Study of the possibility of obtaining composites based on nanoscale hydroxyapatite reinforced with titanium oxide and calcium fluoride

The article discusses the possibility of obtaining a hardened composite material with a porous structure based on nanostructured hydroxyapatite (HAP) synthesized by precipitation from a solution. The new material by the mechanochemical synthesis of hydroxyapatite with aluminum, silicon, nickel, hafn...

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Main Authors: E.A. Bogdanova, V.M. Skachkov, K.V. Nefedova
Format: Article
Language:Russian
Published: Tver State University 2024-12-01
Series:Физико-химические аспекты изучения кластеров, наноструктур и наноматериалов
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Online Access:https://physchemaspects.ru/2024/doi-10-26456-pcascnn-2024-16-779/?lang=en
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author E.A. Bogdanova
V.M. Skachkov
K.V. Nefedova
author_facet E.A. Bogdanova
V.M. Skachkov
K.V. Nefedova
author_sort E.A. Bogdanova
collection DOAJ
description The article discusses the possibility of obtaining a hardened composite material with a porous structure based on nanostructured hydroxyapatite (HAP) synthesized by precipitation from a solution. The new material by the mechanochemical synthesis of hydroxyapatite with aluminum, silicon, nickel, hafnium and titanium was obtained. The synthesized samples are certified using modern physical and chemical methods of analysis. The influence of the qualitative and quantitative composition of the composite on the sintering processes and the strength characteristics of the studied samples is shown. It has been experimentally established that the Ca10(PO4)6(OH)2 – 15%CaF2-15%TiOx. system is the most promising for the development of biocomposites based on it. Composite materials of this composition have a dense uniform structure with a high degree of crystallinity, with developed porosity, and are a promising material for further research in order to introduce it into medical practice. The possibility of practical application of the obtained composite material as a component of a bioactive coating is evaluated. A patent application has been filed for the developed composite material.
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issn 2226-4442
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language Russian
publishDate 2024-12-01
publisher Tver State University
record_format Article
series Физико-химические аспекты изучения кластеров, наноструктур и наноматериалов
spelling doaj-art-bf3348413efe4baaab0b9921dc2f67332025-08-20T02:39:51ZrusTver State UniversityФизико-химические аспекты изучения кластеров, наноструктур и наноматериалов2226-44422658-43602024-12-011677979310.26456/pcascnn/2024.16.779Study of the possibility of obtaining composites based on nanoscale hydroxyapatite reinforced with titanium oxide and calcium fluorideE.A. Bogdanova0V.M. Skachkov1K.V. Nefedova2Institute of Solid State Chemistry of the Ural Branch of RAS, JSC GiredmetInstitute of Solid State Chemistry of the Ural Branch of RASInstitute of Solid State Chemistry of the Ural Branch of RASThe article discusses the possibility of obtaining a hardened composite material with a porous structure based on nanostructured hydroxyapatite (HAP) synthesized by precipitation from a solution. The new material by the mechanochemical synthesis of hydroxyapatite with aluminum, silicon, nickel, hafnium and titanium was obtained. The synthesized samples are certified using modern physical and chemical methods of analysis. The influence of the qualitative and quantitative composition of the composite on the sintering processes and the strength characteristics of the studied samples is shown. It has been experimentally established that the Ca10(PO4)6(OH)2 – 15%CaF2-15%TiOx. system is the most promising for the development of biocomposites based on it. Composite materials of this composition have a dense uniform structure with a high degree of crystallinity, with developed porosity, and are a promising material for further research in order to introduce it into medical practice. The possibility of practical application of the obtained composite material as a component of a bioactive coating is evaluated. A patent application has been filed for the developed composite material. https://physchemaspects.ru/2024/doi-10-26456-pcascnn-2024-16-779/?lang=enhydroxyapatitefluorapatitetitanium oxidecalcium fluoridesinteringcomposite biomaterialsmicrohardnessbioactive coating
spellingShingle E.A. Bogdanova
V.M. Skachkov
K.V. Nefedova
Study of the possibility of obtaining composites based on nanoscale hydroxyapatite reinforced with titanium oxide and calcium fluoride
Физико-химические аспекты изучения кластеров, наноструктур и наноматериалов
hydroxyapatite
fluorapatite
titanium oxide
calcium fluoride
sintering
composite biomaterials
microhardness
bioactive coating
title Study of the possibility of obtaining composites based on nanoscale hydroxyapatite reinforced with titanium oxide and calcium fluoride
title_full Study of the possibility of obtaining composites based on nanoscale hydroxyapatite reinforced with titanium oxide and calcium fluoride
title_fullStr Study of the possibility of obtaining composites based on nanoscale hydroxyapatite reinforced with titanium oxide and calcium fluoride
title_full_unstemmed Study of the possibility of obtaining composites based on nanoscale hydroxyapatite reinforced with titanium oxide and calcium fluoride
title_short Study of the possibility of obtaining composites based on nanoscale hydroxyapatite reinforced with titanium oxide and calcium fluoride
title_sort study of the possibility of obtaining composites based on nanoscale hydroxyapatite reinforced with titanium oxide and calcium fluoride
topic hydroxyapatite
fluorapatite
titanium oxide
calcium fluoride
sintering
composite biomaterials
microhardness
bioactive coating
url https://physchemaspects.ru/2024/doi-10-26456-pcascnn-2024-16-779/?lang=en
work_keys_str_mv AT eabogdanova studyofthepossibilityofobtainingcompositesbasedonnanoscalehydroxyapatitereinforcedwithtitaniumoxideandcalciumfluoride
AT vmskachkov studyofthepossibilityofobtainingcompositesbasedonnanoscalehydroxyapatitereinforcedwithtitaniumoxideandcalciumfluoride
AT kvnefedova studyofthepossibilityofobtainingcompositesbasedonnanoscalehydroxyapatitereinforcedwithtitaniumoxideandcalciumfluoride