C, the samples exhibited a promising set of properties: high thermal shock resistance, modulus of rupture of 17.01 MPa, Young’s modulus of 67.15 GPa, porosity of 16.85%, density of 2.87 g/cm³, and linear shrinkage of 0.33%. These properties are suitable for applications at intermediate temperatures (i.e., petrochemical and non-ferrous industries).http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132025000100307&tlng=enGeopolymerBinderCastableMetakaolinAlumina
spellingShingle B. P. Bezerra
A. P. Luz
Comparative assessment of calcium aluminate cement and potassium-metakaolin-based geopolymer as binders in high-alumina refractories
Cerâmica
Geopolymer
Binder
Castable
Metakaolin
Alumina
title Comparative assessment of calcium aluminate cement and potassium-metakaolin-based geopolymer as binders in high-alumina refractories
title_full Comparative assessment of calcium aluminate cement and potassium-metakaolin-based geopolymer as binders in high-alumina refractories
title_fullStr Comparative assessment of calcium aluminate cement and potassium-metakaolin-based geopolymer as binders in high-alumina refractories
title_full_unstemmed Comparative assessment of calcium aluminate cement and potassium-metakaolin-based geopolymer as binders in high-alumina refractories
title_short Comparative assessment of calcium aluminate cement and potassium-metakaolin-based geopolymer as binders in high-alumina refractories
title_sort comparative assessment of calcium aluminate cement and potassium metakaolin based geopolymer as binders in high alumina refractories
topic Geopolymer
Binder
Castable
Metakaolin
Alumina
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132025000100307&tlng=en
work_keys_str_mv AT bpbezerra comparativeassessmentofcalciumaluminatecementandpotassiummetakaolinbasedgeopolymerasbindersinhighaluminarefractories
AT apluz comparativeassessmentofcalciumaluminatecementandpotassiummetakaolinbasedgeopolymerasbindersinhighaluminarefractories