Study of the Influence of Annealing Temperature on the Structural Properties for (Ni1-xZnxFe2O4) Compounds
Nikel-Znic ferrites with chemical formula Ni1-xZnxFe2O4 for (x:0.00 , 0.5 and 1) were synthesis by chemical co-precipitation method at various annealing temperatures (27°C,300°C,600°C,900°C, 1200°C) for (4h). The samples were examined via X-ray diffraction patterns. The XRD pattern confirm the form...
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| Language: | English |
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Tikrit University
2020-03-01
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| Series: | Tikrit Journal of Pure Science |
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| Online Access: | https://tjpsj.org/index.php/tjps/article/view/253 |
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| author | Najat A. Dahham Abdulsamee F. A. Albayati Inteesar A. Hamed |
| author_facet | Najat A. Dahham Abdulsamee F. A. Albayati Inteesar A. Hamed |
| author_sort | Najat A. Dahham |
| collection | DOAJ |
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Nikel-Znic ferrites with chemical formula Ni1-xZnxFe2O4 for (x:0.00 , 0.5 and 1) were synthesis by chemical co-precipitation method at various annealing temperatures (27°C,300°C,600°C,900°C, 1200°C) for (4h). The samples were examined via X-ray diffraction patterns. The XRD pattern confirm the formation of face centered cubic structure (fcc) for all samples. The particle size, lattice parameter, theoretical density and porosity were also measured by X-ray diffraction, and bulk density. It is noted that granular particle size increases with increasing annealing temperature, while decreasing lattice constant, theoretical density and porosity with increasing annealing temperature. The homogeneity, regularity, particle size and the roughness of sample surfaces were calculated using atomic power microscope technique.
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| format | Article |
| id | doaj-art-bfcec168aaaa4d2e8065a1687685c4a3 |
| institution | Kabale University |
| issn | 1813-1662 2415-1726 |
| language | English |
| publishDate | 2020-03-01 |
| publisher | Tikrit University |
| record_format | Article |
| series | Tikrit Journal of Pure Science |
| spelling | doaj-art-bfcec168aaaa4d2e8065a1687685c4a32025-08-20T03:49:56ZengTikrit UniversityTikrit Journal of Pure Science1813-16622415-17262020-03-0125310.25130/tjps.v25i3.253Study of the Influence of Annealing Temperature on the Structural Properties for (Ni1-xZnxFe2O4) CompoundsNajat A. DahhamAbdulsamee F. A. AlbayatiInteesar A. Hamed Nikel-Znic ferrites with chemical formula Ni1-xZnxFe2O4 for (x:0.00 , 0.5 and 1) were synthesis by chemical co-precipitation method at various annealing temperatures (27°C,300°C,600°C,900°C, 1200°C) for (4h). The samples were examined via X-ray diffraction patterns. The XRD pattern confirm the formation of face centered cubic structure (fcc) for all samples. The particle size, lattice parameter, theoretical density and porosity were also measured by X-ray diffraction, and bulk density. It is noted that granular particle size increases with increasing annealing temperature, while decreasing lattice constant, theoretical density and porosity with increasing annealing temperature. The homogeneity, regularity, particle size and the roughness of sample surfaces were calculated using atomic power microscope technique. https://tjpsj.org/index.php/tjps/article/view/253Nikel – Zinc ferriteschemical precipitation methodXRDAFM analysis |
| spellingShingle | Najat A. Dahham Abdulsamee F. A. Albayati Inteesar A. Hamed Study of the Influence of Annealing Temperature on the Structural Properties for (Ni1-xZnxFe2O4) Compounds Tikrit Journal of Pure Science Nikel – Zinc ferrites chemical precipitation method XRD AFM analysis |
| title | Study of the Influence of Annealing Temperature on the Structural Properties for (Ni1-xZnxFe2O4) Compounds |
| title_full | Study of the Influence of Annealing Temperature on the Structural Properties for (Ni1-xZnxFe2O4) Compounds |
| title_fullStr | Study of the Influence of Annealing Temperature on the Structural Properties for (Ni1-xZnxFe2O4) Compounds |
| title_full_unstemmed | Study of the Influence of Annealing Temperature on the Structural Properties for (Ni1-xZnxFe2O4) Compounds |
| title_short | Study of the Influence of Annealing Temperature on the Structural Properties for (Ni1-xZnxFe2O4) Compounds |
| title_sort | study of the influence of annealing temperature on the structural properties for ni1 xznxfe2o4 compounds |
| topic | Nikel – Zinc ferrites chemical precipitation method XRD AFM analysis |
| url | https://tjpsj.org/index.php/tjps/article/view/253 |
| work_keys_str_mv | AT najatadahham studyoftheinfluenceofannealingtemperatureonthestructuralpropertiesforni1xznxfe2o4compounds AT abdulsameefaalbayati studyoftheinfluenceofannealingtemperatureonthestructuralpropertiesforni1xznxfe2o4compounds AT inteesarahamed studyoftheinfluenceofannealingtemperatureonthestructuralpropertiesforni1xznxfe2o4compounds |