Wafer‐Scale Synthesis of Topological Insulator Sb2Te3 Thin Films

Abstract Recently, metal‐organic chemical vapor deposition (MOCVD) has been proven successful to grow topological insulators such as antimony telluride (Sb2Te3), with their use as efficient spin‐charge converters at room temperature also being reported. On the other hand, a wafer‐scale synthesis of...

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Main Authors: Ali Shafiei, Ahmad Fathi Hafshejani, Rehab M. G. Ahmed, Alessio Lamperti, Emanuele Longo, Lorenzo Locatelli, Christian Martella, Alessandro Molle, Graziella Tallarida, Carlo Zucchetti, Claudia Wiemer, Massimo Longo, Roberto Mantovan
Format: Article
Language:English
Published: Wiley-VCH 2025-06-01
Series:Advanced Materials Interfaces
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Online Access:https://doi.org/10.1002/admi.202400961
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author Ali Shafiei
Ahmad Fathi Hafshejani
Rehab M. G. Ahmed
Alessio Lamperti
Emanuele Longo
Lorenzo Locatelli
Christian Martella
Alessandro Molle
Graziella Tallarida
Carlo Zucchetti
Claudia Wiemer
Massimo Longo
Roberto Mantovan
author_facet Ali Shafiei
Ahmad Fathi Hafshejani
Rehab M. G. Ahmed
Alessio Lamperti
Emanuele Longo
Lorenzo Locatelli
Christian Martella
Alessandro Molle
Graziella Tallarida
Carlo Zucchetti
Claudia Wiemer
Massimo Longo
Roberto Mantovan
author_sort Ali Shafiei
collection DOAJ
description Abstract Recently, metal‐organic chemical vapor deposition (MOCVD) has been proven successful to grow topological insulators such as antimony telluride (Sb2Te3), with their use as efficient spin‐charge converters at room temperature also being reported. On the other hand, a wafer‐scale synthesis of Sb2Te3 thin films showing clear‐cut electrical conduction driven by topologically protected surface states is still missing. Within this work, the growth of Sb2Te3 thin films with variable thicknesses over 4‐inch (4″) wafer‐scale Si(111) substrates as conducted via MOCVD is reported. By performing magnetoconductance measurements, weak antilocalization phenomena are detected over the whole 4″ area, thus proving the possibility to produce wafer‐scale Sb2Te3 topological insulator thin films. Furthermore, comprehensive information on the variability of the functional properties of Sb2Te3 thin films with their morphological, chemical, and structural properties, as probed by scanning electron microscopy, X‐ray diffraction/reflectivity, atomic force microscopy, Raman spectroscopy, time‐of‐flight secondary ion mass spectrometry, and energy‐dispersive X‐ray analyses is reported. This work provides a breakthrough for the technology scale‐up of these novel materials to be employed in future spintronic devices as well as applications in nanoelectronics, thermoelectrics, and quantum computing.
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spelling doaj-art-befdeea22f1546f0a7104a158b9acbd92025-08-20T03:45:49ZengWiley-VCHAdvanced Materials Interfaces2196-73502025-06-011211n/an/a10.1002/admi.202400961Wafer‐Scale Synthesis of Topological Insulator Sb2Te3 Thin FilmsAli Shafiei0Ahmad Fathi Hafshejani1Rehab M. G. Ahmed2Alessio Lamperti3Emanuele Longo4Lorenzo Locatelli5Christian Martella6Alessandro Molle7Graziella Tallarida8Carlo Zucchetti9Claudia Wiemer10Massimo Longo11Roberto Mantovan12CNR‐IMM Unit of Agrate Brianza Via C. Olivetti 2 Agrate Brianza 20864 MB ItalyCNR‐IMM Unit of Agrate Brianza Via C. Olivetti 2 Agrate Brianza 20864 MB ItalyCNR‐IMM Unit of Agrate Brianza Via C. Olivetti 2 Agrate Brianza 20864 MB ItalyCNR‐IMM Unit of Agrate Brianza Via C. Olivetti 2 Agrate Brianza 20864 MB ItalyInstitute of Materials Science of Barcelona (ICMAB‐CSIC) Campus UAB Bellaterra 08193 Catalonia SpainCNR‐IMM Unit of Agrate Brianza Via C. Olivetti 2 Agrate Brianza 20864 MB ItalyCNR‐IMM Unit of Agrate Brianza Via C. Olivetti 2 Agrate Brianza 20864 MB ItalyCNR‐IMM Unit of Agrate Brianza Via C. Olivetti 2 Agrate Brianza 20864 MB ItalyCNR‐IMM Unit of Agrate Brianza Via C. Olivetti 2 Agrate Brianza 20864 MB ItalyPhysics Department Politecnico di Milano piazza Leonardo da Vinci 32 Milan 20133 ItalyCNR‐IMM Unit of Agrate Brianza Via C. Olivetti 2 Agrate Brianza 20864 MB ItalyCNR‐IMM Unit of Agrate Brianza Via C. Olivetti 2 Agrate Brianza 20864 MB ItalyCNR‐IMM Unit of Agrate Brianza Via C. Olivetti 2 Agrate Brianza 20864 MB ItalyAbstract Recently, metal‐organic chemical vapor deposition (MOCVD) has been proven successful to grow topological insulators such as antimony telluride (Sb2Te3), with their use as efficient spin‐charge converters at room temperature also being reported. On the other hand, a wafer‐scale synthesis of Sb2Te3 thin films showing clear‐cut electrical conduction driven by topologically protected surface states is still missing. Within this work, the growth of Sb2Te3 thin films with variable thicknesses over 4‐inch (4″) wafer‐scale Si(111) substrates as conducted via MOCVD is reported. By performing magnetoconductance measurements, weak antilocalization phenomena are detected over the whole 4″ area, thus proving the possibility to produce wafer‐scale Sb2Te3 topological insulator thin films. Furthermore, comprehensive information on the variability of the functional properties of Sb2Te3 thin films with their morphological, chemical, and structural properties, as probed by scanning electron microscopy, X‐ray diffraction/reflectivity, atomic force microscopy, Raman spectroscopy, time‐of‐flight secondary ion mass spectrometry, and energy‐dispersive X‐ray analyses is reported. This work provides a breakthrough for the technology scale‐up of these novel materials to be employed in future spintronic devices as well as applications in nanoelectronics, thermoelectrics, and quantum computing.https://doi.org/10.1002/admi.202400961chalcogenidesmagnetotransportMOCVDspintronicstopological insulatorsweak antilocalization
spellingShingle Ali Shafiei
Ahmad Fathi Hafshejani
Rehab M. G. Ahmed
Alessio Lamperti
Emanuele Longo
Lorenzo Locatelli
Christian Martella
Alessandro Molle
Graziella Tallarida
Carlo Zucchetti
Claudia Wiemer
Massimo Longo
Roberto Mantovan
Wafer‐Scale Synthesis of Topological Insulator Sb2Te3 Thin Films
Advanced Materials Interfaces
chalcogenides
magnetotransport
MOCVD
spintronics
topological insulators
weak antilocalization
title Wafer‐Scale Synthesis of Topological Insulator Sb2Te3 Thin Films
title_full Wafer‐Scale Synthesis of Topological Insulator Sb2Te3 Thin Films
title_fullStr Wafer‐Scale Synthesis of Topological Insulator Sb2Te3 Thin Films
title_full_unstemmed Wafer‐Scale Synthesis of Topological Insulator Sb2Te3 Thin Films
title_short Wafer‐Scale Synthesis of Topological Insulator Sb2Te3 Thin Films
title_sort wafer scale synthesis of topological insulator sb2te3 thin films
topic chalcogenides
magnetotransport
MOCVD
spintronics
topological insulators
weak antilocalization
url https://doi.org/10.1002/admi.202400961
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