Phase transformations during the doping of zinc chloride and silver nitrate into calcium phosphates

This article shows the results of a study on a biocomposite material based on calcium phosphate doped with ZnCl and AgNO3. Calcium phosphates are mainly used in dentistry and orthopedics due to their excellent biocompatibility, osteoconductive properties and similarity to the inorganic components o...

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Main Authors: А.Н. Сағидұғұмар, А. Тұрлыбекұлы, Д. Догадкин, А.Д. Погребняк, Н. Қантай, А. Садибеков
Format: Article
Language:English
Published: Academician Ye.A. Buketov Karaganda University 2022-06-01
Series:Қарағанды университетінің хабаршысы. Физика сериясы
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Online Access:https://phs.buketov.edu.kz/index.php/physics-vestnik/article/view/441
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author А.Н. Сағидұғұмар
А. Тұрлыбекұлы
Д. Догадкин
А.Д. Погребняк
Н. Қантай
А. Садибеков
author_facet А.Н. Сағидұғұмар
А. Тұрлыбекұлы
Д. Догадкин
А.Д. Погребняк
Н. Қантай
А. Садибеков
author_sort А.Н. Сағидұғұмар
collection DOAJ
description This article shows the results of a study on a biocomposite material based on calcium phosphate doped with ZnCl and AgNO3. Calcium phosphates are mainly used in dentistry and orthopedics due to their excellent biocompatibility, osteoconductive properties and similarity to the inorganic components of human bone. The main objective of the study is to investigate the morphology, elemental and phase composition, and physicochemical properties of the obtained material. The test material is obtained in the form of a suspension and subjected to ultrasonic treatment. The microstructure and phase composition of the obtained biocomposites are studied by SEM, XRD, FTIR methods. It is possible to obtain dicalcium phosphate dihydrate (DCPD) by the presented methods, and the results demonstrate a partial replacement of calcium atoms by zinc atoms. Xray phase analysis shows that Ca(HPO4) (H2O)2 phases as well as CaZn2 (PO4)2 (H2O)2 and AgCl phases were formed during the reaction. Fourier transform infrared spectroscopy revealed that the obtained samples contain the groups HPO42 and PO43, with the group PO42 replacing the group CO32. The biocomposite materials could be of great interest in the biomedical field, including the development of coatings that prevent or delay the development of bacterial biofilm.
format Article
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issn 2518-7198
2663-5089
language English
publishDate 2022-06-01
publisher Academician Ye.A. Buketov Karaganda University
record_format Article
series Қарағанды университетінің хабаршысы. Физика сериясы
spelling doaj-art-c0530f53b6ab4e3fbcf0d7c29279fed22025-08-20T02:27:05ZengAcademician Ye.A. Buketov Karaganda UniversityҚарағанды университетінің хабаршысы. Физика сериясы2518-71982663-50892022-06-01106210.31489/2022ph2/18-23Phase transformations during the doping of zinc chloride and silver nitrate into calcium phosphatesА.Н. СағидұғұмарА. ТұрлыбекұлыД. ДогадкинА.Д. ПогребнякН. ҚантайА. Садибеков This article shows the results of a study on a biocomposite material based on calcium phosphate doped with ZnCl and AgNO3. Calcium phosphates are mainly used in dentistry and orthopedics due to their excellent biocompatibility, osteoconductive properties and similarity to the inorganic components of human bone. The main objective of the study is to investigate the morphology, elemental and phase composition, and physicochemical properties of the obtained material. The test material is obtained in the form of a suspension and subjected to ultrasonic treatment. The microstructure and phase composition of the obtained biocomposites are studied by SEM, XRD, FTIR methods. It is possible to obtain dicalcium phosphate dihydrate (DCPD) by the presented methods, and the results demonstrate a partial replacement of calcium atoms by zinc atoms. Xray phase analysis shows that Ca(HPO4) (H2O)2 phases as well as CaZn2 (PO4)2 (H2O)2 and AgCl phases were formed during the reaction. Fourier transform infrared spectroscopy revealed that the obtained samples contain the groups HPO42 and PO43, with the group PO42 replacing the group CO32. The biocomposite materials could be of great interest in the biomedical field, including the development of coatings that prevent or delay the development of bacterial biofilm. https://phs.buketov.edu.kz/index.php/physics-vestnik/article/view/441biocomposite materialcalcium phosphatesmorphologyAg-dopedhydroxyapatitebioactivity
spellingShingle А.Н. Сағидұғұмар
А. Тұрлыбекұлы
Д. Догадкин
А.Д. Погребняк
Н. Қантай
А. Садибеков
Phase transformations during the doping of zinc chloride and silver nitrate into calcium phosphates
Қарағанды университетінің хабаршысы. Физика сериясы
biocomposite material
calcium phosphates
morphology
Ag-doped
hydroxyapatite
bioactivity
title Phase transformations during the doping of zinc chloride and silver nitrate into calcium phosphates
title_full Phase transformations during the doping of zinc chloride and silver nitrate into calcium phosphates
title_fullStr Phase transformations during the doping of zinc chloride and silver nitrate into calcium phosphates
title_full_unstemmed Phase transformations during the doping of zinc chloride and silver nitrate into calcium phosphates
title_short Phase transformations during the doping of zinc chloride and silver nitrate into calcium phosphates
title_sort phase transformations during the doping of zinc chloride and silver nitrate into calcium phosphates
topic biocomposite material
calcium phosphates
morphology
Ag-doped
hydroxyapatite
bioactivity
url https://phs.buketov.edu.kz/index.php/physics-vestnik/article/view/441
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